scholarly journals Characterization of three-point bending properties of metal–resin interpenetrating phase composites

RSC Advances ◽  
2018 ◽  
Vol 8 (29) ◽  
pp. 16171-16177 ◽  
Author(s):  
Bibo Yao ◽  
Zhaoyao Zhou ◽  
Liuyang Duan ◽  
Zengtao Chen

Three-point bending properties of the metal–resin IPCs exhibit anisotropy. Flexural strength increases with increasing fiber fractions and finer fibers improve the properties. The fracture shows both brittle and plastic characteristics.

2021 ◽  
Vol 8 ◽  
Author(s):  
Bencang Cui ◽  
Fengbo Sun ◽  
Qian Ding ◽  
Huining Wang ◽  
Yuanhua Lin ◽  
...  

Although efforts have been put into the research in polymer-infiltrated ceramic network composites (PICNs), data are needed to understand the relationship between surface roughness and flexural strength. In this work, a novel dental restorative composite was fabricated via infiltrating mixtures of Bis-GMA/TEGDMA and UDMA/TEGDMA into partially sintered porous sodium aluminum silicate blocks and curing. Bars with different surface conditions were produced by sanding with abrasive and polishing. Flexural strength was measured using three-point-bending. Scanning electron microscopy (SEM) was employed to observe the microstructure of surface areas. One-way analysis of variance was applied for statistical calculations, with p < 0.05 being considered significant. Weibull plots were used to evaluate the reliability of flexural strength. The results demonstrated that the flexural strength of the resultant composites was affected by the scratch direction and the value of roughness. The flexural strength increased with decrease of surface roughness. A higher strength value was found for parallel types than for vertical types with nearly the same surface roughness. A large roughness value and a scratch direction perpendicular to tensile stress produced a low Weibull modulus. Of particular importance with this work is that these factors should be taken into consideration when using PICNs as dental restorative composites.


Materials ◽  
2021 ◽  
Vol 14 (7) ◽  
pp. 1626
Author(s):  
Pravin Jagdale ◽  
Gianpaolo Serino ◽  
Goldie Oza ◽  
Alberto Luigi Audenino ◽  
Cristina Bignardi ◽  
...  

Employment and the effect of eco-friendly bismuth oxide nanoparticles (BiONPs) in bio-cement were studied. The standard method was adopted to prepare BiONPs-composite. Water was adopted for dispersing BiONPs in the composite. A representative batch (2 wt. % of BiONPs) was prepared without water to study the impact of water on composite properties. For each batch, 10 samples were prepared and tested. TGA (thermogravimetric analysis) performed on composite showed 0.8 wt. % losses in samples prepared without water whereas, maximum 2 wt. % weight losses observed in the water-based composite. Presence of BiONPs resulted in a decrease in depth of curing. Three-point bending flexural strength decreased for increasing BiONPs content. Comparative study between 2 wt. % samples with and without water showed 10.40 (±0.91) MPa and 28.45 (±2.50) MPa flexural strength values, respectively, indicating a significant (p < 0.05) increase of the mechanical properties at the macroscale. Nanoindentation revealed that 2 wt. % without water composites showed significant (p < 0.05) highest nanoindentation modulus 26.4 (±1.28) GPa and hardness 0.46 (±0.013) GPa. Usage of water as dispersion media was found to be deleterious for the overall characteristics of the composite but, at the same time, the BiONPs acted as a very promising filler that can be used in this class of composites.


2019 ◽  
pp. 089270571987822
Author(s):  
Saud Aldajah ◽  
Mohammad Y Al-Haik ◽  
Waseem Siddique ◽  
Mohammad M Kabir ◽  
Yousef Haik

This study reveals the enhancement of mechanical and thermal properties of maleic anhydride-grafted polypropylene (PP- g-MA) with the addition of nanocrystalline cellulose (NCC). A nanocomposite was manufactured by blending various percentages of PP, MA, and NCC nanoparticles by means of a twin-screw extruder. The influence of varying the percentages of NCC on the mechanical and thermal behavior of the nanocomposite was studied by performing three-point bending, nanoindentation, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), scanning electron microscopy (SEM), and Fourier-transform infrared (FTIR) spectroscopy tests. The novelty of this study stems on the NCC nanoparticles and their ability to enhance the mechanical and thermal properties of PP. Three-point bending and nanoindentation tests revealed improvement in the mechanical properties in terms of strength, modulus, and hardness of the PP- g-MA nanocomposites as the addition of NCC increased. SEM showed homogeneity between the mixtures which proved the presence of interfacial adhesion between the PP- g-MA incorporated with NCC nanoparticles that was confirmed by the FTIR results. DSC and TGA measurements showed that the thermal stability of the nanocomposites was not compromised due to the addition of the coupling agent and reinforced nanoparticles.


