Supramolecular porous ionic network based on triazinonide and imidazolium: a template-free synthesis of meso-/macroporous organic materials via a one-pot reaction-assembly procedure

RSC Advances ◽  
2016 ◽  
Vol 6 (95) ◽  
pp. 92443-92448 ◽  
Author(s):  
Ze-Huan Hei ◽  
Gan-Lin Song ◽  
Chen-Yu Zhao ◽  
Wenhao Fan ◽  
Mu-Hua Huang
Keyword(s):  
Organic Materials ◽  
Cyanuric Chloride ◽  
One Pot ◽  
Template Free ◽  
Assembly Procedure

A supramolecular porous ionic network (SPIN-1) was designed and prepared using a one-pot procedure, involving the quaternization of triimidazole triazine with cyanuric chloride followed by hydrolysis andin situassembly.

scholarly journals A facile one-pot synthesis of CaO/CuO hollow microspheres featuring highly porous shells for enhanced CO2 capture in a combined Ca–Cu looping process via a template-free synthesis approach

2019 ◽  
Vol 7 (37) ◽  
pp. 21096-21105 ◽  
Author(s):  
Jian Chen ◽  
Lunbo Duan ◽  
Tian Shi ◽  
Ruoyu Bian ◽  
Yuxiao Lu ◽  
...  
Keyword(s):  
Co2 Capture ◽  
High Performance ◽  
Hollow Microspheres ◽  
One Pot ◽  
One Pot Synthesis ◽  
Template Free ◽  
Synthesis Approach ◽  
Highly Porous

The preparation of CaO/CuO composites with high performance is essential for combined Ca–Cu looping process, where the exothermic reduction of CuO with methane is used in situ to calcine CaCO3.

scholarly journals Hollow Structured Li3VO4 Wrapped with Graphene Nanosheets in Situ Prepared by a One-Pot Template-Free Method as an Anode for Lithium-Ion Batteries

Nano Letters ◽  
2013 ◽  
Vol 13 (10) ◽  
pp. 4715-4720 ◽  
Author(s):  
Yi Shi ◽  
Jia-Zhao Wang ◽  
Shu-Lei Chou ◽  
David Wexler ◽  
Hui-Jun Li ◽  
...  
Keyword(s):  
Lithium Ion Batteries ◽  
Graphene Nanosheets ◽  
Lithium Ion ◽  
One Pot ◽  
Template Free

One-pot, template-free syntheses of spherical ZnS nanocrystals using a new S2−source and their photocatalytic study

CrystEngComm ◽  
2015 ◽  
Vol 17 (11) ◽  
pp. 2359-2367 ◽  
Author(s):  
Manjodh Kaur ◽  
Nipun Kumar Gupta ◽  
C. M. Nagaraja
Keyword(s):  
Solvothermal Method ◽  
Uv Light ◽  
Light Irradiation ◽  
Capping Agent ◽  
Good Activity ◽  
One Pot ◽  
Uv Light Irradiation ◽  
Template Free ◽  
Zns Nanocrystals

A facile, one-pot solvothermal method for the syntheses of template-free ZnS NCs (~3–6 nm) using (C7H7)S2as a newin situsource of S2−ions without and with the use of MCE-capping agent has been demonstrated. Photocatalytic investigation of the NCs revealed very good activity for degradation of MO under UV light irradiation.

Template-free syntheses of hierarchical PbS microstructures using a new sulphur source and their time-dependent morphological evolution and photocatalytic properties

RSC Advances ◽  
2016 ◽  
Vol 6 (62) ◽  
pp. 56790-56799 ◽  
Author(s):  
Manjodh Kaur ◽  
C. M. Nagaraja
Keyword(s):  
Morphological Evolution ◽  
Time Dependent ◽  
Photocatalytic Properties ◽  
One Pot ◽  
Sulphur Source ◽  
Solvothermal Route ◽  
Template Free ◽  
Temperature Controlled

Template-free PbS microstructures composed of nanocrystals exhibiting time-dependent morphological evolution from cubes to dendrites were synthesised by one-pot solvothermal route using DBDS as a new temperature controlled in situ source of S2− ions.

Indium Bromide-catalyzed Unprecedented Hydrogenolysis: A Novel One-Pot Synthesis of Per-O-Acetylated β-carboxymethyl O and S-glycosides

2020 ◽  
Vol 24 (8) ◽  
pp. 900-908
Author(s):  
Ram Naresh Yadav ◽  
Amrendra K Singh ◽  
Bimal Banik
Keyword(s):  
Asymmetric Synthesis ◽  
Chiral Auxiliary ◽  
Bioactive Molecules ◽  
One Pot ◽  
Enantiomerically Pure ◽  
Stereoselective Glycosylation ◽  
One Pot Synthesis ◽  
Wide Range

Numerous O (oxa)- and S (thia)-glycosyl esters and their analogous glycosyl acids have been accomplished through stereoselective glycosylation of various peracetylated bromo sugar with benzyl glycolate using InBr3 as a glycosyl promotor followed by in situ hydrogenolysis of resulting glycosyl ester. A tandem glycosylating and hydrogenolytic activity of InBr3 has been successfully investigated in a one-pot procedure. The resulting synthetically valuable and virtually unexplored class of β-CMGL (glycosyl acids) could serve as an excellent potential chiral auxiliary in the asymmetric synthesis of a wide range of enantiomerically pure medicinally prevalent β-lactams and other bioactive molecules of diverse medicinal interest.

scholarly journals NIR responsive tumor vaccine in situ for photothermal ablation and chemotherapy to trigger robust antitumor immune responses

2021 ◽  
Vol 19 (1) ◽  
Author(s):  
Lirong Zhang ◽  
Jingjing Zhang ◽  
Lixia Xu ◽  
Zijian Zhuang ◽  
Jingjin Liu ◽  
...  
Keyword(s):  
Immune Responses ◽  
Tumor Vaccine ◽  
Oxidative Polymerization ◽  
Delivery Mode ◽  
Tumor Treatment ◽  
One Pot ◽  
Photothermal Ablation ◽  
Prolonged Retention ◽  
The One

Abstract Background Therapeutic tumor vaccine (TTV) that induces tumor-specific immunity has enormous potentials in tumor treatment, but high heterogeneity and poor immunogenicity of tumor seriously impair its clinical efficacy. Herein, a novel NIR responsive tumor vaccine in situ (HA-PDA@IQ/DOX HG) was prepared by integrating hyaluronic acid functionalized polydopamine nanoparticles (HA-PDA NPs) with immune adjuvants (Imiquimod, IQ) and doxorubicin (DOX) into thermal-sensitive hydrogel. Results HA-PDA@IQ NPs with high photothermal conversion efficiency (41.2%) and T1-relaxation efficiency were using HA as stabilizer by the one-pot oxidative polymerization. Then, HA-PDA@IQ loaded DOX via π-π stacking and mixed with thermal-sensitive hydrogel to form the HA-PDA@IQ/DOX HG. The hydrogel-confined delivery mode endowed HA-PDA@IQ/DOX NPs with multiple photothermal ablation performance once injection upon NIR irradiation due to the prolonged retention in tumor site. More importantly, this mode enabled HA-PDA@IQ/DOX NPs to promote the DC maturation, memory T cells in lymphatic node as well as cytotoxic T lymphocytes in spleen. Conclusion Taken together, the HA-PDA@IQ/DOX HG could be served as a theranostic tumor vaccine for complete photothermal ablation to trigger robust antitumor immune responses.

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