An efficient microwave-assisted hydrothermal synthesis of high-quality CuInZnS/ZnS quantum dots

2018 ◽  
Vol 42 (6) ◽  
pp. 4102-4108 ◽  
Author(s):  
Yang Liu ◽  
Xueqian Chen ◽  
Qiang Ma
Keyword(s):  
Quantum Dots ◽  
Hydrothermal Synthesis ◽  
Hydrothermal Method ◽  
High Quality ◽  
Microwave Assisted

In this study, we proposed a microwave-assisted hydrothermal method to synthesize novel CuInZnS/ZnS quantum dots (QDs).

scholarly journals Microwave-Assisted vs. Conventional Hydrothermal Synthesis of MoS2 Nanosheets: Application towards Hydrogen Evolution Reaction

Crystals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1040 ◽  
Author(s):  
Getachew Solomon ◽  
Raffaello Mazzaro ◽  
Vittorio Morandi ◽  
Isabella Concina ◽  
Alberto Vomiero
Keyword(s):  
Hydrothermal Synthesis ◽  
Hydrothermal Method ◽  
Hydrogen Evolution ◽  
Hydrogen Evolution Reaction ◽  
Current Density ◽  
Crystal Morphology ◽  
Synthesis Method ◽  
Synthesis Methods ◽  
Mos2 Nanosheets ◽  
Microwave Assisted

Molybdenum sulfide (MoS2) has emerged as a promising catalyst for hydrogen evolution applications. The synthesis method mainly employed is a conventional hydrothermal method. This method requires a longer time compared to other methods such as microwave synthesis methods. There is a lack of comparison of the two synthesis methods in terms of crystal morphology and its electrochemical activities. In this work, MoS2 nanosheets are synthesized using both hydrothermal (HT-MoS2) and advanced microwave methods (MW-MoS2), their crystal morphology, and catalytical efficiency towards hydrogen evolution reaction (HER) were compared. MoS2 nanosheet is obtained using microwave-assisted synthesis in a very short time (30 min) compared to the 24 h hydrothermal synthesis method. Both methods produce thin and aggregated nanosheets. However, the nanosheets synthesized by the microwave method have a less crumpled structure and smoother edges compared to the hydrothermal method. The as-prepared nanosheets are tested and used as a catalyst for hydrogen evolution results in nearly similar electrocatalytic performance. Experimental results showed that: HT-MoS2 displays a current density of 10 mA/cm2 at overpotential (−280 mV) compared to MW-MoS2 which requires −320 mV to produce a similar current density, suggesting that the HT-MoS2 more active towards hydrogen evolutions reaction.

Rapid microwave assisted hydrothermal synthesis of porous α-Fe2O3 nanostructures as stable and high capacity negative electrode for lithium and sodium ion batteries

RSC Advances ◽  
2015 ◽  
Vol 5 (44) ◽  
pp. 34761-34768 ◽  
Author(s):  
B. Nageswara Rao ◽  
P. Ramesh Kumar ◽  
O. Padmaraj ◽  
M. Venkateswarlu ◽  
N. Satyanarayana
Keyword(s):  
Hydrothermal Synthesis ◽  
Hydrothermal Method ◽  
High Capacity ◽  
Negative Electrode ◽  
Sodium Ion ◽  
Sodium Ion Batteries ◽  
Base Catalyst ◽  
Microwave Assisted

Porous α-Fe2O3 nanostructures were developed in the presence of a base catalyst by a rapid microwave assisted hydrothermal method.

