scholarly journals One-pot reductive amination of aldehydes with nitroarenes over an Au/Al2O3 catalyst in a continuous flow reactor

2015 ◽  
Vol 5 (10) ◽  
pp. 4741-4745 ◽  
Author(s):  
E. A. Artiukha ◽  
A. L. Nuzhdin ◽  
G. A. Bukhtiyarova ◽  
S. Yu. Zaytsev ◽  
P. E. Plyusnin ◽  
...  

Various secondary aromatic amines were synthesized by Au/Al2O3-catalyzed one-pot reductive amination of aldehydes with nitroarenes in a flow reactor.

RSC Advances ◽  
2017 ◽  
Vol 7 (72) ◽  
pp. 45856-45861 ◽  
Author(s):  
Ekaterina A. Artiukha ◽  
Alexey L. Nuzhdin ◽  
Galina A. Bukhtiyarova ◽  
Valerii I. Bukhtiyarov

The reaction of aldehydes with nitroarenes over Ag/Al2O3 catalyst under H2 in a flow reactor gives secondary amines in high yield.


2019 ◽  
Vol 64 (1) ◽  
pp. 1-8
Author(s):  
Balázs Szabó ◽  
Kiara Szakter ◽  
Angelika Thurner ◽  
Ferenc Faigl ◽  
János Éles ◽  
...  

A novel method for synthesis of tricyclic benzimidazole derivatives by using continuous flow reactor is reported. Disadvantages of the well-known batch methods have been avoided utilizing the flow chemistry technology. Beside the one pot reductive cyclization using H-Cube Pro®, the dehydration step was also optimized producing the desired lactam compounds. Then the acylation was optimized under microwave conditions and that reaction was also integrated into the flow system using an Asia heater module. This acylation dramatically reduced the reaction time under continuous-flow conditions, with a residence time of 30 min.


2018 ◽  
Vol 69 (6) ◽  
pp. 1363-1366 ◽  
Author(s):  
Stefania Daniela Bran ◽  
Petre Chipurici ◽  
Mariana Bran ◽  
Alexandru Vlaicu

This paper has aimed at evaluating the concentration of bioethanol obtained using sunflower stem as natural support, molasses as carbon source and Saccharomyces cerevisiae yeast in a continuous flow reactor. The natural support was tested to investigate the immobilization/growth of S. cerevisiae yeast. The concentration of bioethanol produced by fermentation was analyzed by gas chromatography using two methods: aqueous solutions and extraction in organic phase. The CO2 flow obtained during the fermentation process was considered to estimate when the yeast was deactivated. The laboratory experiments have highlighted that the use of plant-based wastes to bioconversion in ethanol could be a non-pollutant and sustainable alternative.


2020 ◽  
Vol 8 (35) ◽  
pp. 13195-13205 ◽  
Author(s):  
Swathi Mukundan ◽  
Daria Boffito ◽  
Abhijit Shrotri ◽  
Luqman Atanda ◽  
Jorge Beltramini ◽  
...  

2019 ◽  
Vol 18 (2) ◽  
pp. 314-318 ◽  
Author(s):  
Martin Dilla ◽  
Ahmet E. Becerikli ◽  
Alina Jakubowski ◽  
Robert Schlögl ◽  
Simon Ristig

Newly developed tubular reactor geometry allows intensive gas–solid interaction in photocatalytic gas-phase CO2 reduction.


2017 ◽  
Vol 115 (3) ◽  
pp. 606-616 ◽  
Author(s):  
Stephanie A. Parker ◽  
Linus Amarikwa ◽  
Kevin Vehar ◽  
Raquel Orozco ◽  
Scott Godfrey ◽  
...  

2006 ◽  
Vol 691 (24-25) ◽  
pp. 5197-5203 ◽  
Author(s):  
Zenon Lysenko ◽  
Bob R. Maughon ◽  
Tezi Mokhtar-Zadeh ◽  
Michael L. Tulchinsky

Sign in / Sign up

Export Citation Format

Share Document