Simultaneous determination of Pb and Cd in low-cost jewelry using differential pulse voltammetry

2016 ◽  
Vol 8 (45) ◽  
pp. 8028-8032
Author(s):  
Taimara Polidoro Ferreira ◽  
Rafael Arromba de Sousa ◽  
Denise Lowinsohn

The simultaneous electrochemical determination of lead (Pb) and cadmium (Cd) in low-cost jewelry was achieved using differential pulse voltammetry (DPV).

2021 ◽  
Author(s):  
Yan Jin ◽  
Tong QI ◽  
Yuqing Ge ◽  
Jin Chen ◽  
Li juan Liang ◽  
...  

In this paper, ultrasensitive electrochemical determination of phosphate in water is achieved by hydrophilic TiO2 modified glassy carbon electrodes for the first time. Differential pulse voltammetry (DPV) method is proposed...


2016 ◽  
Vol 6 (3) ◽  
pp. 265 ◽  
Author(s):  
Shreekant M Patil ◽  
Vijay P Pattar ◽  
Sharanappa T Nandibewoor

<p class="PaperAbstract"><span lang="EN-US">A sensitive and economic voltammetric method was developed for the simultaneous determination of acetaminophen (AMP) and metoclopramide (MCP) using pre-treated graphite pencil electrode (PTGPE). Compared to a graphite pencil electrode, the pre-treated electrode showed an apparent shift of the oxidation potentials in the positive direction and a notable enhancement in the current responses for both AMP and MCP. Cyclic voltammetry (CV) was used to study the voltammetric behavior of the drugs, while differential pulse voltammetry (DPV) was used to determine AMP and MCP simulta­neously. The dependence of the current on scan rate, pH and concentration was investi­gated to boost the experimental conditions for simultaneous determination. The calibra­tion curves were obtained over the range of 0.1</span><span lang="EN-US">×</span><span lang="EN-US">10<sup>-7</sup> to 1.1</span><span lang="EN-US">×</span><span lang="EN-US">10<sup>-7</sup> M, the concentration of each of both the drugs was varied by keeping the other constant, and achieved lower detection limit of 3.25 nM for AMP and 1.16 nM for MCP. The developed method was found to be selective and rapid for the simultaneous determination of AMP and MCP. The proposed method was applied simultaneously in real samples and pharmaceutical samples, with satisfactory results.</span></p>


Talanta ◽  
2019 ◽  
Vol 192 ◽  
pp. 439-447 ◽  
Author(s):  
Khalil Zarnousheh Farahani ◽  
Ali Benvidi ◽  
Masoud Rezaeinasab ◽  
Saleheh Abbasi ◽  
Mohammad Abdollahi-Alibeik ◽  
...  

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