An efficient synthetic method for organometallic radicals: structures and properties of gold(i)-(nitronyl nitroxide)-2-ide complexes

2017 ◽  
Vol 46 (8) ◽  
pp. 2653-2659 ◽  
Author(s):  
Shuichi Suzuki ◽  
Sayaka Kira ◽  
Masatoshi Kozaki ◽  
Masaki Yamamura ◽  
Toru Hasegawa ◽  
...  
Keyword(s):  
Sodium Hydroxide ◽  
Phosphine Ligands ◽  
Synthetic Method ◽  
Nitronyl Nitroxide ◽  
Nitroxide Radicals ◽  
One Pot ◽  
One Pot Synthesis ◽  
Structures And Properties

One-pot synthesis of (nitronyl nitroxide)-gold(i)-phosphine (NN-Au-P) complexes has been developed using chloro(tetrahydrothiophene)gold(i), phosphine ligands, nitronyl nitroxide radicals, and sodium hydroxide.

One pot synthesis, crystal structures and properties of two new MOFs with imidazole-containing tripodal ligand

2014 ◽  
Vol 57 (11) ◽  
pp. 1514-1519 ◽  
Author(s):  
YunZhi Tang ◽  
YinMei Yu ◽  
JianBo Xiong ◽  
Qiong Yao ◽  
YuHui Tan ◽  
...  
Keyword(s):  
Crystal Structures ◽  
One Pot ◽  
Tripodal Ligand ◽  
One Pot Synthesis ◽  
Structures And Properties

scholarly journals A rare γ-pyranopyrazole skeleton: design, one-pot synthesis and computational study

2016 ◽  
Vol 14 (31) ◽  
pp. 7490-7494 ◽  
Author(s):  
Muhammed Üçüncü ◽  
Ceren Cantürk ◽  
Erman Karakuş ◽  
Hüseyin Zeybek ◽  
Uğur Bozkaya ◽  
...  
Keyword(s):  
Computational Study ◽  
Synthetic Method ◽  
One Pot ◽  
One Pot Synthesis

A base mediated one-pot, two-step synthetic method for constructing γ-pyranopyrazoles.

A facile one-pot synthesis of deep blue luminescent lead bromide perovskite microdisks

2015 ◽  
Vol 51 (91) ◽  
pp. 16385-16388 ◽  
Author(s):  
Zhao Yuan ◽  
Yu Shu ◽  
Yu Tian ◽  
Yan Xin ◽  
Biwu Ma
Keyword(s):  
Thin Films ◽  
Room Temperature ◽  
Quantum Yields ◽  
Synthetic Method ◽  
Lateral Size ◽  
One Pot ◽  
One Pot Synthesis ◽  
Deep Blue ◽  
Lead Bromide

We report a facile one-pot synthetic method to prepare highly luminescent layered lead(ii) bromide perovskite microdisks with the lateral size of a few micrometers and thickness of 100–150 nm, featuring narrow deep blue emissions with quantum yields of up to 53% in toluene solutions and thin films at room temperature.

scholarly journals One-pot synthesis, anti-tumor evaluation and structure–activity relationships of novel 25-OCH3-PPD derivatives

MedChemComm ◽  
2017 ◽  
Vol 8 (9) ◽  
pp. 1845-1849 ◽  
Author(s):  
Fan-Zhi Qu ◽  
Chen Zhao ◽  
Jia-Qing Cao ◽  
Yan Zhang ◽  
Yu-Qing Zhao
Keyword(s):  
Panax Ginseng ◽  
Synthetic Method ◽  
Lead Compound ◽  
One Pot ◽  
Structure Activity Relationships ◽  
One Pot Synthesis ◽  
Structure Activity

Based on the fact that 25-OCH3-PPD, a natural ginsengenin isolated from the leaves of Panax ginseng, is a promising lead compound, novel 25-OCH3-PPD derivatives were synthesized to find more potent anti-tumor agents by a simple and facile synthetic method.

scholarly journals One-Pot Synthesis of α-Substituted Acrylates

SynOpen ◽  
2018 ◽  
Vol 02 (02) ◽  
pp. 0161-0167
Author(s):  
Magdalini Matziari ◽  
Yixin Xie
Keyword(s):  
Amino Acids ◽  
Reaction Times ◽  
Synthetic Method ◽  
One Pot ◽  
Biologically Relevant ◽  
Mild Conditions ◽  
One Pot Synthesis ◽  
Acrylic Esters ◽  
Natural Amino Acids ◽  
Work Up

A simple and efficient synthetic method towards α-substituted acrylic esters has been developed using the Horner–Wadsworth–Emmons (HWE) reaction with HCHO after alkylation of phosphonoacetates in a one-pot reaction. This method allows the smooth introduction of various side-chains, such as natural amino acids and other biologically relevant substituents. The use of mild conditions, inexpensive reagents, short reaction times and simple work-up and purification steps provides an effective and general alternative to cumbersome multistep and low-yielding procedures described to date.

