Determination of strontium 90 in environmental samples by triple quadrupole ICP-MS and its application to Fukushima soil samples

2018 ◽  
Vol 33 (6) ◽  
pp. 1081-1085 ◽  
Author(s):  
Takeshi Ohno ◽  
Mutsumi Hirono ◽  
Shinichiro Kakuta ◽  
Shuhei Sakata
Keyword(s):  
Analytical Methods ◽  
Environmental Samples ◽  
Soil Samples ◽  
Triple Quadrupole ◽  
Sample Throughput ◽  
Icp Ms ◽  
Strontium 90

The determination of 90Sr by triple quadrupole ICP-MS is capable of providing a high sample throughput compared with radiometric analytical methods.

Ultratrace Determination of Strontium-90 in Environmental Soil Samples From Qatar by Collision/Reaction Cell-Inductively Coupled Plasma Mass Spectrometry (CRC-ICP-MS/MS)

2013 ◽  
Author(s):  
S. H. Al-Meer ◽  
M. A. Amr ◽  
A. I. Helal ◽  
A. T. Al-Kinani
Keyword(s):  
Mass Spectrometry ◽  
Inductively Coupled Plasma ◽  
Soil Samples ◽  
Standard Reference Materials ◽  
Reaction Cell ◽  
Hot Plate ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Strontium 90

Because of the very low level of 90Sr in the environmental soil samples and its determination by beta counting may take several weeks, we developed a procedure for ultratrace determination of 90Sr using collision reaction cell-inductively coupled plasma tandem mass spectrometry (CRC-ICP-MS/MS, Agilent 8800). Soil samples were dried at 105 °C and then heated in a furnace at 550 °C to remove any organics present. 500 g of each soil samples were aliquoted into 2000 ml glass beakers. Each Soils samples were soaked in 2 ppm Sr solution carrier to allow determination of chemical yield. The solid to liquid ratio was 1:1. Finally the soil samples were dried at 105 °C. Five hundred milliliters concentrated nitric acid and 250 ml hydrochloric acid volumes were added on 500 g soil samples. The samples were digested on hot plate at 80 °C to prevent spraying with continuous manual mixing. The leachate solution was separated. The solids were rinsed with 500 ml deionized water, warmed on a hot plate and the leachate plus previous leachate were filtered and the total volume was reduced to 500 ml by evaporation. Final leachate volume was transferred to a centrifuge tubes. The centrifuge tubes were centrifuged at 3,500 rpm for 10 min. The leachate was transferred to a 1 L beaker and heated on a hot plate to evaporate the leachate to dryness. The reside was re-dissolved in 100 ml of 2% HNO3 and reduced by evaporation to 10 mL. The solution was measured directly by CRC-ICP-MS/MS by setting the first quadruple analyzer to m/z 90 and introducing oxygen gas into the reaction cell for elimination isobar interference from zirconium-90. The method was validated by measurements of standard reference materials and applied on environmental soil samples. The overall time requirement for the measurement of strontium-90 by CRC-ICP-MS/MS is 2 days, significantly shorter than any radioanalytical protocol currently available.

Determination of ultratrace 129I in soil samples by Triple Quadrupole ICP-MS and its application to Fukushima soil samples

2013 ◽  
Vol 28 (8) ◽  
pp. 1283 ◽  
Author(s):  
Takeshi Ohno ◽  
Yasuyuki Muramatsu ◽  
Yasuyuki Shikamori ◽  
Chiaki Toyama ◽  
Nobuaki Okabe ◽  
...  
Keyword(s):  
Soil Samples ◽  
Triple Quadrupole ◽  
Icp Ms

Exploring the ability of triple quadrupole inductively coupled plasma mass spectrometry for the determination of Pu isotopes in environmental samples

2021 ◽  
Author(s):  
Wenting Bu ◽  
Mei Gu ◽  
Xiaotong Ding ◽  
Youyi Ni ◽  
Xuepeng Shao ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Environmental Samples ◽  
Inductively Coupled Plasma ◽  
Triple Quadrupole ◽  
Geochemical Processes ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Plasma Mass Spectrometry ◽  
Pu Isotopes

The monitoring of Pu isotopes in environmental samples was essential for radioactive assessment and tracing the geochemical processes. Triple quadrupole inductively coupled plasma mass spectrometry (ICP-MS/MS) has shown strong ability...

