scholarly journals Integrated microHall magnetometer to measure the magnetic properties of nanoparticles

Lab on a Chip ◽  
2017 ◽  
Vol 17 (23) ◽  
pp. 4000-4007 ◽  
Author(s):  
Changwook Min ◽  
Jongmin Park ◽  
Jae Kyoung Mun ◽  
Yongjun Lim ◽  
Jouha Min ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Small Sample ◽  
Hall Magnetometer

We developed an integrated Hall magnetometer to measure magnetic properties in small sample volumes.

scholarly journals Magnetic properties of pseudotachylytes from western Jämtland, central Swedish Caledonides

Solid Earth ◽  
2020 ◽  
Vol 11 (3) ◽  
pp. 807-828
Author(s):  
Bjarne S. G. Almqvist ◽  
Hagen Bender ◽  
Amanda Bergman ◽  
Uwe Ring
Keyword(s):  
Magnetic Properties ◽  
Magnetic Susceptibility ◽  
Magnetic Anisotropy ◽  
Small Sample ◽  
Magnetic Fabric ◽  
Seismic Slip ◽  
Magnetic Fabrics ◽  
Principal Axes ◽  
Nappe Complex ◽  
Fault Kinematics

Abstract. Fault kinematics can provide information on the relationship and assembly of tectonic units in an orogen. Magnetic fabric studies of faults where pseudotachylytes form have recently been used to determine direction and sense of seismic slip in prehistoric earthquakes. Here we apply this methodology to study magnetic fabrics of pseudotachylytes in field structures of the Köli Nappe Complex (central Swedish Caledonides), with the aim to determine fault kinematics and decipher the role of seismic faulting in the assembly of the Caledonian nappe pile. Because the pseudotachylyte veins are thin, we focused on small (ca. 0.2 to 0.03 cm3) samples for measuring the anisotropy of magnetic susceptibility. The small sample size challenges conventional use of magnetic anisotropy and results acquired from such small specimens demand cautious interpretation. Importantly, we find that magnetic fabric results show inverse proportionality among specimen size, degree of magnetic anisotropy and mean magnetic susceptibility, which is most likely an analytical artifact related to instrument sensitivity and small sample dimensions. In general, however, it is shown that the principal axes of magnetic susceptibility correspond to the orientation of foliation and lineation, where the maximum susceptibility (k1) is parallel to the mineral lineation, and the minimum susceptibility (k3) is dominantly oriented normal to schistosity. Furthermore, the studied pseudotachylytes develop distinct magnetic properties. Pristine pseudotachylytes preserve a signal of ferrimagnetic magnetite that likely formed during faulting. In contrast, portions of the pseudotachylytes have altered, with a tendency of magnetite to break down to form chlorite. Despite magnetite breakdown, the altered pseudotachylyte mean magnetic susceptibility is nearly twice that of altered pseudotachylyte, likely originating from the Fe-rich chlorite, as implied by temperature-dependent susceptibility measurements and thin-section observations. Analysis of structural and magnetic fabric data indicates that seismic faulting occurred during exhumation into the upper crust, but these data yield no kinematic information on the direction and sense of seismic slip. Additionally, the combined structural field and magnetic fabric data suggest that seismic faulting was postdated by brittle E–W extensional deformation along steep normal faults. Although the objective of finding kinematic indicators for the faulting was not fully achieved, we believe that the results from this study may help guide future studies of magnetic anisotropy with small specimens (<1 cm3), as well as in the interpretation of magnetic properties of pseudotachylytes.

scholarly journals Versatile Hall magnetometer with variable sensitivity assembly for characterization of the magnetic properties of nanoparticles

2019 ◽  
Vol 489 ◽  
pp. 165431 ◽  
Author(s):  
Jefferson F.D.F. Araujo ◽  
Daniel R.P. Vieira ◽  
Fredy Osorio ◽  
Walmir E. Pöttker ◽  
Felipe A. La Porta ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Hall Magnetometer ◽  
Variable Sensitivity

