Characterization of CuSbSe2 crystallites synthesized using a hot injection method

RSC Advances ◽  
2016 ◽  
Vol 6 (101) ◽  
pp. 99297-99305 ◽  
Author(s):  
Hsing-I. Hsiang ◽  
Chang-Ting Yang ◽  
Jui-Huan Tu
Keyword(s):  
Single Phase ◽  
Triethylene Glycol ◽  
Reducing Agent ◽  
Injection Method ◽  
Hot Injection ◽  
Low Toxic

In this study, a novel and facile hot injection method for the synthesis of single phase CuSbSe2 crystallites was developed by using low toxic triethylene glycol as both the solvent and reducing agent and triethylenetetramine as co-reducing agent.

scholarly journals Characterization of Cu2ZnSnS4 Particles Obtained by the Hot-Injection Method

ACS Omega ◽  
2020 ◽  
Vol 5 (18) ◽  
pp. 10501-10509
Author(s):  
Sara Engberg ◽  
Joanna Symonowicz ◽  
Jørgen Schou ◽  
Stela Canulescu ◽  
Kirsten M. Ø Jensen
Keyword(s):  
Injection Method ◽  
Hot Injection

scholarly journals Synthesis and characterization of CIGS ink by hot injection method

2020 ◽  
Author(s):  
Atika Sari Puspita Dewi ◽  
Bagas H. Arroyid ◽  
Nandang Mufti ◽  
Markus Diantoro ◽  
Arramel ◽  
...  
Keyword(s):  
Synthesis And Characterization ◽  
Injection Method ◽  
Hot Injection

scholarly journals Synthesis and Characterization of Colloidal CZTS Nanocrystals by a Hot-Injection Method

2016 ◽  
Vol 2016 ◽  
pp. 1-7 ◽  
Author(s):  
A. Méndez-López ◽  
A. Morales-Acevedo ◽  
Y. J. Acosta-Silva ◽  
M. Ortega-López
Keyword(s):  
Thin Films ◽  
Low Cost ◽  
Synthesis And Characterization ◽  
Wurtzite Phase ◽  
Synthesis Time ◽  
Injection Method ◽  
Hot Injection ◽  
Average Size ◽  
Czts Nanocrystals

The present study reports the synthesis of colloidal Cu2ZnSnS4(CZTS) nanocrystals (average size ~4–9 nm) by a simple and low cost hot-injection method. These nanocrystals form larger particles with sizes around 40 nm. Oleylamine (OLA) was used as both the solvent and the nanocrystal stabilizer. The effect of the synthesis time on the structural, compositional, morphological, and optical properties was studied. As revealed by XRD, Raman, and TEM measurements all the prepared samples are comprised of both kesterite and wurtzite CZTS nanocrystals. The wurtzite phase contribution reduces as the reaction time is increased. The “bandgap” of the obtained nanoparticles tends to 1.52 eV for the larger synthesis times (24 h) which is suitable for an absorber layer in thin films solar cells.

Analysis and characterization of iron pyrite nanocrystals and nanocrystalline thin films derived from bromide anion synthesis

2015 ◽  
Vol 3 (13) ◽  
pp. 6853-6861 ◽  
Author(s):  
Khagendra P. Bhandari ◽  
Paul J. Roland ◽  
Tyler Kinner ◽  
Yifang Cao ◽  
Hyekyoung Choi ◽  
...  
Keyword(s):  
Thin Films ◽  
Stable Phase ◽  
Iron Pyrite ◽  
Injection Method ◽  
Bromide Anion ◽  
Hot Injection ◽  
Phase Pure ◽  
Nanocrystalline Thin Films

We use a solution-based bromide anion hot injection method to synthesize stable, phase pure and highly crystalline cubic iron pyrite (FeS2) nanocrystals, with size varying from ∼70 to ∼150 nm.

Synthesis and 31 P NMR characterization of new low toxic highly sensitive pH probes designed for in vivo acidic pH studies

2002 ◽  
Vol 10 (5) ◽  
pp. 1451-1458 ◽  
Author(s):  
Sophie Martel ◽  
Jean-Louis Clément ◽  
Agnès Muller ◽  
Marcel Culcasi ◽  
Sylvia Pietri
Keyword(s):  
Acidic Ph ◽  
Highly Sensitive ◽  
Nmr Characterization ◽  
Low Toxic ◽  
Ph Probes

scholarly journals Fabrication and Characterization of Quinary High Entropy-Ultra-High Temperature Diborides

Ceramics ◽  
2021 ◽  
Vol 4 (2) ◽  
pp. 108-120
Author(s):  
Simone Barbarossa ◽  
Roberto Orrù ◽  
Valeria Cannillo ◽  
Antonio Iacomini ◽  
Sebastiano Garroni ◽  
...  
Keyword(s):  
High Temperature ◽  
Single Phase ◽  
Nominal Composition ◽  
High Entropy ◽  
Chemical Complexity ◽  
Alternative Processing ◽  
Plasma Sintering ◽  
High Temperature Synthesis ◽  
Spark Plasma

Due to their inherent chemical complexity and their refractory nature, the obtainment of highly dense and single-phase high entropy (HE) diborides represents a very hard target to achieve. In this framework, homogeneous (Hf0.2Nb0.2Ta0.2Mo0.2Ti0.2)B2, (Hf0.2Zr0.2Ta0.2Mo0.2Ti0.2)B2, and (Hf0.2Zr0.2Nb0.2Mo0.2Ti0.2)B2 ceramics with high relative densities (97.4, 96.5, and 98.2%, respectively) were successfully produced by spark plasma sintering (SPS) using powders prepared by self-propagating high-temperature synthesis (SHS). Although the latter technique did not lead to the complete conversion of initial precursors into the prescribed HE phases, such a goal was fully reached after SPS (1950 °C/20 min/20 MPa). The three HE products showed similar and, in some cases, even better mechanical properties compared to ceramics with the same nominal composition attained using alternative processing methods. Superior Vickers hardness and elastic modulus values were found for the (Hf0.2Nb0.2Ta0.2Mo0.2Ti0.2)B2 and the (Hf0.2Zr0.2Ta0.2Mo0.2Ti0.2)B2 systems, i.e., 28.1 GPa/538.5 GPa and 28.08 GPa/498.1 GPa, respectively, in spite of the correspondingly higher residual porosities (1.2 and 2.2 vol.%, respectively). In contrast, the third ceramic, not containing tantalum, displayed lower values of these two properties (25.1 GPa/404.5 GPa). However, the corresponding fracture toughness (8.84 MPa m1/2) was relatively higher. This fact can be likely ascribed to the smaller residual porosity (0.3 vol.%) of the sintered material.

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