Direct thermal desorption gas chromatographic determination of toxicologically relevant concentrations of ethylene glycol in whole blood

The Analyst ◽  
2018 ◽  
Vol 143 (4) ◽  
pp. 963-969 ◽  
Author(s):  
James Robson ◽  
Stephen Townsend ◽  
Paul Bowdler ◽  
Kevin C. Honeychurch

A simple and rapid method involving thermal desorption gas chromatography (TD-GC) with flame ionisation detection has been successfully developed for the determination of ethylene glycol in whole blood.

1972 ◽  
Vol 55 (3) ◽  
pp. 657-659
Author(s):  
Alan R Hanks ◽  
Barbara S Engdahl

Abstract A simple and rapid method is desorihed for the determination of terraehlor in fertilizers. Terrachlor is extracted with chloroform, and aldrin is added as an internal standard. The extract is injected into a gas chromatography and peak height ratios are used for quantitative measurement. Analysis of commercial samples gives good precision while analysis of prepared samples gives recoveries ranging from 99.3 to 100.4%.


1974 ◽  
Vol 20 (7) ◽  
pp. 820-824 ◽  
Author(s):  
R L Peterson ◽  
D O Rodgerson

Abstract We have developed a method for detection and quantitation of ethylene glycol in serum, based on the gas chromatography of its dibenzoate ester. No special reagents or equipment are required. The method is virtually free of interference and sensitive to less than 0.02 mg of ethylene glycol per milliliter. The total analysis time is about 90 min.


2019 ◽  
Vol 37 (1) ◽  
pp. 116
Author(s):  
Chenliang FAN ◽  
Yuhong ZHANG ◽  
Chuan WANG ◽  
Zhenlei PENG ◽  
Zhirong GAO

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