Synthesis and characterization of trinuclear N-heterocyclic carbene–palladium(ii) complexes and their applications in the Suzuki–Miyaura cross-coupling reaction

RSC Advances ◽  
2016 ◽  
Vol 6 (103) ◽  
pp. 100690-100695 ◽  
Author(s):  
Tao Wang ◽  
Lantao Liu ◽  
Kai Xu ◽  
Huanping Xie ◽  
Hui Shen ◽  
...  
Keyword(s):  
Coupling Reaction ◽  
Cross Coupling ◽  
Synthesis And Characterization ◽  
Effective Catalyst ◽  
Cross Coupling Reaction ◽  
One Step

Five novel trinuclear N-heterocyclic carbene–palladium(ii) complexes 5a–e were conveniently synthesized in one step. The obtained palladium(ii) complexes were the effective catalyst precursors for the Suzuki–Miyaura coupling.

scholarly journals Synthesis and Characterization of N,N-Dimethylformamide-Protected Palladium Nanoparticles and Their Use in the Suzuki–Miyaura Cross-Coupling Reaction

ACS Omega ◽  
2020 ◽  
Vol 5 (16) ◽  
pp. 9598-9604
Author(s):  
Junya Ishida ◽  
Masato Nakatsuji ◽  
Tatsuki Nagata ◽  
Hideya Kawasaki ◽  
Takeyuki Suzuki ◽  
...  
Keyword(s):  
Palladium Nanoparticles ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Synthesis And Characterization ◽  
Cross Coupling Reaction

scholarly journals Synthesis and characterization of the cyanobenzene-ethylenedithio-TTF donor

2015 ◽  
Vol 11 ◽  
pp. 951-956 ◽  
Author(s):  
Sandrina Oliveira ◽  
Dulce Belo ◽  
Isabel Cordeiro Santos ◽  
Sandra Rabaça ◽  
Manuel Almeida
Keyword(s):  
Coupling Reaction ◽  
Cross Coupling ◽  
Triethyl Phosphite ◽  
High Yield ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cross Coupling Reaction ◽  
Uv Visible

A dissymmetric TTF-type electron donor, cyanobenzene-ethylenedithio-tetrathiafulvalene (CNB-EDT-TTF), was obtained in high yield, by a cross-coupling reaction with triethyl phosphite between 2-thioxobenzo[d][1,3]dithiole-5-carbonitrile and 5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-one. This new donor was characterized namely by single crystal X-ray diffraction, cyclic voltammetry, NMR, UV-visible and IR spectroscopy.

scholarly journals Green synthesis of graphene oxide (GO)-anchored Pd/Cu bimetallic nanoparticles using Ocimum sanctum as bio-reductant: an efficient heterogeneous catalyst for the Sonogashira cross-coupling reaction

RSC Advances ◽  
2020 ◽  
Vol 10 (39) ◽  
pp. 23108-23120 ◽  
Author(s):  
Samim Sultana ◽  
Swapna Devi Mech ◽  
Farhaz Liaquat Hussain ◽  
Pallab Pahari ◽  
Geetika Borah ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Reduction Method ◽  
Bimetallic Nanoparticles ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Synthesis And Characterization ◽  
Ocimum Sanctum ◽  
Cross Coupling Reaction ◽  
Efficient Heterogeneous Catalyst

Here we report the synthesis and characterization of graphene oxide anchored Pd–Cu bimetallic nanoparticles by bio reduction method and its application in Sonogashira cross-coupling reaction.

scholarly journals Synthesis of Functionalized Cannabilactones

Molecules ◽  
2020 ◽  
Vol 25 (3) ◽  
pp. 684
Author(s):  
Yingpeng Liu ◽  
Thanh C. Ho ◽  
Mohammed Baradwan ◽  
Maria Pascual Lopez-Alberca ◽  
Christos Iliopoulos-Tsoutsouvas ◽  
...  
Keyword(s):  
Coupling Reaction ◽  
Cross Coupling ◽  
New Approach ◽  
Structural Modifications ◽  
Cross Coupling Reaction ◽  
One Step

A new approach to synthesize cannabilactones using Suzuki cross-coupling reaction followed by one-step demethylation-cyclization is presented. The two key cannabilactone prototypes AM1710 and AM1714 were obtained selectively in high overall yields and in a lesser number of synthetic steps when compared to our earlier synthesis. The new approach expedited the synthesis of cannabilactone analogs with structural modifications at the four potential pharmacophoric regions.

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