Microwave-assisted fast synthesis of hierarchical NiCo2O4 nanoflower-like supported Ni(OH)2 nanoparticles with an enhanced electrocatalytic activity towards methanol oxidation

2018 ◽  
Vol 5 (1) ◽  
pp. 172-182 ◽  
Author(s):  
Bingrong Wang ◽  
Yang Cao ◽  
Yong Chen ◽  
Ruzhi Wang ◽  
Xiaohong Wang ◽  
...  
Keyword(s):  
Hydrothermal Method ◽  
Methanol Oxidation ◽  
Electrocatalytic Activity ◽  
Homogeneous Precipitation ◽  
Microwave Assisted ◽  
Supported Ni ◽  
Fast Synthesis

NiCo2O4/Ni(OH)2 synthesizing through microwave-assisted hydrothermal method and coordination of homogeneous precipitation, exhibiting excellent electrocatalytic activity.

Hydrothermal synthesis of Pt–Ag alloy nano-octahedra and their enhanced electrocatalytic activity for the methanol oxidation reaction

Nanoscale ◽  
2014 ◽  
Vol 6 (21) ◽  
pp. 12310-12314 ◽  
Author(s):  
Geng-Tao Fu ◽  
Ru-Guang Ma ◽  
Xue-Qing Gao ◽  
Yu Chen ◽  
Ya-Wen Tang ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Hydrothermal Method ◽  
Methanol Oxidation ◽  
Electrocatalytic Activity ◽  
Oxidation Reaction ◽  
Methanol Oxidation Reaction ◽  
High Quality ◽  
One Pot

High-quality Pt48Ag52 alloy nano-octahedra are synthesized via one-pot hydrothermal method showing excellent electrocatalytic activity and stability for methanol oxidation reaction.

Fast synthesis of Na2Ti3O7 system synthesized by microwave-assisted hydrothermal method: Electrical properties

2020 ◽  
Vol 46 (15) ◽  
pp. 23834-23839
Author(s):  
L.A.L. Basilio ◽  
F. Xavier ◽  
J.C.C. Sales ◽  
J.C.S. Andrade ◽  
J. Anglada- Rivera ◽  
...  
Keyword(s):  
Electrical Properties ◽  
Hydrothermal Method ◽  
Microwave Assisted ◽  
Fast Synthesis

Ultra Fast Hematite Preparation using a Microwave-Assisted Hydrothermal Method

2013 ◽  
Vol 3 (4) ◽  
pp. 477-484
Author(s):  
Arnayra Silva ◽  
Jefferson Andrade ◽  
Graziela Casali ◽  
Severino Lima ◽  
Elson Longo ◽  
...  
Keyword(s):  
Hydrothermal Method ◽  
Microwave Assisted

Luminescent properties of Y(OH)3: Tb nanopowders synthesized by microwave-assisted hydrothermal method

2019 ◽  
Vol 21 (5) ◽  
Author(s):  
I. A. Garduño-Wilches ◽  
G. Alarcón-Flores ◽  
S. Carmona-Téllez ◽  
J. Guzmán ◽  
M. Aguilar-Frutis
Keyword(s):  
Hydrothermal Method ◽  
Luminescent Properties ◽  
Microwave Assisted

scholarly journals Microwave-Assisted vs. Conventional Hydrothermal Synthesis of MoS2 Nanosheets: Application towards Hydrogen Evolution Reaction

Crystals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1040 ◽  
Author(s):  
Getachew Solomon ◽  
Raffaello Mazzaro ◽  
Vittorio Morandi ◽  
Isabella Concina ◽  
Alberto Vomiero
Keyword(s):  
Hydrothermal Synthesis ◽  
Hydrothermal Method ◽  
Hydrogen Evolution ◽  
Hydrogen Evolution Reaction ◽  
Current Density ◽  
Crystal Morphology ◽  
Synthesis Method ◽  
Synthesis Methods ◽  
Mos2 Nanosheets ◽  
Microwave Assisted

Molybdenum sulfide (MoS2) has emerged as a promising catalyst for hydrogen evolution applications. The synthesis method mainly employed is a conventional hydrothermal method. This method requires a longer time compared to other methods such as microwave synthesis methods. There is a lack of comparison of the two synthesis methods in terms of crystal morphology and its electrochemical activities. In this work, MoS2 nanosheets are synthesized using both hydrothermal (HT-MoS2) and advanced microwave methods (MW-MoS2), their crystal morphology, and catalytical efficiency towards hydrogen evolution reaction (HER) were compared. MoS2 nanosheet is obtained using microwave-assisted synthesis in a very short time (30 min) compared to the 24 h hydrothermal synthesis method. Both methods produce thin and aggregated nanosheets. However, the nanosheets synthesized by the microwave method have a less crumpled structure and smoother edges compared to the hydrothermal method. The as-prepared nanosheets are tested and used as a catalyst for hydrogen evolution results in nearly similar electrocatalytic performance. Experimental results showed that: HT-MoS2 displays a current density of 10 mA/cm2 at overpotential (−280 mV) compared to MW-MoS2 which requires −320 mV to produce a similar current density, suggesting that the HT-MoS2 more active towards hydrogen evolutions reaction.

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