Simultaneous ultrafast determination of six alkaloids in mainstream cigarette smoke by DART-MS/MS

2018 ◽  
Vol 10 (39) ◽  
pp. 4793-4800 ◽  
Author(s):  
Chao Li ◽  
E'xian Li ◽  
Yiqin Wu ◽  
Junheng You ◽  
Wei Liu ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Cigarette Smoke ◽  
Direct Analysis ◽  
Injection Rate ◽  
Ionization Technique ◽  
Extraction Solvent ◽  
Novel Method ◽  
Rate Type ◽  
Mainstream Cigarette Smoke

To determine nicotine, nornicotine, myosmine, anatabine, anabasine and nicotyrine in mainstream cigarette smoke simultaneously, a novel method based on Direct Analysis in Real Time (DART) Ionization technique combined with mass spectrometry was established by optimizing parameters such as injection rate, type of extraction solvent and extraction solvent dosage.

scholarly journals Quantitative Determination of Menthol in a Single Puff of Mainstream Cigarette Smoke

2013 ◽  
Vol 25 (5) ◽  
pp. 528-534
Author(s):  
NK Meruva ◽  
MT Smith ◽  
SE Plunkett
Keyword(s):  
Mass Spectrometry ◽  
Cigarette Smoke ◽  
Gas Chromatography Mass Spectrometry ◽  
Filter Method ◽  
Mainstream Smoke ◽  
Total Particulate Matter ◽  
The Individual ◽  
Single Puff ◽  
Mainstream Cigarette Smoke

AbstractA method for the determination of menthol in a single puff of mainstream cigarette smoke is reported. A rotary smoking machine with a twin filter interface was used to smoke cigarettes with varying menthol and “tar” deliveries determined based on the Cambridge filter method. The twin filter interface mechanically switches to a new filter pad for collection of smoke from each cigarette puff. The individual filter pad extracts were analyzed by gas chromatography-mass spectrometry (GC-MS) to determine menthol puff-by-puff deliveries. Menthol puff-by-puff profiles show an increase in menthol smoke delivery with increasing puff count, a trend consistent with total particulate matter and smoke delivery profiles of other mainstream smoke constituents. The sum of single puff menthol deliveries is comparable to the whole cigarette menthol smoke delivery as collected on a single filter pad. This method can also determine quantitative puff-by-puff deliveries of other mainstream cigarette smoke constituents.

Determination of ochratoxin A in wine by direct analysis in real time-tandem mass spectrometry

2017 ◽  
Vol 35 (2) ◽  
pp. 185 ◽  
Author(s):  
Xiaoming GONG ◽  
Ronghui MA ◽  
Hongtao WANG ◽  
Liqiang GUO ◽  
Kai LI ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Tandem Mass Spectrometry ◽  
Real Time ◽  
Ochratoxin A ◽  
Direct Analysis ◽  
Tandem Mass

Rapid analysis of four Sudan dyes using direct analysis in real time-mass spectrometry

2015 ◽  
Vol 7 (1) ◽  
pp. 86-90 ◽  
Author(s):  
Ze Li ◽  
Yi-Wei Zhang ◽  
Yi-Ding Zhang ◽  
Yu Bai ◽  
Hu-Wei Liu
Keyword(s):  
Mass Spectrometry ◽  
Real Time ◽  
Rapid Determination ◽  
Direct Analysis ◽  
Rapid Analysis ◽  
Sudan Dyes ◽  
Chili Powder

A simple direct analysis in a real time-mass spectrometry (DART-MS) method was developed for the rapid determination of four Sudan dyes (I–IV) in chili powder.

Determination of UV-327 and its metabolites in human urine using dispersive liquid-liquid microextraction and gas chromatography-tandem mass spectrometry

2021 ◽  
Vol 13 (35) ◽  
pp. 3978-3986
Author(s):  
Corinna Fischer ◽  
Thomas Göen
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Tandem Mass Spectrometry ◽  
Human Urine ◽  
Tandem Mass ◽  
Extraction Solvent ◽  
Chromatography Tandem Mass Spectrometry ◽  
Dispersive Liquid Liquid Microextraction ◽  
Liquid Microextraction

A method is presented for the extraction of the UV stabilizer UV-327 and its metabolites from urine with acetonitrile (disperser solvent) and chloroform (extraction solvent), followed by instrumental analysis of the trimethylsilylated analytes.

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