Synthesis of (E)-β-iodo vinylsulfones via iodine-promoted iodosulfonylation of alkynes with sodium sulfinates in an aqueous medium at room temperature

2017 ◽  
Vol 19 (5) ◽  
pp. 1255-1258 ◽  
Author(s):  
Yadong Sun ◽  
Ablimit Abdukader ◽  
Dong Lu ◽  
Haiyan Zhang ◽  
Chenjiang Liu

An efficient and facile molecular iodine-promoted method for the synthesis of (E)-β-iodo vinylsulfones with high regio- and stereoselectivity using water as the solvent at room temperature is presented.

RSC Advances ◽  
2016 ◽  
Vol 6 (27) ◽  
pp. 22320-22330 ◽  
Author(s):  
Nazia Kausar ◽  
Indranil Roy ◽  
Dipankar Chattopadhyay ◽  
Asish R. Das

Graphene oxide nanosheet catalyzed strategies for construction of 2,3-dihydroquinazolinones and quinazolin-4(3H)-ones starting from anthranilamide and an aldehyde/ketone in aqueous medium at room temperature have been realized.


2018 ◽  
Vol 3 (46) ◽  
pp. 13197-13206 ◽  
Author(s):  
Bipin Shinde ◽  
Santosh B. Kamble ◽  
Dattaprasad M. Pore ◽  
Prasad Gosavi ◽  
Amol Gaikwad ◽  
...  

2017 ◽  
Vol 19 (11) ◽  
pp. 7772-7787 ◽  
Author(s):  
Soumadwip Ghosh ◽  
Souvik Dey ◽  
Mahendra Patel ◽  
Rajarshi Chakrabarti

The folding/unfolding equilibrium of proteins in aqueous medium can be altered by adding small organic molecules generally termed as co-solvents.


2017 ◽  
Vol 19 (22) ◽  
pp. 5385-5389 ◽  
Author(s):  
Amrendra Kumar ◽  
Ramanand Ramanand ◽  
Narender Tadigoppula

An efficient and metal-free method has been developed for the synthesis of polysubstituted pyrrole derivatives with combination of sodium dodecyl sulphate (SDS) and Triton X-100 surfactants using water as a solvent at room temperature in 2–6 h and under microwave conditions (10 min) with good to excellent yields.


2019 ◽  
Vol 43 (42) ◽  
pp. 16441-16444 ◽  
Author(s):  
Zan Yang ◽  
Liping Hu ◽  
Ting Cao ◽  
Li An ◽  
Lijun Li ◽  
...  

Herein, an efficient, metal-free process for the α-C–H thiocyanation of enaminones was developed using PhI(OAc)2 as an oxidant at room temperature in an aqueous medium.


2020 ◽  
Vol 7 (2) ◽  
pp. 217-225
Author(s):  
Fatemeh K. Damghani ◽  
Hamzeh Kiyani ◽  
Seied A. Pourmousavi

A one-pot three-component reaction promoted by choline chloride: zinc(II) chloride deepeutectic solvent (ChCl-ZnCl2 DES) in an aqueous medium for the synthesis of several merocyanin dyes based on isoxazol-5(4H)-ones is presented. This three-component approach is efficient, clean, experimentally simple, convenient, safe, and environmentally friendly. This reaction was performed at room temperature without using energy sources such as heat, microwave and ultrasound waves. Nonuse of toxic solvents, available materials, one-vessel, no wasted reagents, simple preparation, and recyclability of DES are other important points of this method that is significant from the perspective of green chemistry.


Sign in / Sign up

Export Citation Format

Share Document