Silica-supported NiO nanocomposites prepared via a sol–gel technique and their excellent catalytic performance for one-pot multicomponent synthesis of benzodiazepine derivatives under microwave irradiation

2017 ◽  
Vol 41 (13) ◽  
pp. 5893-5903 ◽  
Author(s):  
Zeba Nasir ◽  
Abad Ali ◽  
Mohammad Shakir ◽  
Rizwan Wahab ◽  
Shamsuzzaman Shamsuzzaman ◽  
...  

Heterogeneous and versatile NiO–SiO2 NCs were synthesized by a sol–gel technique and used as a catalyst for the one-pot multicomponent synthesis of benzodiazepines.

RSC Advances ◽  
2020 ◽  
Vol 10 (47) ◽  
pp. 28100-28105
Author(s):  
Hualiang An ◽  
Di Wang ◽  
Shuang Miao ◽  
Qiusheng Yang ◽  
Xinqiang Zhao ◽  
...  

The prepared Ni-IL/SiO2 catalyst exhibits an excellent catalytic performance in the one-pot synthesis of 2-propylheptanol: the yield of 2-propylheptanol attained 75.4%.


SynOpen ◽  
2021 ◽  
Author(s):  
Mina Ghassemi ◽  
Ali Maleki

Copper ferrite (CuFe2O4) magnetic nanoparticles (MNPs) were synthesized via thermal decomposition method and applied as a reusable and green catalyst in the synthesis of functionalized 4H-pyran derivatives using malononitrile, an aromatic aldehyde and a β-ketoester in ethanol at room temperature. Then it was characterized by Fourier transform infrared spectroscopy (FT-IR), energy-dispersive X-ray spectroscopy (EDX) analysis, scanning electron microscopy (SEM) images, thermo gravimetric and differential thermo gravimetric (TGA/DTG) analysis. The catalyst was recovered from the reaction mixture by applying an external magnet and decanting the mixture. Recycled catalyst was reused for several times without significant loss in its activity. Running the one-pot three-component reaction at room temperature, no use of eternal energy source and using a green solvent provide benign, mild, and environmentally friendly reaction conditions; as well, ease of catalyst recovering, catalyst recyclability, no use of column chromatography and good to excellent yields are extra advantages of this work.


Tetrahedron ◽  
2006 ◽  
Vol 62 (17) ◽  
pp. 4059-4064 ◽  
Author(s):  
Rina Ghosh ◽  
Swarupananda Maiti ◽  
Arijit Chakraborty ◽  
Santu Chakraborty ◽  
Alok K. Mukherjee

2018 ◽  
Vol 5 (1) ◽  
pp. 49-58 ◽  
Author(s):  
Yu.S. Demidova ◽  
I.L. Simakova ◽  
E.V. Suslov ◽  
K.P. Volcho ◽  
N.F. Salakhutdinov ◽  
...  

Abstract In the current work gold catalysts supported on both commercial oxides and oxides synthesized by the sol-gel method were used for the one-pot alcohol amination of myrtenol. In general, utilization of metal oxides synthesized by the sol-gel method as the gold catalyst support enhanced the knowledge regarding key parameters determining catalytic behavior. Synthesized alumina was characterized by stronger acid sites favoring primary amine accumulation on the catalyst surface, as compared to the commercial oxide. Utilization of mixed metal oxides synthesized by the sol-gel method resulted in the non-additive behavior of different oxides enhancing the catalytic activity. Introduction of ceria into alumina modified the support basicity resulting in more efficient alcohol activation.


2018 ◽  
Vol 48 (16) ◽  
pp. 2061-2073 ◽  
Author(s):  
Saba Kauser Jaweed Shaikh ◽  
Ravindra Ramappa Kamble ◽  
Shilpa M. Somagond ◽  
Atulkumar A. Kamble ◽  
Mahadev N. Kumbar

2015 ◽  
Vol 39 (6) ◽  
pp. 4647-4657 ◽  
Author(s):  
Balu L. Gadilohar ◽  
Haribhau S. Kumbhar ◽  
Ganapati S. Shankarling

The sequential one-pot multicomponent synthesis of Betti bases and bisamides using biodegradable choline persulfate.


2018 ◽  
Vol 8 (17) ◽  
pp. 4485-4493 ◽  
Author(s):  
J. Iglesias ◽  
J. A. Melero ◽  
G. Morales ◽  
M. Paniagua ◽  
B. Hernández ◽  
...  

Controlling the zirconia coating thickness in ZrO2-SBA-15 materials allows tuning their catalytic performance in the one-pot transformation of furfural into GVL.


2018 ◽  
Vol 42 (13) ◽  
pp. 10861-10867 ◽  
Author(s):  
Junling Tu ◽  
Jiaojiao Yuan ◽  
Shimin Kang ◽  
Yongjun Xu ◽  
Tiejun Wang

Fe3O4@C nanoparticles with tunable size exhibit excellent catalytic performance in the direct synthesis of gasoline fuels.


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