Multinuclear solid-state NMR study: a powerful tool for understanding the structure of ZnO hybrid nanoparticles

2018 ◽  
Vol 20 (18) ◽  
pp. 12413-12421 ◽  
Author(s):  
Grégory Spataro ◽  
Yohan Champouret ◽  
Pierre Florian ◽  
Yannik Coppel ◽  
Myrtil L. Kahn
Keyword(s):  
Solid State ◽  
Hybrid Materials ◽  
Solid State Nmr ◽  
Hybrid Nanoparticles ◽  
Nmr Study

Characterization of hybrid materials is crucial for gaining an in-depth understanding of nano-objects.

Synthesis and solid state NMR characterization of novel peptide/silica hybrid materials

2015 ◽  
Vol 72 ◽  
pp. 73-78 ◽  
Author(s):  
Mayke Werner ◽  
Andreas Heil ◽  
Niels Rothermel ◽  
Hergen Breitzke ◽  
Pedro Braga Groszewicz ◽  
...  
Keyword(s):  
Solid State ◽  
Hybrid Materials ◽  
Solid State Nmr ◽  
Nmr Characterization ◽  
Silica Hybrid

Synthesis and Characterization of a Novel Cyclic Aluminophosphinate:  Structure and Solid-State NMR Study

2002 ◽  
Vol 41 (4) ◽  
pp. 981-988 ◽  
Author(s):  
Thierry Azaïs ◽  
Laure Bonhomme-Coury ◽  
Jacqueline Vaissermann ◽  
Philippe Bertani ◽  
Jérôme Hirschinger ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Synthesis And Characterization ◽  
Nmr Study

scholarly journals Characterization of Bulk and Surface Chemical States on Electrochemically Cycled LiFePO4: A Solid State NMR Study

2014 ◽  
Vol 161 (6) ◽  
pp. A1012-A1018 ◽  
Author(s):  
Keiji Shimoda ◽  
Hidetaka Sugaya ◽  
Miwa Murakami ◽  
Hajime Arai ◽  
Yoshiharu Uchimoto ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Surface Chemical ◽  
Nmr Study ◽  
Chemical States

Structure, Mobility, and Interface Characterization of Self-Organized Organic−Inorganic Hybrid Materials by Solid-State NMR

1999 ◽  
Vol 121 (24) ◽  
pp. 5727-5736 ◽  
Author(s):  
Susan M. De Paul ◽  
Josef W. Zwanziger ◽  
Ralph Ulrich ◽  
Ulrich Wiesner ◽  
Hans W. Spiess
Keyword(s):  
Solid State ◽  
Hybrid Materials ◽  
Solid State Nmr ◽  
Inorganic Hybrid ◽  
Interface Characterization ◽  
Self Organized

scholarly journals Use of Solid-State NMR Spectroscopy for the Characterization of Molecular Structure and Dynamics in Solid Polymer and Hybrid Electrolytes

Polymers ◽  
2021 ◽  
Vol 13 (8) ◽  
pp. 1207
Author(s):  
Gabrielle Foran ◽  
Nina Verdier ◽  
David Lepage ◽  
Cédric Malveau ◽  
Nicolas Dupré ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Pulse Sequence ◽  
Dynamic Properties ◽  
Double Resonance ◽  
Solid Polymer ◽  
Pulse Field ◽  
Solid State Nmr Spectroscopy

Solid-state NMR spectroscopy is an established experimental technique which is used for the characterization of structural and dynamic properties of materials in their native state. Many types of solid-state NMR experiments have been used to characterize both lithium-based and sodium-based solid polymer and polymer–ceramic hybrid electrolyte materials. This review describes several solid-state NMR experiments that are commonly employed in the analysis of these systems: pulse field gradient NMR, electrophoretic NMR, variable temperature T1 relaxation, T2 relaxation and linewidth analysis, exchange spectroscopy, cross polarization, Rotational Echo Double Resonance, and isotope enrichment. In this review, each technique is introduced with a short description of the pulse sequence, and examples of experiments that have been performed in real solid-state polymer and/or hybrid electrolyte systems are provided. The results and conclusions of these experiments are discussed to inform readers of the strengths and weaknesses of each technique when applied to polymer and hybrid electrolyte systems. It is anticipated that this review may be used to aid in the selection of solid-state NMR experiments for the analysis of these systems.

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