scholarly journals X-ray Raman scattering for bulk chemical and structural insight into green carbon

2020 ◽  
Vol 22 (33) ◽  
pp. 18435-18446
Author(s):  
Luke J. R. Higgins ◽  
Christoph J. Sahle ◽  
Mahalingam Balasubramanian ◽  
Bhoopesh Mishra

X-ray Raman scattering (XRS) spectroscopy provides access to element-specific core photo-absorption edges of low Z-elements (e.g. K-edges of C, N, O), using hard X-ray photons enabling bulk and in situ study of green carbons.

2018 ◽  
Vol 57 (18) ◽  
pp. 11422-11435 ◽  
Author(s):  
Victor A. Streltsov ◽  
Ruwini S. K. Ekanayake ◽  
Simon C. Drew ◽  
Christopher T. Chantler ◽  
Stephen P. Best

Structure ◽  
2001 ◽  
Vol 9 (5) ◽  
pp. 419-429 ◽  
Author(s):  
Constanze Breithaupt ◽  
Jochen Strassner ◽  
Ulrike Breitinger ◽  
Robert Huber ◽  
Peter Macheroux ◽  
...  

2017 ◽  
Vol 24 (2) ◽  
pp. 521-530 ◽  
Author(s):  
S. Huotari ◽  
Ch. J. Sahle ◽  
Ch. Henriquet ◽  
A. Al-Zein ◽  
K. Martel ◽  
...  

An end-station for X-ray Raman scattering spectroscopy at beamline ID20 of the European Synchrotron Radiation Facility is described. This end-station is dedicated to the study of shallow core electronic excitations using non-resonant inelastic X-ray scattering. The spectrometer has 72 spherically bent analyzer crystals arranged in six modular groups of 12 analyzer crystals each for a combined maximum flexibility and large solid angle of detection. Each of the six analyzer modules houses one pixelated area detector allowing for X-ray Raman scattering based imaging and efficient separation of the desired signal from the sample and spurious scattering from the often used complicated sample environments. This new end-station provides an unprecedented instrument for X-ray Raman scattering, which is a spectroscopic tool of great interest for the study of low-energy X-ray absorption spectra in materials under in situ conditions, such as in operando batteries and fuel cells, in situ catalytic reactions, and extreme pressure and temperature conditions.


2021 ◽  
Vol 32 (29) ◽  
pp. 295701
Author(s):  
Yalan Huang ◽  
He Zhu ◽  
Hekang Zhu ◽  
Jian Zhang ◽  
Yang Ren ◽  
...  

2005 ◽  
Vol 20 (12) ◽  
pp. 3270-3273 ◽  
Author(s):  
F. Berberich ◽  
H. Graafsma ◽  
B. Rousseau ◽  
A. Canizares ◽  
R. Ramy Ratiarison ◽  
...  

A unique combination of in situ synchrotron x-ray diffraction and in situ micro-Raman spectroscopy was used to study the growth process of YBa2Cu3O6+x films obtained by metal organic decomposition using trifluoroacetate precursor on LaAlO3 substrates. The techniques give complementary information: x-ray diffraction gives insight into the structural growth, whereas micro-Raman spectroscopy gives information of the chemical composition with additional information on the texture. To perform both experiments in situ, a special high-temperature process chamber was designed.


2021 ◽  
Author(s):  
Matthias Schwartzkopf ◽  
Sven-Jannik Wöhnert ◽  
Vivian Waclawek ◽  
Niko Carstens ◽  
André Rothkirch ◽  
...  

At the nascence of a metal–polymer hybrid material primarily vertical Au dimers and free adatoms diffuse on and into the polymer matrix revealed in situ by sub-millisecond time-resolved surface-sensitive X-ray scattering (GISAXS).


2012 ◽  
Vol 151 (5) ◽  
pp. 483-492 ◽  
Author(s):  
Yukiko Sakakibara ◽  
Hitoshi Kimura ◽  
Akira Iwamura ◽  
Takashi Saitoh ◽  
Takahisa Ikegami ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document