AEM analysis of crystallization in Ti-based amorphous alloys

1983 ◽  
Vol 41 ◽  
pp. 270-271
Author(s):  
A.R. Pelton ◽  
A.F. Marshall ◽  
Y.S. Lee
Keyword(s):  
Magnetic Properties ◽  
Amorphous Alloys ◽  
Amorphous Materials ◽  
Isothermal Annealing ◽  
Amorphous Matrix ◽  
Nucleation And Growth ◽  
Current Interest ◽  
Amorphous Films ◽  
Electrical And Magnetic Properties

Amorphous materials are of current interest due to their desirable mechanical, electrical and magnetic properties. Furthermore, crystallizing amorphous alloys provides an avenue for discerning sequential and competitive phases thus allowing access to otherwise inaccessible crystalline structures. Previous studies have shown the benefits of using AEM to determine crystal structures and compositions of partially crystallized alloys. The present paper will discuss the AEM characterization of crystallized Cu-Ti and Ni-Ti amorphous films.Cu60Ti40: The amorphous alloy Cu60Ti40, when continuously heated, forms a simple intermediate, macrocrystalline phase which then transforms to the ordered, equilibrium Cu3Ti2 phase. However, contrary to what one would expect from kinetic considerations, isothermal annealing below the isochronal crystallization temperature results in direct nucleation and growth of Cu3Ti2 from the amorphous matrix.

Probing the ultrastructure of the mitotic and meiotic spindle in eggs: An expeditious approach based on semi-thin (0.25 μm) serial sections

1983 ◽  
Vol 41 ◽  
pp. 552-555
Author(s):  
Conly L. Rieder ◽  
S. Bowser ◽  
R. Nowogrodzki ◽  
K. Ross ◽  
G. Sluder
Keyword(s):  
Small Sample Size ◽  
Small Sample ◽  
Meiotic Spindle ◽  
Serial Sections ◽  
Mitotic Apparatus ◽  
Thin Sections ◽  
Cell Cycles ◽  
Ultrastructural Studies

Eggs have long been a favorite material for studying the mechanism of karyokinesis in-vivo and in-vitro. They can be obtained in great numbers and, when fertilized, divide synchronously over many cell cycles. However, they are not considered to be a practical system for ultrastructural studies on the mitotic apparatus (MA) for several reasons, the most obvious of which is that sectioning them is a formidable task: over 1000 ultra-thin sections need to be cut from a single 80-100 μm diameter egg and of these sections only a small percentage will contain the area or structure of interest. Thus it is difficult and time consuming to obtain reliable ultrastructural data concerning the MA of eggs; and when it is obtained it is necessarily based on a small sample size.We have recently developed a procedure which will facilitate many studies concerned with the ultrastructure of the MA in eggs. It is based on the availability of biological HVEM's and on the observation that 0.25 μm thick serial sections can be screened at high resolution for content (after mounting on slot grids and staining with uranyl and lead) by phase contrast light microscopy (LM; Figs 1-2).

Microstructure in soft magnetic E3 (S1, Al) (Sendust) alloys

1988 ◽  
Vol 46 ◽  
pp. 770-771
Author(s):  
June D. Kim
Keyword(s):  
Electron Microscopy ◽  
Magnetic Properties ◽  
Ternary Phase Diagram ◽  
Vertical Tube ◽  
Vacuum Induction Melting ◽  
Induction Melting ◽  
Soft Magnetic ◽  
Quenching Temperature ◽  
Thin Foils ◽  
Vertical Tube Furnace

Iron-base alloys containing 8-11 wt.% Si, 4-8 wt.% Al, known as “Sendust” alloys, show excellent soft magnetic properties. These magnetic properties are strongly dependent on heat treatment conditions, especially on the quenching temperature following annealing. But little has been known about the microstructure and the Fe-Si-Al ternary phase diagram has not been established. In the present investigation, transmission electron microscopy (TEM) has been used to study the microstructure in a Sendust alloy as a function of temperature.An Fe-9.34 wt.% Si-5.34 wt.% Al (approximately Fe3Si0.6Al0.4) alloy was prepared by vacuum induction melting, and homogenized at 1,200°C for 5 hrs. Specimens were heat-treated in a vertical tube furnace in air, and the temperature was controlled to an accuracy of ±2°C. Thin foils for TEM observation were prepared by jet polishing using a mixture of perchloric acid 15% and acetic acid 85% at 10V and ∼13°C. Electron microscopy was performed using a Philips EM 301 microscope.

