Glycidylmethacrylate based resin functionalized with graphene oxide for column preconcentration and trace determination of Cd(ii) and Ni(ii) in environmental and food samples

RSC Advances ◽  
2016 ◽  
Vol 6 (81) ◽  
pp. 77629-77635 ◽  
Author(s):  
Aminul Islam ◽  
Suneel Kumar

Graphene oxide decorated glycidylmethacrylate chelating resin was synthesized using a diethylenetriamine spacer arm and explored for the preconcentration/determination of Ni and Cd in environmental and food samples.

Author(s):  
Cengiz Soykan

The waste of trace metals are led the pollutions of water, soil and air. That’s why the accurate and sensitive identification of amount of trace metals in food samples and environment are gained importance in analytical chemistry because of their toxicity to human health. Besides, the direct determination of trace metals, presented at very low concentration especially in real samples, is difficult. In this content, before determination of trace metals by instrumental methods can be achieved successfully using separation/preconcentration procedures. The different synthesized chelating polymer resin adsorbents are successfully used for the SPE of trace metals. The trace metals, such as Cu, Cr, Co, Mn, Zn and Fe, are necessary for human health, when it has been taken at certain limits. But, the trace metals, such as Hg, Cd, Pb, Ni and As are toxic metals for the human body. About this, there are studies on the determination of trace elements and mineral in food samples and environment. In this study, new methods in the synthesis of (meth)acrylamides and use as a sorbent in the trace metals extraction was identified.


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