scholarly journals One-pot synthesis of substituted pyrrolo[3,4-b]pyridine-4,5-diones based on the reaction of N-(1-(4-hydroxy-6-methyl-2-oxo-2H-pyran-3-yl)-2-oxo-2-arylethyl)acetamide with amines

2019 ◽  
Vol 15 ◽  
pp. 2840-2846
Author(s):  
Valeriya G Melekhina ◽  
Andrey N Komogortsev ◽  
Boris V Lichitsky ◽  
Vitaly S Mityanov ◽  
Artem N Fakhrutdinov ◽  
...  
Keyword(s):  
Starting Material ◽  
Primary Amines ◽  
Synthetic Method ◽  
One Pot ◽  
One Pot Synthesis ◽  
Major Reaction Product ◽  
Major Reaction

The condensation of primary amines with N-(1-(4-hydroxy-6-methyl-2-oxo-2H-pyran-3-yl)-2-oxo-2-arylethyl)acetamides was explored. Thus, a previously unknown recyclization of the starting material was observed in acidic ethanol in the presence of an amine, which provided the corresponding dihydropyrrolone derivative as the major reaction product. Based on this transformation, a practical and convenient one-pot synthetic method for substituted pyrrolo[3,4-b]pyridin-5-ones could be devised.

One-pot synthesis of bi-metallic PdRu tripods as an efficient catalyst for electrocatalytic nitrogen reduction to ammonia

2019 ◽  
Vol 7 (2) ◽  
pp. 801-805 ◽  
Author(s):  
Hongjing Wang ◽  
Yinghao Li ◽  
Chunjie Li ◽  
Kai Deng ◽  
Ziqiang Wang ◽  
...  
Keyword(s):  
Synthetic Method ◽  
One Pot ◽  
Efficient Catalyst ◽  
Nitrogen Reduction ◽  
One Pot Synthesis ◽  
One Step

A very simple one-step synthetic method is developed for fabrication of PdRu tripods for electrochemical nitrogen reduction to ammonia.

Transition-metal-free, one-pot synthesis of Benzoxaboroles from o-bromobenzaldehydes via visible-light-promoted borylation

2021 ◽  
Author(s):  
Jinghan Luo ◽  
Xingxing Jia ◽  
Yanjun Hu ◽  
Jianchao Chen ◽  
Tiemin Sun
Keyword(s):  
Transition Metal ◽  
Visible Light ◽  
Synthetic Method ◽  
One Pot ◽  
Metal Free ◽  
One Pot Synthesis ◽  
Stepwise Method

A novel and simple one-pot stepwise method to synthesize benzoxaboroles was demonstrated. This step-by-step synthetic method includes photocatalytic boronization with phenothiazine as photocatalyst and sequencely water-induced reduction in the presence...

scholarly journals Rhodium (II)-Catalyzed Synthesis of Tetracyclic 3,4-Fused Indoles and Dihydroindoles

Catalysts ◽  
2020 ◽  
Vol 10 (8) ◽  
pp. 920
Author(s):  
Hongwei Qiao ◽  
Jiakun Bai ◽  
Mengyao Zhu ◽  
Juanhong Gao ◽  
Anna ◽  
...  
Keyword(s):  
Synthetic Method ◽  
One Pot ◽  
One Pot Synthesis ◽  
Fused Heterocycles ◽  
Xanthene Derivatives

An efficient synthetic method of tetracyclic 3,4-fused indoles and dihydroindoles via rhodium-catalyzed (3+2) cycloaddition of N-tosyl-4-(2-phenoxyphenyl)-1,2,3-triazole was described. The aromatized xanthene derivatives can be achieved in a one-pot synthesis starting from 1-ethynyl-2-phenoxybenzene. The xanthene-based fused heterocycles were considered as the valuable fluorophore.

scholarly journals A SIMPLE ONE-POT SYNTHESIS OF PYRIMIDO[4,5-C]PYRIDAZINES AND IN SILICO STUDIES OF HUMAN AKT1 INHIBITORS

2021 ◽  
Vol 9 (10) ◽  
pp. 136-142
Author(s):  
Laldingluaia Khiangte ◽  
Keyword(s):  
Binding Energy ◽  
Multicomponent Reaction ◽  
In Silico ◽  
Synthetic Method ◽  
Autodock Vina ◽  
One Pot ◽  
One Pot Synthesis ◽  
In Silico Studies ◽  
Inhibitory Activities

A simple one-pot and efficient synthetic method for the synthesis of pyrimido[4,5-c]pyridazine by a multicomponent reaction. The synthesis compounds are study for their inhibitory activities towards AKT1 pathways by using in silico method. It was found that all compounds have binding energy lower than -7.9 kcal/mol and compound 3a is the most active with binding energy -9.65 kcal/mol, which have been performed using autodock vina.

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