Hydrothermal synthesis of Pt–Ag alloy nano-octahedra and their enhanced electrocatalytic activity for the methanol oxidation reaction

Nanoscale ◽  
2014 ◽  
Vol 6 (21) ◽  
pp. 12310-12314 ◽  
Author(s):  
Geng-Tao Fu ◽  
Ru-Guang Ma ◽  
Xue-Qing Gao ◽  
Yu Chen ◽  
Ya-Wen Tang ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Hydrothermal Method ◽  
Methanol Oxidation ◽  
Electrocatalytic Activity ◽  
Oxidation Reaction ◽  
Methanol Oxidation Reaction ◽  
High Quality ◽  
One Pot

High-quality Pt48Ag52 alloy nano-octahedra are synthesized via one-pot hydrothermal method showing excellent electrocatalytic activity and stability for methanol oxidation reaction.

Microwave-assisted hydrothermal synthesis of amorphous MoS2 catalysts and their activities in the hydrodeoxygenation of p-cresol

RSC Advances ◽  
2016 ◽  
Vol 6 (84) ◽  
pp. 80641-80648 ◽  
Author(s):  
Kui Wu ◽  
Weiyan Wang ◽  
Song Tan ◽  
Guohua Zhu ◽  
Liang Tan ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
High Activity ◽  
Hydrothermal Method ◽  
Microwave Assisted ◽  
Mos2 Catalysts

MoS2 was fast synthesized by microwave-assisted hydrothermal method using MoCl5 and (NH2)2CS as starting materials and exhibited high activity: the deoxygenation degree reached to 92.4% in the HDO of p-cresol at 300 °C for 6 h.

Microwave-assisted aqueous synthesis of Mn-doped ZnS quantum dots and their room-temperature phosphorescence detection of indapamide

2014 ◽  
Vol 6 (18) ◽  
pp. 7489-7495 ◽  
Author(s):  
Dong Zhu ◽  
Wei Li ◽  
Hong-Mei Wen ◽  
Qian Chen ◽  
Li Ma ◽  
...  
Keyword(s):  
Aqueous Solution ◽  
Quantum Dots ◽  
Room Temperature ◽  
Synthetic Approach ◽  
Room Temperature Phosphorescence ◽  
High Quality ◽  
Aqueous Synthesis ◽  
Microwave Assisted ◽  
Mn Doped

High-quality Mn-doped ZnS QDs were prepared using a green and rapid microwave-assisted synthetic approach in an aqueous solution, which were used for room-temperature phosphorescence (RTP) detection of indapamide.

scholarly journals Hydrothermal synthesis of nitrogen and boron doped carbon quantum dots with yellow-green emission for sensing Cr(vi), anti-counterfeiting and cell imaging

RSC Advances ◽  
2017 ◽  
Vol 7 (76) ◽  
pp. 48386-48393 ◽  
Author(s):  
Yongming Guo ◽  
Yuzhi Chen ◽  
Fengpu Cao ◽  
Lijuan Wang ◽  
Zhuo Wang ◽  
...  
Keyword(s):  
Quantum Dots ◽  
Hydrothermal Synthesis ◽  
Hydrothermal Method ◽  
Cell Imaging ◽  
Green Emission ◽  
Carbon Quantum Dots ◽  
Fluorometric Detection ◽  
Great Stability ◽  
Boron Doped ◽  
Co Doped

Nitrogen and boron co-doped carbon quantum dots with great stability in high-salt conditions and good photostability are prepared through hydrothermal method and utilized for fluorometric detection of Cr(vi), anti-counterfeiting and cell imaging.

Microwave-assisted hydrothermal synthesis of solid-state carbon dots with intensive emission for white light-emitting devices

2017 ◽  
Vol 5 (32) ◽  
pp. 8105-8111 ◽  
Author(s):  
Jingxia Zheng ◽  
Yaling Wang ◽  
Feng Zhang ◽  
Yongzhen Yang ◽  
Xuguang Liu ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Solid State ◽  
Hydrothermal Method ◽  
White Light ◽  
Carbon Dots ◽  
Light Emitting ◽  
Light Emitting Devices ◽  
Microwave Assisted ◽  
State Luminescence

Carbon dots synthesized by a microwave-assisted hydrothermal method exhibit efficient solid-state luminescence for white light-emitting devices.

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