scholarly journals Gas phase dehydration of glycerol to acrolein over WO3-based catalysts prepared by non-hydrolytic sol–gel synthesis

RSC Advances ◽  
2018 ◽  
Vol 8 (24) ◽  
pp. 13344-13352 ◽  
Author(s):  
L. Nadji ◽  
A. Massó ◽  
D. Delgado ◽  
R. Issaadi ◽  
E. Rodriguez-Aguado ◽  
...  

Active and selective W–Si–(Zr)–O catalysts for glycerol dehydration to acrolein have been successfully prepared by non-hydrolytic sol gel method.

2013 ◽  
Vol 2013 ◽  
pp. 1-6 ◽  
Author(s):  
Ekaterina V. Borisova ◽  
Alexey V. Ignatov ◽  
Eugeni I. Get'man ◽  
Stanislav N. Loboda ◽  
Lyudmyla I. Ardanova ◽  
...  

Sodium europium silicate, NaEu9(SiO4)6O2, with apatite structure has been obtained and studied using X-ray diffraction and SEM. It has been shown that sodium sublimation does not take place upon synthesis by the sol-gel method. Rietveld refinement has revealed that sodium atoms are ordered and occupy the 4f position. O(4) atoms not related to silicate ions are placed at the centers of Eu(2) triangles. DC and AC electric conductivity and activation energy have been determined for the compound studied.


CrystEngComm ◽  
2016 ◽  
Vol 18 (3) ◽  
pp. 407-416 ◽  
Author(s):  
K. McBride ◽  
J. Cook ◽  
S. Gray ◽  
S. Felton ◽  
L. Stella ◽  
...  

A range of lanthanum strontium manganates (La1−xSrxMnO3) where 0 ≤ x ≤ 0.4 were prepared using a modified peroxide sol–gel synthesis. The crystal structure of these materials was investigated and their potential as mediators for magnetic fluid hyperthermia was evaluated.


2011 ◽  
Vol 12 (14) ◽  
pp. 1291-1294 ◽  
Author(s):  
Yue Liu ◽  
Yuejun Wang ◽  
Haiqiang Wang ◽  
Zhongbiao Wu

RSC Advances ◽  
2015 ◽  
Vol 5 (22) ◽  
pp. 17054-17059 ◽  
Author(s):  
Hany El-Shinawi ◽  
Colin Greaves ◽  
Jürgen Janek

A room-temperature stable α-LiZr2(PO4)3 phase is prepared by a modified sol–gel method, and shows bulk conductivity as high as 1.58 × 10−4 Scm−1.


2020 ◽  
Vol 44 (5) ◽  
pp. 1888-1904 ◽  
Author(s):  
T. N. Ravishankar ◽  
M. de O. Vaz ◽  
S. R. Teixeira

Effective and low-cost CuO/TiO2 nanocomposites were prepared at room temperature by a surfactant-assisted sol–gel method for photocatalytic activities under UV-visible and visible light irradiations.


2003 ◽  
Vol 2003 (7) ◽  
pp. 423-425 ◽  
Author(s):  
Suzuko Yamazaki ◽  
Tomoko Hayashi

The effects of alkoxides, solvents, and the peptization and dialysis procedures in the sol-gel synthesis of TiO2 on the degradation rates of ethylene were investigated.


2009 ◽  
Vol 148 (1-2) ◽  
pp. 115-118 ◽  
Author(s):  
J. Hernández-Fernández ◽  
A. Aguilar-Elguezabal ◽  
S. Castillo ◽  
B. Ceron-Ceron ◽  
R.D. Arizabalo ◽  
...  

2011 ◽  
Vol 25 (21) ◽  
pp. 2823-2839 ◽  
Author(s):  
Y. VAHIDSHAD ◽  
H. ABDIZADEH ◽  
H. R. BAHARVANDI ◽  
M. AKBARI BASERI

A sol-gel method is investigated to synthesize CuO – ZrO 2 nanoparticles as catalyst for hydrogen production from methanol. Finer precursor nanoparticles give rise to larger specific areas in catalyst which result in a high hydrogen production. The effects of some critical process parameters on the sol-gel synthesis of CuO – ZrO 2 nanoparticles are studied. These parameters are affected on synthesis of CuO – ZrO 2 when it is prepared with sol-gel method. Particle size and distribution are considered as the results. The parameters including the effect of calcination temperature, aging temperature, nature and concentration of catalyst (acidic or basic conditions), H 2 O /precursor molar ratio, and chelating agent that have been identified as most important, are focused. It is found that the calcination temperature strongly influenced the morphology and interaction between the active species and support, and hence the structure and catalytic performance. Nature and concentration of catalyst ( pH value), chelating agent, ( H 2 O /precursor) molar ratio and also aging temperature have influence on the nanoparticles. Thus, by controlling these factors, it is possible to vary the morphology and properties of the sol-gel-derived inorganic network over wide ranges. Morphology, particle size and distribution, phase evaluation, structure, and chemical analysis of the products are investigated by SEM, TEM, DTA/TG, XRD and EDX respectively.


1998 ◽  
Vol 13 (11) ◽  
pp. 3022-3026
Author(s):  
Y. Masuda ◽  
J-S. Jin ◽  
K. Nakanishi ◽  
K. Tanabe

(Ba1−xLax)3Cu3(O, F)y films were prepared using a sol-gel method. Phases, the c lattice parameters of which are about 13.8, 13.1, and 11.6 Å, respectively, were formed in the films. The compound with the c parameter of ˜13.8 Å is considered to be a Ba2−xLaxCuO2F2+δ which has the La2CuO4-type structure inserted with fluorine. The compound with the c parameter of ˜11.6 Å is thought to have a three-layered structure of the perovskite block which is arisen by ordering between La and Ba elements. The films containing these compounds showed some interesting anomalies in SQUID measurements. However, no film showed a drastic decrease of electrical resistance.


Author(s):  
Hong Wang ◽  
Ling Du ◽  
Lili Yang ◽  
Wenjie Zhang ◽  
Hongbo He

AbstractA sol-gel method was used to synthesis La


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