Fabrication of a bismuth nanoparticle/Nafion modified screen-printed graphene electrode for in situ environmental monitoring

2019 ◽  
Vol 11 (12) ◽  
pp. 1591-1603 ◽  
Author(s):  
Shirley Palisoc ◽  
Vince Aaron Sow ◽  
Michelle Natividad

Bismuth nanoparticle (BiNP)/Nafion modified screen-printed electrodes were fabricated through screen printing and drop coating.

2015 ◽  
Vol 183 (2) ◽  
pp. 503-517 ◽  
Author(s):  
John Barton ◽  
María Begoña González García ◽  
David Hernández Santos ◽  
Pablo Fanjul-Bolado ◽  
Alberto Ribotti ◽  
...  

2010 ◽  
Vol 2 (6) ◽  
pp. 645 ◽  
Author(s):  
Mohamed Khairy ◽  
Rashid O. Kadara ◽  
Dimitrios K. Kampouris ◽  
Craig E. Banks

2020 ◽  
Vol 9 (2) ◽  
pp. 293-300
Author(s):  
Nils Donker ◽  
Anastasiya Ruchets ◽  
Daniela Schönauer-Kamin ◽  
Jens Zosel ◽  
Ulrich Guth ◽  
...  

Abstract. Symmetrical Pt|YSZ|Pt sensors were produced by screen printing with frit-containing and fritless Pt pastes and fired at 950, 1100, and 1300 ∘C. Subsequently, the sensors were operated by pulsed polarization, and the NO sensitivity was investigated. The sensitivity of the sensors with fritless pastes was found to be significantly higher. The influence of the firing temperature was low in contrast to the influence of the paste. The low NO sensitivity of the frit-containing electrodes was attributed to a blocking effect that probably occurs at the triple-phase boundaries. Therefore, the oxygen transport through the sensor is inhibited, which, however, seems to be necessary for the sensor effect.


2021 ◽  
Vol 76 (2) ◽  
pp. 243-251
Author(s):  
Mohamed K. Abd El-Rahman ◽  
Rania A. Sayed ◽  
Manal S. El-Masry ◽  
Wafaa S. Hassan ◽  
Abdalla Shalaby

Sensors ◽  
2020 ◽  
Vol 20 (13) ◽  
pp. 3702
Author(s):  
Daniel Antuña-Jiménez ◽  
David Ibáñez ◽  
María Begoña González-García ◽  
David Hernández-Santos ◽  
Pablo Fanjul-Bolado

Metal phthalocyanines are well-known sensing phases with applications in different scientific fields due to their interesting properties. Detailed characterization by Raman spectroscopy was performed in order to study the shifting of the vibrational bands related to the coordination sphere of each metal phthalocyanine. In this work, a study involving the use of screen-printed electrodes (SPEs) with various metal phthalocyanines to electrochemically detect and quantify chlorine (Cl2) gas is presented. The Cl2 gas was generated in-situ via oxidation of the chloride present in form of aqueous salt solutions. The developed method offers not only the possibility to quantify chlorine, but also to discriminate among several chlorinated species due to the changes observed in the voltammetric profiles associated with the interaction between the specie assayed and the phthalocyanine metallic center. Optimization of detecting parameters was also performed to apply this procedure for the quantification of chlorine generated from commercial chlorine tablets. The development of this proof of concept shows interesting possibilities and easy-to-use applications with novel on metal phthalocyanines based SPE sensors.


2021 ◽  
Vol 10 (1) ◽  
pp. 129-138
Author(s):  
Mylena Lorenz ◽  
Nahum Travitzky ◽  
Carlos R. Rambo

AbstractThis work reports on the development of pastes containing Ti, TiC, Si, and C elementary powders for in situ synthesis of Ti3SiC2 via screen printing. Four paste compositions were manufactured using two powder mixtures (Ti/Si/C and Ti/TiC/Si/C) with different stoichiometry. The pastes were screen printed onto Al2O3 substrates and sintered at 1400 ℃ in argon varying the dwell time from 1 to 5 h. The printed pastes containing TiC and excess of Si exhibited the lowest surface roughness and after 5 h sintering comprised of Ti3SiC2 as the majority phase. The electrical conductivity of this sample was found to range from 4.63×104 to 2.57×105 S·m–1 in a temperature range of 25–400 ℃.


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