Synthesis and characterization of self-assembled three-dimensional flower-like iron(iii) oxide–indium(iii) oxide binary nanocomposites

RSC Advances ◽  
2015 ◽  
Vol 5 (48) ◽  
pp. 38093-38099 ◽  
Author(s):  
Zongqi Li ◽  
Hua-Feng Fei ◽  
Yongxia Tan ◽  
Xuezhong Zhang ◽  
Zemin Xie ◽  
...  
Keyword(s):  
Metal Oxide ◽  
Thermal Resistance ◽  
Silicone Rubber ◽  
Three Dimensional ◽  
Synthesis And Characterization ◽  
Binary Metal ◽  
Binary Metal Oxide ◽  
Self Assembled

Three-dimensional flower-like iron(iii) oxide–indium(iii) oxide binary metal oxide nanocomposites were successfully fabricated by a simple and economical route; and it can be used as fillers to significantly enhance the thermal resistance of silicone rubber under nitrogen.

Synthesis and characterization of a multifunctional nanocatalyst based on a novel type of binary-metal-oxide-coated Fe3O4–Au nanoparticle

RSC Advances ◽  
2016 ◽  
Vol 6 (22) ◽  
pp. 18685-18694 ◽  
Author(s):  
Hongxing Zhang ◽  
Yiwei Zhang ◽  
Yuming Zhou ◽  
Chao Zhang ◽  
Qianli Wang ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Metal Oxide ◽  
Mixed Oxide ◽  
Synthesis Method ◽  
Au Nanoparticle ◽  
Synthesis And Characterization ◽  
Au Nps ◽  
Binary Metal ◽  
Binary Metal Oxide

A novel type of binary-metal-oxide-coated Au nanocatalyst, including a mixed oxide layer, a moveable magnetic Fe3O4 core and some Au NPs of 2–5 nm, has been synthesized successfully by a facile hydrothermal synthesis method.

scholarly journals Synthesis and Characterization of a Bioconjugate Based on Oleic Acid and L-Cysteine

Polymers ◽  
2021 ◽  
Vol 13 (11) ◽  
pp. 1791
Author(s):  
Marco Vizcarra-Pacheco ◽  
María Ley-Flores ◽  
Ana Mizrahim Matrecitos-Burruel ◽  
Ricardo López-Esparza ◽  
Daniel Fernández-Quiroz ◽  
...  
Keyword(s):  
Oleic Acid ◽  
Materials Science ◽  
Critical Micellar Concentration ◽  
Synthesis And Characterization ◽  
New Materials ◽  
Visible Spectroscopy ◽  
Amide Bonds ◽  
Transmission Electron ◽  
Self Assembled

One of the main challenges facing materials science today is the synthesis of new biodegradable and biocompatible materials capable of improving existing ones. This work focused on the synthesis of new biomaterials from the bioconjugation of oleic acid with L-cysteine using carbodiimide. The resulting reaction leads to amide bonds between the carboxylic acid of oleic acid and the primary amine of L-cysteine. The formation of the bioconjugate was corroborated by Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy, and nuclear magnetic resonance (NMR). In these techniques, the development of new materials with marked differences with the precursors was confirmed. Furthermore, NMR has elucidated a surfactant structure, with a hydrophilic part and a hydrophobic section. Ultraviolet-visible spectroscopy (UV-Vis) was used to determine the critical micellar concentration (CMC) of the bioconjugate. Subsequently, light diffraction (DLS) was used to analyze the size of the resulting self-assembled structures. Finally, transmission electron microscopy (TEM) was obtained, where the shape and size of the self-assembled structures were appreciated.

scholarly journals Synthesis and Characterization of Ligand‐Linked Pt Nanoparticles: Tunable, Three‐Dimensional, Porous Networks for Catalytic Hydrogen Sensing

ChemistryOpen ◽  
2021 ◽  
Vol 10 (7) ◽  
pp. 697-712
Author(s):  
Daniel Loof ◽  
Oliver Thüringer ◽  
Marco Schowalter ◽  
Christoph Mahr ◽  
Anmona Shabnam Pranti ◽  
...  
Keyword(s):  
Three Dimensional ◽  
Pt Nanoparticles ◽  
Synthesis And Characterization ◽  
Hydrogen Sensing ◽  
Porous Networks ◽  
Catalytic Hydrogen

Synthesis and characterization of hydrophobic long-chain fatty acylated cellulose and its self-assembled nanoparticles

2012 ◽  
Vol 69 (4) ◽  
pp. 389-403 ◽  
Author(s):  
Yanzhu Guo ◽  
Xiaohui Wang ◽  
Dong Li ◽  
Hong Du ◽  
Xiaoying Wang ◽  
...  
Keyword(s):  
Synthesis And Characterization ◽  
Self Assembled ◽  
Long Chain

scholarly journals Synthesis and Characterization of Mixed Metal Oxide Nanocomposite Energetic Materials

2003 ◽  
Vol 800 ◽  
Author(s):  
Brady J. Clapsaddle ◽  
Lihua Zhao ◽  
Alex E. Gash ◽  
Joe H. Satcher ◽  
Kenneth J. Shea ◽  
...  
Keyword(s):  
Mass Transport ◽  
Metal Oxide ◽  
Energetic Materials ◽  
Silicon Oxide ◽  
Sol Gel ◽  
Synthesis And Characterization ◽  
Mixed Metal Oxide ◽  
Organic Additives ◽  
Metal Oxide Silicon

ABSTRACTIn the field of composite energetic materials, properties such as ingredient distribution, particle size, and morphology, affect both sensitivity and performance. Since the reaction kinetics of composite energetic materials are typically controlled by the mass transport rates between reactants, one would anticipate new and potentially exceptional performance from energetic nanocomposites. We have developed a new method of making nanostructured energetic materials, specifically explosives, propellants, and pyrotechnics, using sol-gel chemistry. A novel sol-gel approach has proven successful in preparing metal oxide/silicon oxide nanocomposites in which the metal oxide is the major component. Two of the metal oxides are tungsten trioxide and iron(III) oxide, both of which are of interest in the field of energetic materials. Furthermore, due to the large availability of organically functionalized silanes, the silicon oxide phase can be used as a unique way of introducing organic additives into the bulk metal oxide materials. As a result, the desired organic functionality is well dispersed throughout the composite material on the nanoscale. By introducing a fuel metal into the metal oxide/silicon oxide matrix, energetic materials based on thermite reactions can be fabricated. The resulting nanoscale distribution of all the ingredients displays energetic properties not seen in its microscale counterparts due to the expected increase of mass transport rates between the reactants. The synthesis and characterization of these metal oxide/silicon oxide nanocomposites and their performance as energetic materials will be discussed.

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