A general and rapid room-temperature synthesis approach for metal sulphide nanocrystals with tunable properties

Nanoscale ◽  
2019 ◽  
Vol 11 (1) ◽  
pp. 136-144 ◽  
Author(s):  
Yang Liu ◽  
Maixian Liu ◽  
Deqiang Yin ◽  
Dewei Zhu ◽  
Mark T. Swihart
Keyword(s):  
Room Temperature ◽  
Solution Phase ◽  
High Quality ◽  
Temperature Synthesis ◽  
Phase Synthesis ◽  
Metal Sulphide ◽  
Room Temperature Synthesis ◽  
Tunable Properties ◽  
Solution Phase Synthesis ◽  
Synthesis Approach

A rapid, room-temperature, and solution-phase synthesis produces high-quality, monodisperse metal sulphide nanocrystals with tunable properties.

Solution-phase synthesis of monodispersed SnTe nanocrystallites at room temperature

2003 ◽  
Vol 6 (2) ◽  
pp. 181-184 ◽  
Author(s):  
Changhua An ◽  
Kaibin Tang ◽  
Bin Hai ◽  
Guozhen Shen ◽  
Chunrui Wang ◽  
...  
Keyword(s):  
Room Temperature ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Solution Phase Synthesis

Facile room-temperature solution-phase synthesis of a spherical covalent organic framework for high-resolution chromatographic separation

2015 ◽  
Vol 51 (61) ◽  
pp. 12254-12257 ◽  
Author(s):  
Cheng-Xiong Yang ◽  
Chang Liu ◽  
Yi-Meng Cao ◽  
Xiu-Ping Yan
Keyword(s):  
High Resolution ◽  
Surface Area ◽  
Chromatographic Separation ◽  
Room Temperature ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Covalent Organic Framework ◽  
Solution Phase Synthesis ◽  
Temperature Solution ◽  
Organic Framework

Facile room-temperature solution-phase synthesis of a spherical covalent organic framework with large surface area and good stability for high-resolution chromatographic separation.

scholarly journals Room-Temperature Synthesis of CuInQ2 (Q = S or Se) in Non-Aqueous Solution Using an Organoindium Reagent

1993 ◽  
Vol 327 ◽  
Author(s):  
Aloysius F. Hepp ◽  
Maria T. Andras ◽  
Christopher C. Landry ◽  
Andrew R. Barron
Keyword(s):  
Aqueous Solution ◽  
Particle Size ◽  
Room Temperature ◽  
Analogous Reaction ◽  
Temperature Synthesis ◽  
Two Phase ◽  
Phase Synthesis ◽  
Room Temperature Synthesis

AbstractWe have discovered a novel two-phase synthesis of CuInSe2 at 25° from Cu2Se and (C5H5)3In in 4-methylpyridine (4-MePy). An analogous reaction to produce CulnS2 must be run at 140°C in refluxing 4-MePy in the presence of 2-mercaptopyridine. Microscopy of CuInSe2 produced at 25°C shows it to be platelet-shaped crystallites with an approximate particle size of 10 microns, less than 2% C and H, with a small amount of unidentified crystalline impurity. Our results demonstrate that it is possible to produce from solution a material that is ordinarily synthesized in bulk or films at much higher temperatures or using extraneous reagents and/or electrons.

A facile solution-phase synthesis of high quality water-soluble anatase TiO2 nanocrystals

2007 ◽  
Vol 314 (1) ◽  
pp. 337-340 ◽  
Author(s):  
Ping Wang ◽  
Dejun Wang ◽  
Haiyan Li ◽  
Tengfeng Xie ◽  
Hongzhe Wang ◽  
...  
Keyword(s):  
Anatase Tio2 ◽  
Water Soluble ◽  
Solution Phase ◽  
Tio2 Nanocrystals ◽  
High Quality ◽  
Phase Synthesis ◽  
Solution Phase Synthesis ◽  
Quality Water

Template-free room temperature solution phase synthesis of Cu2O hollow spheres

CrystEngComm ◽  
2010 ◽  
Vol 12 (3) ◽  
pp. 700-701 ◽  
Author(s):  
Wenzhong Wang ◽  
Pengcheng Zhang ◽  
Lei Peng ◽  
Wenjuan Xie ◽  
Guling Zhang ◽  
...  
Keyword(s):  
Room Temperature ◽  
Hollow Spheres ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Solution Phase Synthesis ◽  
Temperature Solution ◽  
Template Free

scholarly journals Towards the room-temperature synthesis of covalent organic frameworks: a mini-review

2020 ◽  
Vol 56 (2) ◽  
pp. 1116-1132
Author(s):  
Ahmad Reza Bagheri ◽  
Nahal Aramesh
Keyword(s):  
Room Temperature ◽  
High Surface ◽  
Physical Stability ◽  
High Surface Area ◽  
Covalent Organic Frameworks ◽  
Temperature Synthesis ◽  
Crystalline Materials ◽  
Room Temperature Synthesis ◽  
Covalent Interactions ◽  
Synthesis Approach

Abstract Covalent organic frameworks (COFs) are porous and crystalline materials which are formed based on the covalent interactions between the building monomers. These materials possess fascinating properties in terms of predesignable structure, controllable morphology, and manageable functionality which distinguished them from other polymers. COFs have also high chemical and physical stability, high surface area, and high adsorption capacity that these attributes make them excellent candidates for use in different fields. However, there are several approaches for the synthesis of COFs among which room-temperature synthesis approach is a green, versatile, and popular method which is due to its exceptional properties including simplicity, easy operation, and cost-effectiveness. In this regard, this review article presents a comprehensive view of the synthesis of COFs at room temperature as well as their applications, their limitations, and also their future perspectives.

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