Polymers ◽  
2021 ◽  
Vol 13 (13) ◽  
pp. 2139
Author(s):  
Wei Shian Tey ◽  
Chao Cai ◽  
Kun Zhou

Multi Jet Fusion (MJF) is a recently developed polymeric powder bed fusion (PBF) additive manufacturing technique that has received considerable attention in the industrial and scientific community due to its ability to fabricate functional and complex polymeric parts efficiently. In this work, a systematic characterization of the physicochemical properties of MJF-certified polyamide 11 (PA11) and thermoplastic polyurethane (TPU) powder was conducted. The mechanical performance and print quality of the specimens printed using both powders were then evaluated. Both PA11 and TPU powders showed irregular morphology with sharp features and had broad particle size distribution, but such features did not impair their printability significantly. According to the DSC scans, the PA11 specimen exhibited two endothermic peaks, while the TPU specimen exhibited a broad endothermic peak (116–150 °C). The PA11 specimens possessed the highest tensile strength in the Z orientation, as opposed to the TPU specimens which possessed the lowest tensile strength along the same orientation. The flexural properties of the PA11 and TPU specimens displayed a similar anisotropy where the flexural strength was highest in the Z orientation and lowest in the X orientation. The porosity values of both the PA11 and the TPU specimens were observed to be the lowest in the Z orientation and highest in the X orientation, which was the opposite of the trend observed for the flexural strength of the specimens. The PA11 specimen possessed a low coefficient of friction (COF) of 0.13 and wear rate of 8.68 × 10−5 mm3/Nm as compared to the TPU specimen, which had a COF of 0.55 and wear rate of 0.012 mm3/Nm. The PA11 specimens generally had lower roughness values on their surfaces (Ra < 25 μm), while the TPU specimens had much rougher surfaces (Ra > 40 μm). This investigation aims to uncover and explain phenomena that are unique to the MJF process of PA11 and TPU while also serving as a benchmark against similar polymeric parts printed using other PBF processes.


Author(s):  
Yi Sun ◽  
Yuan Tian ◽  
Dongming Zheng ◽  
Gui Liu ◽  
Xingxing Pan ◽  
...  

2014 ◽  
Vol 56 ◽  
pp. 522-527 ◽  
Author(s):  
Wei Zhou ◽  
Qinghui Wang ◽  
Weisong Ling ◽  
Liangzong He ◽  
Yong Tang ◽  
...  

2007 ◽  
Vol 539-543 ◽  
pp. 1863-1867 ◽  
Author(s):  
X.F. Tao ◽  
Li Ping Zhang ◽  
Y.Y. Zhao

This paper investigated the mechanical response of porous copper manufactured by LCS under three-point bending and Charpy impact conditions. The effects of the compaction pressure and K2CO3 particle size used in producing the porous copper samples and the relative density of the samples were studied. The apparent modulus, flexural strength and energy absorption capacity in three-point bending tests increased exponentially with increasing relative density. The impact strength was not markedly sensitive to relative density and had values within 7 – 9 kJ/m2 for the relative densities in the range 0.17 – 0.31. The amount of energy absorbed by a porous copper sample in the impact test was much higher than that absorbed in the three-point bending test, impling that loading strain rate had a significant effect on the deformation mechanisms. Increasing compaction pressure and increasing K2CO3 particle size resulted in significant increases in the flexural strength and the bending energy absorption capacity, both owing to the reduced sintering defects.


2006 ◽  
Vol 321-323 ◽  
pp. 913-916
Author(s):  
Sang Ll Lee ◽  
Yun Seok Shin ◽  
Jin Kyung Lee ◽  
Jong Baek Lee ◽  
Jun Young Park

The microstructure and the mechanical property of liquid phase sintered (LPS) SiC materials with oxide secondary phases have been investigated. The strength variation of LPS-SiC materials exposed at the elevated temperatures has been also examined. LPS-SiC materials were sintered at the different temperatures using two types of Al2O3/Y2O3 compositional ratio. The characterization of LPS-SiC materials was investigated by means of SEM with EDS, three point bending test and indentation test. The LPS-SiC material with a density of about 3.2 Mg/m3 represented a flexural strength of about 800 MPa and a fracture toughness of about 9.0 MPa⋅√m.


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