scholarly journals Design and 3D printing of a stainless steel reactor for continuous difluoromethylations using fluoroform

2017 ◽  
Vol 2 (6) ◽  
pp. 919-927 ◽  
Author(s):  
Bernhard Gutmann ◽  
Manuel Köckinger ◽  
Gabriel Glotz ◽  
Tania Ciaglia ◽  
Eyke Slama ◽  
...  

The design and 3D printing of a stainless steel reactor for reaction with a gaseous reagent is described.

1982 ◽  
Vol 47 (7) ◽  
pp. 1838-1847 ◽  
Author(s):  
Martin Bajus ◽  
Jozef Baxa

Pyrolysis of tetraline, decaline, 1,1'-bicyclohexane, cyclohexylbenzene and gas oil was studied in stainless steel and quartz flow tubular reactors at 780 and 800 °C, residence time 0.08 to 0.5 s and at the mass ratio of steam to the raw material changing from 0.5 to 1.5. The effect of reaction temperature, the mass ratio of steam to the raw material, reactor material and of the added elemental sulphur on the yields of individual reaction products is reported. Of bicyclic hydrocarbons, condensed hydrocarbons are more stable than those with noncondensed rings, cyclanoaromates being more stable than bicyclanes. Pyrolysis of gas oil in the stainless steel reactor yields greater amounts of ethylene, propylene, butadiene and smaller amounts of methane and ethane, compared to the pyrolysis carried out under identical conditions in the quartz reactor. Elemental sulphur increases the conversion of gas oil into gaseous pyrolysis products.


2009 ◽  
Vol 23 (11) ◽  
pp. 5663-5676 ◽  
Author(s):  
Julien Gornay ◽  
Lucie Coniglio ◽  
Francis Billaud ◽  
Gabriel Wild

2017 ◽  
Vol 62 (3) ◽  
pp. 345-350 ◽  
Author(s):  
José Miguel Hidalgo-Herrador ◽  
Zdeněk Tišler

Two VOx/SBA-15 catalysts and three VOx/SiO2-fumed silica, with 5, 10 and 1, 5, 10 %wt. vanadium content respectively, were tested in a stainless steel continuous flow reactor for the partial oxidation of ethanol. The catalysts were tested at 150 – 300 °C. Products were analyzed by GC-FID, GC-OFID and GC-MS. The aim was exploring the problematics which could be found when more industrial close conditions are used. The total conversion of ethanol and selectivity to acetaldehyde were different than the expected ones. For VOx/SiO2-fumed silica, the total conversion was higher with a lower selectivity to acetaldehyde compared to VOx/SBA-15 catalysts.


Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 774 ◽  
Author(s):  
Damir Godec ◽  
Santiago Cano ◽  
Clemens Holzer ◽  
Joamin Gonzalez-Gutierrez

Fused filament fabrication (FFF) combined with debinding and sintering could be an economical process for three-dimensional (3D) printing of metal parts. In this paper, compounding, filament making, and FFF processing of feedstock material with 55% vol. of 17-4PH stainless steel powder in a multicomponent binder system are presented. The experimental part of the paper encompasses central composite design for optimization of the most significant 3D printing parameters (extrusion temperature, flow rate multiplier, and layer thickness) to obtain maximum tensile strength of the 3D-printed specimens. Here, only green specimens were examined in order to be able to determine the optimal parameters for 3D printing. The results show that the factor with the biggest influence on the tensile properties was flow rate multiplier, followed by the layer thickness and finally the extrusion temperature. Maximizing all three parameters led to the highest tensile properties of the green parts.


2017 ◽  
Vol 134 ◽  
pp. 218-223 ◽  
Author(s):  
Glauco R. Betemps ◽  
Lucas A. Silveira ◽  
Daniele M. Sampaio ◽  
Mozart D. Bispo ◽  
Laiza C. Krause ◽  
...  

2017 ◽  
Vol 48 (10) ◽  
pp. 4831-4841 ◽  
Author(s):  
Lina Ji ◽  
Changzhen Wang ◽  
Wenjie Wu ◽  
Chao Tan ◽  
Guoyu Wang ◽  
...  

1988 ◽  
Vol 2 (3) ◽  
pp. 278-282 ◽  
Author(s):  
Richard H. Schlosberg ◽  
W. N. Olmstead ◽  
M. A. Francisco ◽  
A. Lindgren

The Analyst ◽  
2014 ◽  
Vol 139 (24) ◽  
pp. 6343-6347 ◽  
Author(s):  
S. Sandron ◽  
B. Heery ◽  
V. Gupta ◽  
D. A. Collins ◽  
E. P. Nesterenko ◽  
...  

3D printing of metal alloys, both stainless steel and titanium, has been used for the creation of long capillary columns (600 mm) within small footprint designs (30 mm × 58 mm) for use in high-pressure liquid chromatography applications.


2019 ◽  
Vol 2019 (04) ◽  
pp. 3338-3346
Author(s):  
P. Masek ◽  
T. Fornusek ◽  
P. Zeman ◽  
M. Bucko ◽  
J. Smolik ◽  
...  

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