Determination of Mn, Fe, Ni, Cu, Zn, Cd and Pb in seawater using offline extraction and triple quadrupole ICP-MS/MS

2018 ◽  
Vol 33 (2) ◽  
pp. 304-313 ◽  
Author(s):  
S. L. Jackson ◽  
J. Spence ◽  
D. J. Janssen ◽  
A. R. S. Ross ◽  
J. T. Cullen
Keyword(s):  
Trace Elements ◽  
Spatial Distributions ◽  
Triple Quadrupole ◽  
Ocean Water ◽  
Sample Throughput ◽  
Accuracy And Precision ◽  
Icp Ms ◽  
Temporal And Spatial ◽  
Insight Into

Highly resolved temporal and spatial distributions of trace elements in ocean water can provide insight into ocean processes but carry a significant analytical demand which requires methods that combine accuracy and precision with high sample throughput.

scholarly journals Multi-residue analytical methods for the determination of pesticides and PPCPs in water by LC-MS/MS: a review

2012 ◽  
Vol 10 (3) ◽  
pp. 876-899 ◽  
Author(s):  
Ednei Primel ◽  
Sergiane Caldas ◽  
Ana Escarrone
Keyword(s):  
Mass Spectrometry ◽  
Analytical Methods ◽  
Environmental Samples ◽  
World Wide ◽  
Matrix Effects ◽  
Tandem Mass ◽  
Selective Determination ◽  
Chromatography Tandem Mass Spectrometry ◽  
Liquid Chromatography Tandem Mass

AbstractResidues of pesticides, pharmaceutical and personal care products (PPCPs) are contaminants of world-wide concern. Consequently, there is a growing need to develop reliable analytical methods, which enable rapid, sensitive and selective determination of these pollutants in environmental samples, at trace levels. In this paper, a review of the liquid chromatography-tandem mass spectrometry (LC-MS/MS) based methods for the determination of pesticides and PPCPs in the environment is presented. Advanced aspects of current LC-MS/MS methodology, including sample preparation and matrix effects, are discussed.

Ti-containing mesoporous silica packed microcolumn separation/preconcentration combined with inductively coupled plasma-mass spectrometry for the determination of trace Cr, Cu, Cd and Pb in environmental samples

2015 ◽  
Vol 30 (6) ◽  
pp. 1386-1394 ◽  
Author(s):  
Chao Cui ◽  
Hanyong Peng ◽  
Yanan Zhang ◽  
Kai Nan ◽  
Man He ◽  
...  
Keyword(s):  
Mesoporous Silica ◽  
Environmental Samples ◽  
Inductively Coupled Plasma ◽  
Solid Phase ◽  
Trace Metal Analysis ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Plasma Mass Spectrometry ◽  
Microcolumn Separation

Solid phase extraction with Ti-containing mesoporous silica as adsorbent combined with ICP-MS for trace metal analysis in environmental samples.

Multi-element determination of Pt, Pd and Ir traces in environmental samples by ICP-MS after pre-concentration

Talanta ◽  
2012 ◽  
Vol 99 ◽  
pp. 853-858 ◽  
Author(s):  
Manuel L. Alonso Castillo ◽  
Amparo García de Torres ◽  
Elisa Vereda Alonso ◽  
Ma Teresa Siles Cordero ◽  
José Manuel Cano Pavón
Keyword(s):  
Environmental Samples ◽  
Element Determination ◽  
Icp Ms

Determination of chloride in crude oils by direct dilution using inductively coupled plasma tandem mass spectrometry (ICP-MS/MS)

2019 ◽  
Vol 34 (7) ◽  
pp. 1433-1438 ◽  
Author(s):  
Jenny Nelson ◽  
Laura Poirier ◽  
Francisco Lopez-Linares
Keyword(s):  
Mass Spectrometry ◽  
Tandem Mass Spectrometry ◽  
Inductively Coupled Plasma ◽  
Crude Oils ◽  
Tandem Mass ◽  
Triple Quadrupole ◽  
Petroleum Crude ◽  
Inductively Coupled ◽  
Icp Ms

The potential of using inductively coupled plasma tandem mass spectrometry, ICP-MS/MS, (also known as triple quadrupole ICP-MS) for the determination of chloride in petroleum crude samples following direct dilution was investigated.

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