Magnetic molecularly imprinted polymers–silver nanoparticle based micro-solid phase extraction for the determination of polycyclic aromatic hydrocarbons in water samples

RSC Advances ◽  
2016 ◽  
Vol 6 (60) ◽  
pp. 54702-54708 ◽  
Author(s):  
Mostafa Khajeh ◽  
Marzieh Sharifirad ◽  
Mousa Bohlooli ◽  
Mansour Ghaffari-Moghaddam

In this study, an efficient and sensitive magnetic molecularly imprinted polymer–silver nanoparticle (MMIPS) system was successfully synthesized.

2018 ◽  
Vol 42 (19) ◽  
pp. 16144-16153 ◽  
Author(s):  
Arash Asfaram ◽  
Maryam Arabi ◽  
Abbas Ostovan ◽  
Hossein Sadeghi ◽  
Mehrorang Ghaedi

In the present study, a D-μ-SPE clean-up method was established for the analysis of quercetin in extracts of plants and food samples using a magnetic molecularly imprinted polymer as the sorbent by HPLC-UV detection.


The Analyst ◽  
2022 ◽  
Author(s):  
Ying Wang ◽  
Xiaomin Yang ◽  
Lin Pang ◽  
Pengfei Geng ◽  
Fang Mi ◽  
...  

Specific recognition and highly sensitive detection of biomarkers play an essential role in identifying, early diagnosis and prevention of many diseases. Magnetic molecularly imprinted polymers (MMIP) have been widely used...


2017 ◽  
Vol 9 (17) ◽  
pp. 2585-2589 ◽  
Author(s):  
Jieping Luo ◽  
Ning Chen ◽  
Zaiyue Yang ◽  
Jiyong Han ◽  
Wanying Zhu ◽  
...  

A reliable pretreatment method of magnetic molecularly imprinted polymers/dispersive solid-phase extraction was developed for selectivity and enrichment of targets.


2021 ◽  
Vol 50 (1) ◽  
pp. 123-133
Author(s):  
Siti Nurul Umira Mohd Sabari ◽  
Saw Hong Loh ◽  
Sazlinda Kamaruzaman ◽  
Noorfatimah Yahaya ◽  
Wan Mohd Afiq Wan Mohd Khalik

Sample pre-treatment is often the bottleneck in an analytical process. Due to the drawbacks of conventional sample pre-treatment methods, microextraction utilizing lower amounts of adsorbents and organic solvents are therefore favoured. A micro-solid phase extraction (μ-SPE) technique coupled with gas chromatography-flame ionization detection (GC-FID) was successfully developed for the analysis of selected polycyclic aromatic hydrocarbons (PA Hs), namely phenanthrene, fluoranthene, and pyrene, in environmental water. In this study, μ-SPE techniques using C18 and molecularly imprinted polymer (MIP) membranes were optimized, validated, and applied to the analysis of selected PA Hs in environmental water samples. The analytical merits were compared, and the two methods were evaluated in terms of linearity, repeatability, and relative recovery. Under the optimal extraction conditions, both μ-SPE techniques using either C18 or MIP membranes as the adsorbents offered comparable ultratrace analysis of the selected PA Hs in the range of 0.003 to 0.01 μg L–1. The extraction strength of C18 membranes was superior to that of MIP membranes for the extraction of low molecular weights PA Hs from water in the presence of humic acid as a matrix factor. The C18membranes overcome the non-covalence interaction between PA Hs and humic acid and thus achieve better recovery.


RSC Advances ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 5394-5401 ◽  
Author(s):  
Wei Huang ◽  
Xingyu Hou ◽  
Yukui Tong ◽  
Miaomiao Tian

Boronate-affinity magnetic hollow molecularly imprinted polymers were prepared with sialic acid (SA) as a template to selectively extract SA from serum samples coupled with HPLC-UV.


2014 ◽  
Vol 6 (15) ◽  
pp. 5546-5553 ◽  
Author(s):  
Ping-Ping Zhan ◽  
Wen-Jie Gong ◽  
Yong-Gang Zhao

Determination of ultratrace levels of BPA in water by MSPD with a core–shell nanoring amino-functionalized magnetic molecularly imprinted polymer adsorbent followed by UFLC-MS/MS.


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