scholarly journals Direct solid state NMR observation of the 105Pd nucleus in inorganic compounds and palladium metal systems

2018 ◽  
Vol 20 (41) ◽  
pp. 26734-26743 ◽  
Author(s):  
Thomas J. N. Hooper ◽  
Thomas A. Partridge ◽  
Gregory J. Rees ◽  
Dean S. Keeble ◽  
Nigel A. Powell ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Inorganic Compounds ◽  
Palladium Metal ◽  
Direct Solid

Although 105Pd is a very challenging nucleus for solid state NMR, these initial observations demonstrate its potential for characterising catalytically relevant Pd metal systems.

Solid-state NMR characterization of the structure and thermal stability of hybrid organic–inorganic compounds based on a HLaNb2O7 Dion–Jacobson layered perovskite

2016 ◽  
Vol 18 (31) ◽  
pp. 21903-21912 ◽  
Author(s):  
Alice S. Cattaneo ◽  
Chiara Ferrara ◽  
Adriana Mossuto Marculescu ◽  
Francesco Giannici ◽  
Antonino Martorana ◽  
...  
Keyword(s):  
Thermal Stability ◽  
Solid State ◽  
Solid State Nmr ◽  
Inorganic Compounds ◽  
Layered Perovskite ◽  
Nmr Characterization ◽  
Thermal Stability Of

Hybrids obtained via intercalation of alkylamines or propanol show peculiar structure and thermal stability, which are influenced by the nature and the amount of the intercalated chains.

A natural abundance 77Se solid-state NMR study of inorganic compounds

2008 ◽  
Vol 34 (4) ◽  
pp. 224-227 ◽  
Author(s):  
T.F. Kemp ◽  
A. Wong ◽  
M.E. Smith ◽  
P.T. Bishop ◽  
N. Carthey
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Inorganic Compounds ◽  
Natural Abundance ◽  
Nmr Study

scholarly journals Bulk Hyperpolarization of Inorganic Materials

2021 ◽  
Vol 75 (4) ◽  
pp. 333-337
Author(s):  
Snædís Björgvinsdóttir ◽  
Lyndon Emsley
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Inorganic Compounds ◽  
Lithium Titanate ◽  
Inorganic Materials ◽  
Level Information ◽  
Recent Method ◽  
Nmr Sensitivity ◽  
Low Sensitivity

Solid-state NMR spectroscopy is a well-established method to obtain atomic-level information about the structure of inorganic materials, but its use is often limited by low sensitivity. We review how solvent generated dynamic nuclear polarization can be used to increase sensitivity in solid-state NMR of inorganic materials, with emphasis on our recent method for hyperpolarization of proton-free bulk. We use selected examples to show how overall gains in sensitivity can be observed in both the surface and bulk spectra of inorganic compounds such as lithium titanate. The hyperpolarization methods reviewed here can be used to improve NMR sensitivity for a range of inorganic materials.

A useful tool for the elaboration of new solid-state NMR experiments: PULSAR

1995 ◽  
Vol 92 ◽  
pp. 1939-1942 ◽  
Author(s):  
JP Amoureux ◽  
C Fernandez ◽  
Y Dumazy
Keyword(s):  
Solid State ◽  
Solid State Nmr
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