Magnetic properties of new charge-transfer complexes based on manganese porphyrins

1997 ◽  
Vol 90 (3) ◽  
pp. 407-413
Author(s):  
MARC KELEMEN ◽  
CHRISTOPH WACHTER ◽  
HUBERT WINTER ◽  
ELMAR DORMANN ◽  
RUDOLF GOMPPER ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Charge Transfer ◽  
Charge Transfer Complexes ◽  
Manganese Porphyrins

Validating the Factor Structure of the Stigma of Suicide Scale–Short Form Spanish Version Among Healthcare Students

Crisis ◽  
2020 ◽  
pp. 1-5
Author(s):  
Ruthmarie Hernández-Torres ◽  
Paola Carminelli-Corretjer ◽  
Nelmit Tollinchi-Natali ◽  
Ernesto Rosario-Hernández ◽  
Yovanska Duarté-Vélez ◽  
...  
Keyword(s):  
Factor Structure ◽  
Structural Equation ◽  
Short Form ◽  
Small Sample Size ◽  
Small Sample ◽  
Spanish Version ◽  
Equation Modeling ◽  
Cross Sectional ◽  
Healthcare Students ◽  
Spanish Speaking

Abstract. Background: Suicide is a leading cause of death among Spanish-speaking individuals. Suicide stigma can be a risk factor for suicide. A widely used measure is the Stigma of Suicide Scale-Short Form (SOSS-SF; Batterham, Calear, & Christensen, 2013 ). Although the SOSS-SF has established psychometric properties and factor structure in other languages and cultural contexts, no evidence is available from Spanish-speaking populations. Aim: This study aims to validate a Spanish translation of the SOSS-SF among a sample of Spanish-speaking healthcare students ( N = 277). Method: We implemented a cross-sectional design with quantitative techniques. Results: Following a structural equation modeling approach, a confirmatory factor analysis (CFA) supported the three-factor model proposed by Batterham and colleagues (2013) . Limitations: The study was limited by the small sample size and recruitment by availability. Conclusion: Findings suggest that the Spanish version of the SOSS-SF is a valid and reliable tool with which to examine suicide stigma among Spanish-speaking populations.

An Initial Investigation of Suicide Attempt Disclosures Among US Veterans

Crisis ◽  
2020 ◽  
pp. 1-7
Author(s):  
Brooke A. Ammerman ◽  
Sarah P. Carter ◽  
Heather M. Gebhardt ◽  
Jonathan Buchholz ◽  
Mark A. Reger
Keyword(s):  
Suicide Attempt ◽  
Mental Health Professionals ◽  
Help Seeking ◽  
Psychiatric Treatment ◽  
Small Sample Size ◽  
Romantic Partners ◽  
Small Sample ◽  
Professional Care ◽  
Patient Disclosure ◽  
Previous Suicide Attempt

Abstract. Background: Patient disclosure of prior suicidal behaviors is critical for effectively managing suicide risk; however, many attempts go undisclosed. Aims: The current study explored how responses following a suicide attempt disclosure may relate to help-seeking outcomes. Method: Participants included 37 veterans with a previous suicide attempt receiving inpatient psychiatric treatment. Veterans reported on their most and least helpful experiences disclosing their suicide attempt to others. Results: Veterans disclosed their suicide attempt to approximately eight individuals. Mental health professionals were the most cited recipient of their most helpful disclosure; romantic partners were the most common recipient of their least helpful disclosures. Positive reactions within the context of the least helpful disclosure experience were positively associated with a sense of connection with the disclosure recipient. Positive reactions within the most helpful disclosure experience were positively associated with the likelihood of future disclosure. No reactions were associated with having sought professional care or likelihood of seeking professional care. Limitations: The results are considered preliminary due to the small sample size. Conclusion: Findings suggest that while positive reactions may influence suicide attempt disclosure experiences broadly, additional research is needed to clarify factors that drive the decision to disclose a suicide attempt to a professional.

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