One-step rapid synthesis of Ni6(C12H25S)12 nanoclusters for electrochemical sensing of ascorbic acid

The Analyst ◽  
2020 ◽  
Vol 145 (7) ◽  
pp. 2621-2630
Author(s):  
Zhihua Zhuang ◽  
Wei Chen

Ni6(C12H25S)12 clusters and their single crystals are synthesized successfully and the Ni6 clusters show high electrochemical sensing performance for the detection of ascorbic acid.

2018 ◽  
Vol 27 (1) ◽  
pp. 58-64 ◽  
Author(s):  
Lizhai Pei ◽  
Fanglv Qiu ◽  
Yue Ma ◽  
Feifei Lin ◽  
Chuangang Fan ◽  
...  

Polymers ◽  
2019 ◽  
Vol 11 (8) ◽  
pp. 1346 ◽  
Author(s):  
Salma Bilal ◽  
Ayesha Akbar ◽  
Anwar-ul-Haq Ali Shah

The surface of an Au-disc electrode was modified through electro polymerization of aniline, in the presence of dodecyl benzene sulphonic acid (DBSA) and sulphuric acid (H2SO4) solution. The polymerization conditions were pre-optimized so that micelle formation and solution coagulation could be minimized and surfactant doped polyaniline film could be obtained through a quick, simple and one step polymerization route. The synthesized material was characterized via Fourier transform infrared (FTIR) spectroscopy, thermogravimetric analysis (TGA), scanning electron microscopy (SEM) and cyclic voltammetry (CV). The effective surface area of the Au-disc, calculated through cyclic voltammetry, was immensely increased through a polyaniline (PANI) coating (0.04 and 0.11 cm2 for bare and PANI coated gold respectively). The modified electrode was utilized for ascorbic acid (AA) sensing. The changing pH of electrolyte and scan rate influenced the PANI electrode response towards AA. The modified electrode was highly selective towards AA oxidation and showed a very low limit of detection i.e. 0.0267 μmol·L–1. Moreover, the PANI coating greatly reduced the sensing potential for AA by a value of around 140 mV when compared to that on a bare gold electrode.


Author(s):  
Irene Taurino ◽  
Gabriella Sanzo ◽  
Sandro Carrara ◽  
Giovanni De Micheli ◽  
Gabriele Favero ◽  
...  

2015 ◽  
Vol 7 (2) ◽  
pp. 779-786 ◽  
Author(s):  
S. Ramakrishnan ◽  
K. R. Pradeep ◽  
A. Raghul ◽  
R. Senthilkumar ◽  
Murali Rangarajan ◽  
...  

Platinum nanoparticle-decorated graphene and carbon nanotube (Pt-Gr-CNT) nanocomposites synthesized by a single step chemical vapor deposition process, serve as a promising platform for the simultaneous electrochemical sensing of dopamine, uric acid and ascorbic acid.


2021 ◽  
Vol 9 (13) ◽  
pp. 8308-8316
Author(s):  
Facai Wei ◽  
Yonghui Zhong ◽  
Hao Luo ◽  
Yong Wu ◽  
Jianwei Fu ◽  
...  

We propose a facile soft template-mediated coupling construction strategy for one-step fabrication of sandwiched mesoporous PPy/Ag nanoplates at the liquid interface, and the hybrid showed great chemical sensing performance for NH3 gas.


2021 ◽  
Author(s):  
Ngo Xuan Dinh ◽  
Tuyet Nhung Pham ◽  
Tran Quang Huy ◽  
Do Quang Trung ◽  
Pham Anh Tuan ◽  
...  

This work contributes to a deeper understanding of the effects of functional 2D nanomaterials on the electrochemical sensing performance of SPE-based portable sensors for the rapid, accurate, and on-site determination of CAP in food samples.


CrystEngComm ◽  
2016 ◽  
Vol 18 (27) ◽  
pp. 5202-5208 ◽  
Author(s):  
Lianjie Zhu ◽  
Yanxing Zhao ◽  
Wenjun Zheng ◽  
Ningning Ba ◽  
Guangzhi Zhang ◽  
...  

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