Investigation of PDMS based bi-layer elasticity via interpretation of apparent Young's modulus

Soft Matter ◽  
2016 ◽  
Vol 12 (7) ◽  
pp. 2200-2207 ◽  
Author(s):  
Baptiste Sarrazin ◽  
Rémy Brossard ◽  
Patrick Guenoun ◽  
Florent Malloggi

As the need of new methods for the investigation of thin films on various kinds of substrates becomes greater, a novel approach based on AFM nanoindentation is explored. In particular, a successful method for the investigation of thin layers on soft substrates is demonstrated.

Coatings ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 153
Author(s):  
Chuen-Lin Tien ◽  
Tsai-Wei Lin

This paper proposes a measuring apparatus and method for simultaneous determination of the thermal expansion coefficient and biaxial Young’s modulus of indium tin oxide (ITO) thin films. ITO thin films simultaneously coated on N-BK7 and S-TIM35 glass substrates were prepared by direct current (DC) magnetron sputtering deposition. The thermo-mechanical parameters of ITO thin films were investigated experimentally. Thermal stress in sputtered ITO films was evaluated by an improved Twyman–Green interferometer associated with wavelet transform at different temperatures. When the heating temperature increased from 30 °C to 100 °C, the tensile thermal stress of ITO thin films increased. The increase in substrate temperature led to the decrease of total residual stress deposited on two glass substrates. A linear relationship between the thermal stress and substrate heating temperature was found. The thermal expansion coefficient and biaxial Young’s modulus of the films were measured by the double substrate method. The results show that the out of plane thermal expansion coefficient and biaxial Young’s modulus of the ITO film were 5.81 × 10−6 °C−1 and 475 GPa.


1999 ◽  
Vol 594 ◽  
Author(s):  
T. Y. Zhang ◽  
Y. J. Su ◽  
C. F. Qian ◽  
M. H. Zhao ◽  
L. Q. Chen

AbstractThe present work proposes a novel microbridge testing method to simultaneously evaluate the Young's modulus, residual stress of thin films under small deformation. Theoretic analysis and finite element calculation are conducted on microbridge deformation to provide a closed formula of deflection versus load, considering both substrate deformation and residual stress in the film. Silicon nitride films fabricated by low pressure chemical vapor deposition on silicon substrates are tested to demonstrate the proposed method. The results show that the Young's modulus and residual stress for the annealed silicon nitride film are respectively 202 GPa and 334.9 MPa.


2016 ◽  
Vol 18 (31) ◽  
pp. 21508-21517 ◽  
Author(s):  
Xiao-Ye Zhou ◽  
Bao-Ling Huang ◽  
Tong-Yi Zhang

Surfaces of nanomaterials play an essential role in size-dependent material properties.


1994 ◽  
Vol 60 (572) ◽  
pp. 1108-1113
Author(s):  
Hidetoshi Yanai ◽  
Nobuyuki Kishine ◽  
Yukari Komaba ◽  
Yukitaka Murakami

2012 ◽  
Vol 455-456 ◽  
pp. 8-12 ◽  
Author(s):  
Bin Li ◽  
Ping Xie ◽  
Su Ying Zhang ◽  
Ding Quan Liu

A mechanically robust infrared high-index coating material is essential to the infrared interference coatings. Lead germanium telluride (Pb1-xGexTe) is a pseudo-binary alloy of IV-VI narrow gap semiconductors of PbTe and GeTe. In our investigation, the hardness and Young’s modulus of thin films of Pb1-xGexTe, which were deposited on silicon substrates using electron beam evaporation, were identified by means of nanoindentation measurement. It is demonstrated that layers of Pb1-xGexTe have greater hardness and Young’s modulus compared with those of PbTe. These mechanical behaviors of layers can be linked to a ferroelectric phase transition from a cubic paraelectric phase to a rhombohedral, ferroelectric phase. Moreover, the strength loss in the layers of Pb1-xGexTe can be also explained in light of strong localized elastic-strain fields in concentrated solid solutions.


2021 ◽  
Author(s):  
Juan C Acosta ◽  
Mark E Curtis ◽  
Carl H Sondergeld ◽  
Chandra S Rai

Abstract Volcanic ash beds are thin layers commonly observed in the Eagle Ford, Niobrara and, Vaca Muerta formations. Because of their differences in composition, sedimentary structures, and diagenetic alteration, they exhibit a significant contrast in mechanical properties with respect to surrounding formation layers. This can impact hydraulic fracturing, affecting fracture propagation and fracture geometry. Quantifying the mechanical properties of ash beds becomes significant; however, it is a challenge with traditional testing methods. Common logging fails to identify the ash beds, and core plug testing is not possible because of their friability. In this study, nanoindentation was used to measure the mechanical properties (Young's modulus, creep, and anisotropy) in Eagle Ford ash beds, and to determine the contrast with the formation matrix properties. Two separate ash beds of high clay and plagioclase composition were epoxied in an aluminum tray and left for 48 hours curing time. Horizontal and vertical samples of ash beds were acquired and mounted on a metal stub, followed by polishing and broad beam ion milling. Adjacent samples were also prepared for high-resolution Scanning Electron Microscope (SEM) microstructural analysis. The Young's modulus in ash beds ranged from 12 to 24 GPa, with the horizontal direction Young's modulus being slightly greater than that of the vertical samples. The Young's modulus contrast with adjacent layers was calculated to be 1:2 with clay-rich zones and 1:4 with calcite rich zones. The creep deformation rate was three times higher for ash beds compared to other zones. Using Backus averaging, it was determined that the presence of ash beds can increase the anisotropy in the formation by 15-25%. SEM results showed a variation in microstructure between the ash beds with evidence of diagenetic conversion of rhyolitic material into clays. Key differences between the two ash beds were due to the presence of plagioclase and the occurrence of porosity within kaolinite. Overall porosity varied between the two ash beds and adjacent carbonate layers showing a significant increase in porosity. Understanding the moduli contrast between adjacent layers can improve the hydraulic fracturing design when ash beds are encountered. In addition, the presence of these beds can lead to proppant embedment and loss in fracture connectivity. These results can be used for improving geomechanical models.


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