Synthesis and characterization of metallapentalenoxazetes by the [2+2] cycloaddition of metallapentalynes with nitrosoarenes

Zhihong Deng; Congqing Zhu; Yuhui Hua; Guomei He; Ying Guo; Ruqiang Lu; Xiaoyu Cao; Jiangxi Chen; Haiping Xia

doi:10.1039/c9cc02594d

Synthesis and characterization of metallapentalenoxazetes by the [2+2] cycloaddition of metallapentalynes with nitrosoarenes

Chemical Communications ◽

10.1039/c9cc02594d ◽

2019 ◽

Vol 55 (44) ◽

pp. 6237-6240 ◽

Cited By ~ 4

Author(s):

Zhihong Deng ◽

Congqing Zhu ◽

Yuhui Hua ◽

Guomei He ◽

Ying Guo ◽

...

Keyword(s):

Synthesis And Characterization ◽

Metal Fragment

The cycloaddition of metallapentalynes with nitrosoarenes produces metallapentalenoxazetes, in which two unstable frameworks are stabilized with a metal fragment.

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Synthesis and Characterization of Conductng Orented Fibres of Poly-Para-Phenylene

Molecular Crystals and Liquid Crystals ◽

10.1080/00268948408071657 ◽

1984 ◽

Vol 105 (1) ◽

pp. 259-271 ◽

Cited By ~ 8

Author(s):

M. Staeim

Keyword(s):

Synthesis And Characterization

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Synthesis and Characterization of the Three Dicyclopentapyrenes

The Journal of Organic Chemistry ◽

10.1021/jo964001e ◽

1996 ◽

Vol 61 (10) ◽

pp. 3572-3572

Author(s):

Lawrence T. Scott ◽

Atena Necula

Keyword(s):

Synthesis And Characterization

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Heterobimetallic single-source precursors for MOCVD. Synthesis and characterization of volatile mixed ligand complexes of lanthanides, barium and magnesium β-diketonates with d-element containing ligands

Journal de Physique IV (Proceedings) ◽

10.1051/jp4:19998119 ◽

1999 ◽

Vol 09 (PR8) ◽

pp. Pr8-943-Pr8-951 ◽

Cited By ~ 8

Author(s):

A. N. Gleizes ◽

F. Senocq ◽

M. Julve ◽

J. L. Sanz ◽

N. Kuzmina ◽

...

Keyword(s):

Mixed Ligand ◽

Mixed Ligand Complexes ◽

Synthesis And Characterization ◽

Single Source ◽

Single Source Precursors

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Synthesis and characterization of β-glucogallin as an aldose reductase inhibitor from Emblica officinalis

Planta Medica ◽

10.1055/s-0032-1320987 ◽

2012 ◽

Vol 78 (11) ◽

Author(s):

J Ponder ◽

JM Petrash ◽

DV LaBarbera

Keyword(s):

Aldose Reductase ◽

Reductase Inhibitor ◽

Aldose Reductase Inhibitor ◽

Synthesis And Characterization ◽

Emblica Officinalis

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Synthesis and characterization of TiN / Ti / AISI 410 coatings

Journal of Sciences and Engineering ◽

10.32829/sej.v2i1.54 ◽

2018 ◽

Vol 2 (1) ◽

pp. 7

Author(s):

S Chirino ◽

Jaime Diaz ◽

N Monteblanco ◽

E Valderrama

Keyword(s):

Synthesis And Characterization ◽

Photoemission Spectroscopy ◽

X Ray Diffraction ◽

X Ray ◽

Columnar Grains ◽

Tin Thin Films ◽

Steel Aisi ◽

Interacting Surfaces ◽

Stainless Steel Aisi

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified. Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.

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