Gold nanocone arrays directly grown on nickel foam for improved SERS detection of aromatic dyes

2018 ◽  
Vol 10 (26) ◽  
pp. 3170-3177 ◽  
Author(s):  
Fugang Xu ◽  
Huasheng Lai ◽  
Hui Xu
Keyword(s):  
Nickel Foam ◽  
Sensitive Detection ◽  
Sers Substrate ◽  
Ni Foam ◽  
Sers Detection

An efficient SERS substrate composed of gold nanocone arrays with abundant sharp tips directly grown on 3D porous Ni foam (AuNCA@Ni foam) was developed for sensitive detection of aromatic dyes.

Recasting Ni-foam into NiF2 nanorod arrays via a hydrothermal process for hydrogen evolution reaction application

2021 ◽  
Author(s):  
Nanasaheb M. Shinde ◽  
Siddheshwar D. Raut ◽  
Balaji G. Ghule ◽  
Krishna Chaitanya Gunturu ◽  
James J. Pak ◽  
...  
Keyword(s):  
Hydrogen Evolution ◽  
Hydrogen Evolution Reaction ◽  
Nickel Foam ◽  
Hydrothermal Process ◽  
Reduction Process ◽  
Nanorod Arrays ◽  
Ni Foam

A promising electrode for hydrogen evolution reaction (HER) has been prepared via a reduction process to form NiF2 nanorod arrays directly grown on a 3D nickel foam.

Vertically oriented Ni3S2/RGO/Ni3S2 nanosheets on Ni foam for superior supercapacitors

RSC Advances ◽  
2015 ◽  
Vol 5 (78) ◽  
pp. 63528-63536 ◽  
Author(s):  
Chongjun Zhao ◽  
Zhuomin Zhang ◽  
Qian Wang ◽  
Shudi Min ◽  
Xiuzhen Qian
Keyword(s):  
Sandwich Structure ◽  
Nickel Foam ◽  
Hydrothermal Process ◽  
Ni Foam ◽  
One Step

A unique sandwich structure of Ni3S2/RGO/Ni3S2 was designed on nickel foam by a one-step hydrothermal process.

Facile growth of transition metal hydroxide nanosheets on porous nickel foam for efficient electrooxidation of benzyl alcohol

2021 ◽  
Vol 23 (19) ◽  
pp. 7825-7830
Author(s):  
Liying Ming ◽  
Xiao-Yuan Wu ◽  
Sa-Sa Wang ◽  
Weiming Wu ◽  
Can-Zhong Lu
Keyword(s):  
Transition Metal ◽  
Benzyl Alcohol ◽  
Nickel Foam ◽  
Metal Hydroxide ◽  
Porous Nickel ◽  
Ni Foam ◽  
Electrodeposition Method

Porous transition metal hydroxide nanosheet/Ni foam electrodes were prepared by a facile electrodeposition method for efficient electrooxidation of benzyl alcohol.

scholarly journals Commercial Gold Nanoparticles on Untreated Aluminum Foil: Versatile, Sensitive, and Cost-Effective SERS Substrate

2017 ◽  
Vol 2017 ◽  
pp. 1-8 ◽  
Author(s):  
Kristina Gudun ◽  
Zarina Elemessova ◽  
Laura Khamkhash ◽  
Ekaterina Ralchenko ◽  
Rostislav Bukasov
Keyword(s):  
Gold Nanoparticles ◽  
Low Cost ◽  
Aluminum Foil ◽  
Cost Effective ◽  
Sers Substrate ◽  
Au Film ◽  
Response Range ◽  
Sers Detection ◽  
Film Substrate ◽  
Linear Response Range

We introduce low-cost, tunable, hybrid SERS substrate of commercial gold nanoparticles on untreated aluminum foil (AuNPs@AlF). Two or three AuNP centrifugation/resuspension cycles are proven to be critical in the assay preparation. The limits of detection (LODs) for 4-nitrobenzenethiol (NBT) and crystal violet (CV) on this substrate are about 0.12 nM and 0.19 nM, respectively, while maximum analytical SERS enhancement factors (AEFs) are about 107. In comparative assays LODs for CV measured on AuNPs@Au film and AuNPs@glass are about 0.35 nM and 2 nM, respectively. The LOD for melamine detected on AuNPs@ Al foil is 27 ppb with 3 orders of magnitude for linear response range. Overall, AuNPs@AlF demonstrated competitive performance in comparison with AuNPs@ Au film substrate in SERS detection of CV, NBT, and melamine. To check the versatility of the AuNPs@AlF substrate we also detected KNO3 with LODs of 0.7 mM and SERS EF around 2 × 103, which is on the same order with SERS EF reported for this compound in the literature.

scholarly journals Application of Aluminum Hydroxide for Improvement of Label-Free SERS Detection of Some Cephalosporin Antibiotics in Urine

