scholarly journals Optical in situ study of de-alloying kinetics in nanoporous gold sponges

RSC Advances ◽  
2016 ◽  
Vol 6 (89) ◽  
pp. 85773-85778 ◽  
Author(s):  
M. C. Tai ◽  
A. Gentle ◽  
M. D. Arnold ◽  
M. B. Cortie

Nanoporous gold sponges are useful for a variety of applications but the kinetics of the dissolution process used to make them is not well understood.

1993 ◽  
Vol 03 (C9) ◽  
pp. C9-461-C9-467 ◽  
Author(s):  
M. Juez-Lorenzo ◽  
V. Kolarik ◽  
N. Eisenreich ◽  
W. Engel ◽  
A. J. Criado

2018 ◽  
Vol 25 (5) ◽  
pp. 1371-1378
Author(s):  
L. D. Connor ◽  
P. M. Mignanelli ◽  
K. A. Christofidou ◽  
N. G. Jones ◽  
A. R. Baker ◽  
...  

The new long duration experiment facility on beamline I11 at Diamond Light Source has been used to study the kinetics of sigma phase formation in three Cr–Co–Ni alloys. Diffraction data acquired during in situ exposure at 800°C for 50 d showed progressive increases in the sigma fraction. This was accompanied by changes in the proportions of the other phases, which differed markedly between the alloys studied. These results demonstrate the capabilities of the long duration facility for the study of metallurgical phenomena over periods of months to years, a capability not previously available at a synchrotron source.


2008 ◽  
Vol 42 (1) ◽  
pp. 74-79 ◽  
Author(s):  
A. N. Semenov ◽  
O. G. Lyublinskaya ◽  
V. A. Solov’ev ◽  
B. Ya. Mel’tser ◽  
S. V. Ivanov

1985 ◽  
Vol 62 ◽  
Author(s):  
Woonsup park ◽  
Samuel M. Allen

ABSTRACTThe migration kinetics of antiphase boundaries (APBs) in long-range ordered Fe-Al alloys are analyzed using in-situ hot-stage transmission electron microscopy, making it possible to observe the interfacial migration directly as it occurs. The observed domain structures are essentially two dimensional due to the thin foil configuration of the specimen, facilitating analytical interpretation of the data. By measuring the local curvatures and migration distances from a series of micrographs taken at a constant temperature, the proportionality constant relating velocity to curvature can be determined. This proportionality constant, called the mobility for APB migration, is found to be independent of the curvature for <100> APBs in Fe-27 atomic percent Al at 745K, having the value of 4.8×10−19 m2/s.


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