bcTol: a highly water-soluble biradical for efficient dynamic nuclear polarization of biomolecules

2016 ◽  
Vol 52 (43) ◽  
pp. 7020-7023 ◽  
Author(s):  
Anil P. Jagtap ◽  
Michel-Andreas Geiger ◽  
Daniel Stöppler ◽  
Marcella Orwick-Rydmark ◽  
Hartmut Oschkinat ◽  
...  
Keyword(s):  
Solid State ◽  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Water Soluble ◽  
Glycerol Water

The crystalline spirocyclohexanolyl-derived nitroxide biradical bcTol was shown to have unprecedented solubility in glycerol/water mixtures and display a large DNP enhancement (244) for a sample of a microcrystalline SH3 protein by solid-state NMR.

scholarly journals TinyPols: a family of water-soluble binitroxides tailored for dynamic nuclear polarization enhanced NMR spectroscopy at 18.8 and 21.1 T

2020 ◽  
Vol 11 (10) ◽  
pp. 2810-2818 ◽  
Author(s):  
Alicia Lund ◽  
Gilles Casano ◽  
Georges Menzildjian ◽  
Monu Kaushik ◽  
Gabriele Stevanato ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Magnetic Fields ◽  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Water Soluble ◽  
High Magnetic Fields ◽  
Solid State Nmr Spectroscopy ◽  
Enhancement Factors

TinyPol binitroxides provide significantly higher DNP enhancement factors for solid-state NMR spectroscopy at high magnetic fields than today's reference radical AMPUPol.

scholarly journals Dynamic Nuclear Polarization / solid-state NMR of membranes. Thermal effects and sample geometry

2019 ◽  
Vol 100 ◽  
pp. 70-76 ◽  
Author(s):  
Evgeniy Sergeevich Salnikov ◽  
Fabien Aussenac ◽  
Sebastian Abel ◽  
Armin Purea ◽  
Paul Tordo ◽  
...  
Keyword(s):  
Solid State ◽  
Dynamic Nuclear Polarization ◽  
Thermal Effects ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Sample Geometry

scholarly journals Solid-State NMR/Dynamic Nuclear Polarization of Polypeptides in Planar Supported Lipid Bilayers

2015 ◽  
Vol 119 (46) ◽  
pp. 14574-14583 ◽  
Author(s):  
Evgeniy S. Salnikov ◽  
Hiba Sarrouj ◽  
Christian Reiter ◽  
Christopher Aisenbrey ◽  
Armin Purea ◽  
...  
Keyword(s):  
Solid State ◽  
Lipid Bilayers ◽  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Supported Lipid Bilayers

scholarly journals Solid-state NMR enhanced by dynamic nuclear polarization as a novel tool for ribosome structural biology

2013 ◽  
Vol 56 (2) ◽  
pp. 85-93 ◽  
Author(s):  
Ioannis Gelis ◽  
Veronika Vitzthum ◽  
Neha Dhimole ◽  
Marc A. Caporini ◽  
Andreas Schedlbauer ◽  
...  
Keyword(s):  
Solid State ◽  
Structural Biology ◽  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
Nuclear Polarization

Up to 100% Improvement in Dynamic Nuclear Polarization Solid-State NMR Sensitivity Enhancement of Polymers by Removing Oxygen

2015 ◽  
Vol 36 (15) ◽  
pp. 1416-1421 ◽  
Author(s):  
Dao Le ◽  
Fabio Ziarelli ◽  
Trang N. T. Phan ◽  
Giulia Mollica ◽  
Pierre Thureau ◽  
...  
Keyword(s):  
Solid State ◽  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Sensitivity Enhancement ◽  
Nmr Sensitivity

scholarly journals Improved Structural Elucidation of Synthetic Polymers by Dynamic Nuclear Polarization Solid-State NMR Spectroscopy

2013 ◽  
Vol 2 (8) ◽  
pp. 715-719 ◽  
Author(s):  
Olivier Ouari ◽  
Trang Phan ◽  
Fabio Ziarelli ◽  
Gilles Casano ◽  
Fabien Aussenac ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Synthetic Polymers ◽  
Structural Elucidation ◽  
Solid State Nmr Spectroscopy
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