A facile alkali metal hydroxide-assisted controlled and targeted synthesis of 1T MoS2 single-crystal nanosheets for lithium ion battery anodes

Nanoscale ◽  
2019 ◽  
Vol 11 (31) ◽  
pp. 14857-14862 ◽  
Author(s):  
Zhao Li ◽  
Xun Zhan ◽  
Shuhua Qi

High-quality metallic 1T phase MoS2 single-crystal nanosheets were synthesized by a facile alkali metal hydroxide-assisted approach via the calcination of lithium hydroxide and ammonium tetrathiomolybdate under argon atmosphere at 1000 °C

2020 ◽  
Vol 26 (7) ◽  
pp. 1497-1500
Author(s):  
Evan L. Thomas ◽  
Samantha Stegman ◽  
Suntharalingam Skanthakumar ◽  
Richard E. Wilson

2018 ◽  
Vol 259 ◽  
pp. 48-55 ◽  
Author(s):  
Liansheng Jiao ◽  
Zhenbang Liu ◽  
Zhonghui Sun ◽  
Tongshun Wu ◽  
Yuzhou Gao ◽  
...  

ChemSusChem ◽  
2017 ◽  
Vol 11 (1) ◽  
pp. 299-310 ◽  
Author(s):  
Qiang Guo ◽  
Li Chen ◽  
Zizhao Shan ◽  
Wee Siang Vincent Lee ◽  
Wen Xiao ◽  
...  

1988 ◽  
Vol 31 (1) ◽  
pp. 62-70
Author(s):  
Take-aki MITSUDO ◽  
Yukiatsu KOMIYA ◽  
Hideki BOKU ◽  
Atsushi ISHIHARA ◽  
Satoshi MURACHI ◽  
...  

2018 ◽  
Vol 6 (9) ◽  
pp. 3857-3863 ◽  
Author(s):  
Jun Liu ◽  
Ai Xiang Wei ◽  
Minghua Chen ◽  
Xinhui Xia

High-quality Li4Ti5O12/N-doped carbon (LTO/N-C) nanotube arrays on a conductive substrate are fabricated via a new ALD-assisted method for lithium ion battery applications. The designed LTO/N-C nanotube arrays show very impressive high-rate capacity (153 mA h g−1 at 5C) and stable capacity: 98% retention after 6000 cycles at 40C.


2017 ◽  
Vol 5 (18) ◽  
pp. 8744-8751 ◽  
Author(s):  
Dong Jun Lee ◽  
Seung-Ho Yu ◽  
Hyeon Seok Lee ◽  
Aihua Jin ◽  
Jisoo Lee ◽  
...  

We report a facile approach to synthesize hexagon-shaped nanoplates of various metal (oxy)hydroxides under aqueous solutions while avoiding complex processes.


2019 ◽  
Vol 944 ◽  
pp. 1179-1186 ◽  
Author(s):  
Yue Hua Wang ◽  
Li Wen Ma ◽  
Yun He Zhang ◽  
Zhao Jie Huang ◽  
Xiao Li Xi

With the development of new energy vehicles, urgent issues have attracted considerable attention. Some power batteries have entered the scrapping period, with the imperative recycling of used power batteries. Some studies have predicted that by 2020, the amount of power lithium battery scrap will reach 32.2 GWh, corresponding to ~500,000 tons, and by 2023, the scrap will reach 101 GWh, corresponding to ~1.16 million tons. In this study, nickel-cobalt-lithium LiNi0.7Co0.3O2cathode materials are regenerated from spent lithium-ion battery cathode materials as the raw material, which not only aids in the reduction of pressure on the environment but also leads to the recycling of resources. First, extraction is employed using extracting agent p204 to remove aluminum ions from an acid leaching solution. Extraction conditions for aluminum ions are: include a phase ratio of 1:2,a pH of 3, an extractant concentration of 30%, and a saponification rate of 70%.Next, the precursor was prepared by co-precipitation using sodium hydroxide and ammonia water as the precipitant and complexion agents, respectively; hence, the cathode material can be uniformly mixed at the atomic level. The precursor and lithium hydroxide were subjected to calcination at high temperature using a high-temperature solid-phase method. The Calcination conditions include an air atmosphere ; a calcination temperature of 800° °C ; a calcination time of 15 h, an n (precursor): n (lithium hydroxide) ratio of 1:1.1.The Thermogravimetric analysis revealed that the synthesis temperature should not exceed 850°C. X-ray diffraction analysis, scanning electron microscopy, and energy spectrum analysis of the cathode material revealed a composition comprising Li, Ni, and Co oxides. After analysis, the material obtained is lithium nickel-cobalt-oxide, LiNi0.7Co0.3O2, which is a positive electrode material with good crystallinity and a regular layered structure.


Sign in / Sign up

Export Citation Format

Share Document