Biosensors ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 91 ◽  
Author(s):  
Natalia E. Markina ◽  
Alexey V. Markin
Keyword(s):  
Aluminum Hydroxide ◽  
Surface Enhanced Raman Spectroscopy ◽  
Negative Influence ◽  
Quantitative Detection ◽  
Therapeutic Drug ◽  
Excitation Wavelength ◽  
Sers Substrate ◽  
Label Free ◽  
Surface Enhanced Raman ◽  
Sers Detection

This report is dedicated to development of surface-enhanced Raman spectroscopy (SERS) based analysis protocol for detection of antibiotics in urine. The key step of the protocol is the pretreatment of urine before the detection to minimize background signal. The pretreatment includes extraction of intrinsic urine components using aluminum hydroxide gel (AHG) and further pH adjusting of the purified sample. The protocol was tested by detection of a single antibiotic in artificially spiked samples of real urine. Five antibiotics of cephalosporin class (cefazolin, cefoperazone, cefotaxime, ceftriaxone, and cefuroxime) were used for testing. SERS measurements were performed using a portable Raman spectrometer with 638 nm excitation wavelength and silver nanoparticles as SERS substrate. The calibration curves of four antibiotics (cefuroxime is the exception) cover the concentrations required for detection in patient’s urine during therapy (25/100‒500 μg/mL). Random error of the analysis (RSD < 20%) and limits of quantification (20‒90 μg/mL) for these antibiotics demonstrate the applicability of the protocol for reliable quantitative detection during therapeutic drug monitoring. The detection of cefuroxime using the protocol is not sensitive enough, allowing only for qualitative detection. Additionally, time stability and batch-to-batch reproducibility of AHG were studied and negative influence of the pretreatment protocol and its limitations were estimated and discussed.

scholarly journals Preparation of Hydrophobic Film by Electrospinning for Rapid SERS Detection of Trace Triazophos

Sensors ◽  
2020 ◽  
Vol 20 (15) ◽  
pp. 4120
Author(s):  
Fei Shao ◽  
Jiaying Cao ◽  
Ye Ying ◽  
Ying Liu ◽  
Dan Wang ◽  
...  
Keyword(s):  
Hot Spots ◽  
Large Scale ◽  
Limit Of Detection ◽  
Small Region ◽  
Sers Substrate ◽  
Ag Nps ◽  
Electrospinning Technique ◽  
Heterocyclic Molecules ◽  
Surface Enhanced Raman ◽  
Sers Detection

For real application, it is an urgent demand to fabricate stable and flexible surface-enhanced Raman scattering (SERS) substrates with high enhancement factors in a large-scale and facile way. Herein, by using the electrospinning technique, a hydrophobic and flexible poly(styrene-co-butadiene) (SB) fibrous membrane is obtained, which is beneficial for modification of silver nanoparticles (Ag NPs) colloid in a small region and then formation of more “hot spots” by drying; the final SERS substrate is designated as Ag/SB. Hydrophobic Ag/SB can efficiently capture heterocyclic molecules into the vicinity of hot spots of Ag NPs. Such Ag/SB films are used to quantitatively detect trace triazophos residue on fruit peels or in the juice, and the limit of detection (LOD) of 2.5 × 10−8 M is achieved. Ag/SB films possess a capability to resist heat. As a case, 6-mercaptopurine (6MP) that just barely dissolves in 90 °C water is picked for conducting Ag/SB-film-based experiments.

Effect of Dealloying Process on Microstructure and Electrochemical Properties of Ni Foam

2018 ◽  
Vol 922 ◽  
pp. 3-7
Author(s):  
Guang Ya Hou ◽  
Ji Yu Li ◽  
Lian Kui Wu ◽  
Yi Ping Tang ◽  
Hua Zhen Cao ◽  
...  
Keyword(s):  
Electrochemical Properties ◽  
Electroless Plating ◽  
Electrochemical Etching ◽  
Nickel Foam ◽  
Chemical Properties ◽  
Ni Foam ◽  
Electrochemical Testing ◽  
Cu Alloy ◽  
Hierarchical Pore ◽  
Counter Diffusion

Ni foam with 3D porous structure has attracted attention in the field of catalysis. Expanding the specific surface area of Ni foam is an important method to enhance its chemical properties. In this study, the Cu-Ni/Ni foam were obtained by electroless plating copper on Ni foam and then heat treatment for homogenizing at 750°C. The dealloying of the Cu-Ni/Ni foam was carried out by electrochemical etching for obtaining the Ni foam with hierarchical pore structure. The microstructure, phase and electrochemical performance were characterized by SEM, XRD and electrochemical testing. The results showed that the optimized temperature of electroless plating Cu on Ni foam is 60oC. Ni-Cu alloy can be obtained by counter diffusion above 750°C. With prolonging time of etching, the content of Cu component decreased and the size of pores on the sturts of the Cu-Ni/Ni foam changed from nano to micro scale. The electrochemical properties of the alloywere significantly higher than that of the pure nickel foam.

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