Efficient synthesis of esters through oxone-catalyzed dehydrogenation of carboxylic acids and alcohols

Fei Hou; Xi-Cun Wang; Zheng-Jun Quan

doi:10.1039/c8ob02539h

Efficient synthesis of esters through oxone-catalyzed dehydrogenation of carboxylic acids and alcohols

Organic & Biomolecular Chemistry ◽

10.1039/c8ob02539h ◽

2018 ◽

Vol 16 (48) ◽

pp. 9472-9476 ◽

Cited By ~ 4

Author(s):

Fei Hou ◽

Xi-Cun Wang ◽

Zheng-Jun Quan

Keyword(s):

Carboxylic Acids ◽

Environmentally Friendly ◽

Attractive Alternative ◽

Efficient Synthesis

An environmentally friendly oxone (20 mol%) catalyzed esterification of carboxylic acids with alcohols has been developed, providing an attractive alternative to the construction of valuable carbonyl esters.

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ChemInform Abstract: Condensation Between Isocyanates and Carboxylic Acids in the Presence of 4-Dimethylaminopyridine (DMAP): A Mild and Efficient Synthesis of Amides.

ChemInform ◽

10.1002/chin.200124086 ◽

2010 ◽

Vol 32 (24) ◽

pp. no-no

Author(s):

Anne C. Schuemacher ◽

R. W. Hoffmann

Keyword(s):

Carboxylic Acids ◽

Efficient Synthesis

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ChemInform Abstract: Pd(0)/Ag+-Cocatalyzed Cyclization Reaction of 1,2-Allenic Carboxylic Acids with Aryl/Alkenyl Halides. An Efficient Synthesis of Butenolides.

ChemInform ◽

10.1002/chin.199906099 ◽

2010 ◽

Vol 30 (6) ◽

pp. no-no

Author(s):

S. MA ◽

Z. SHI

Keyword(s):

Carboxylic Acids ◽

Cyclization Reaction ◽

Efficient Synthesis

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ChemInform Abstract: An Efficient Synthesis of N-Methoxy-N-methylamides from Carboxylic Acids Using N-Methoxy-N-methylcarbamoyl Chloride.

ChemInform ◽

10.1002/chin.200236060 ◽

2010 ◽

Vol 33 (36) ◽

pp. no-no

Author(s):

Jae In Lee ◽

Hyun Park

Keyword(s):

Carboxylic Acids ◽

Efficient Synthesis

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Efficient synthesis of glycosylamines in solventless conditions promoted by mechanical milling

RSC Advances ◽

10.1039/c4ra04321a ◽

2014 ◽

Vol 4 (68) ◽

pp. 36350-36356 ◽

Cited By ~ 7

Author(s):

Cédric Epoune Lingome ◽

Gwladys Pourceau ◽

Virginie Gobert-Deveaux ◽

Anne Wadouachi

Keyword(s):

Mechanical Milling ◽

Environmentally Friendly ◽

Efficient Synthesis ◽

Environmentally Friendly Approach

A mecanosynthesis of glycosylamines under solventless conditions was established. This environmentally friendly approach optimized with l-rhamnose, was investigated using a variety of amines and other carbohydrates.

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ChemInform Abstract: Facile and Efficient Synthesis of Quinoline-4-carboxylic Acids under Microwave Irradiation.

ChemInform ◽

10.1002/chin.201020116 ◽

2010 ◽

Vol 41 (20) ◽

Author(s):

Hui Zhu ◽

Ri Fang Yang ◽

Liu Hong Yun ◽

Jin Li

Keyword(s):

Microwave Irradiation ◽

Carboxylic Acids ◽

Efficient Synthesis

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ChemInform Abstract: An Efficient Synthesis of α,β-Unsaturated Carboxylic Acids and Nitriles.

ChemInform ◽

10.1002/chin.199036109 ◽

1990 ◽

Vol 21 (36) ◽

Author(s):

C. K. LEE ◽

J. Y. SHIM

Keyword(s):

Carboxylic Acids ◽

Efficient Synthesis ◽

Unsaturated Carboxylic Acids

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Environmentally friendly efficient synthesis and mechanism of triazenes derived from cyclic amines on clays, HZSM-5 and sulfated zirconia

Applied Catalysis B Environmental ◽

10.1016/j.apcatb.2007.05.002 ◽

2007 ◽

Vol 76 (1-2) ◽

pp. 24-33 ◽

Cited By ~ 8

Author(s):

H.A. Dabbagh ◽

A. Teimouri ◽

A. Najafi Chermahini

Keyword(s):

Sulfated Zirconia ◽

Environmentally Friendly ◽

Efficient Synthesis ◽

Cyclic Amines

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Cover Picture: Copper(II)/Silver(I)-Catalyzed Sequential Alkynylation and Annulation of Aliphatic Amides with Alkynyl Carboxylic Acids: Efficient Synthesis of Pyrrolidones (Adv. Synth. Catal. 5/2016)

Advanced Synthesis & Catalysis ◽

10.1002/adsc.201600126 ◽

2016 ◽

Vol 358 (5) ◽

pp. 674-674

Author(s):

Jitan Zhang ◽

Danyang Li ◽

Hui Chen ◽

Binjie Wang ◽

Zhanxiang Liu ◽

...

Keyword(s):

Carboxylic Acids ◽

Efficient Synthesis

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DBU-mediated Ireland–Claisen rearrangement of allyl alk-3-enoates: an efficient synthesis of 2-ethylidene-γ,δ-unsaturated carboxylic acids

Tetrahedron ◽

10.1016/j.tet.2007.07.031 ◽

2007 ◽

Vol 63 (39) ◽

pp. 9605-9613 ◽

Cited By ~ 3

Author(s):

Yunxia Li ◽

Andreas Goeke ◽

Ruiyao Wang ◽

Quanrui Wang ◽

Georg Fráter

Keyword(s):

Carboxylic Acids ◽

Claisen Rearrangement ◽

Efficient Synthesis ◽

Unsaturated Carboxylic Acids

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Efficient synthesis of pyrido[2,3-d]pyrimidine-7-carboxylic acids catalyzed by a TiO2/SiO2 nanocomposite in aqueous media at room temperature

Zeitschrift für Naturforschung B ◽

10.1515/znb-2018-0076 ◽

2018 ◽

Vol 73 (9) ◽

pp. 641-645 ◽

Cited By ~ 1

Author(s):

Sepehr Sadegh-Samiei ◽

Shahrzad Abdolmohammadi

Keyword(s):

Heterogeneous Catalyst ◽

Carboxylic Acids ◽

Room Temperature ◽

Aqueous Media ◽

Reaction Times ◽

Molar Ratio ◽

Efficient Synthesis ◽

Reaction Conditions ◽

Moderate Reaction ◽

Recyclable Heterogeneous Catalyst

AbstractA novel and efficient synthesis of eight 5-aryl-1,3-dimethyl-2,4-dioxo-1,2,3,4,5,8-hexahydropyrido[2,3-d]pyrimidine-7-carboxylic acids using a TiO2/SiO2 nanocomposite with a molar ratio of 1:1 as a recyclable heterogeneous catalyst is described. The desired products, five of which are new, are formed in short reaction times (2–3 h) with high to excellent yields (94%–98%) under very moderate reaction conditions (room temperature, aqueous media).

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