α-MoO3 nanoparticles: solution combustion synthesis, photocatalytic and electrochemical properties

RSC Advances ◽  
2014 ◽  
Vol 4 (100) ◽  
pp. 56784-56790 ◽  
Author(s):  
G. P. Nagabhushana ◽  
D. Samrat ◽  
G. T. Chandrappa

Nanoparticles of ultra-porous MoO3 were synthesized in a single step by a solution combustion reaction using molybdenum metal powder for the first time as a precursor.

2009 ◽  
Vol 24 (1) ◽  
pp. 245-252 ◽  
Author(s):  
Robert Ianoş

Single-phase nanocrystalline 4CaO·Al2O3·Fe2O3 powders were prepared directly from the combustion reaction using a new cost-effective, time-saving, and environmentally friendly version of solution combustion synthesis. Instead of a single fuel, a fuel mixture of urea and β-alanine was used. It was shown by x-ray diffraction, energy-dispersive x-ray analysis, thermogravimetric analysis, and optical microscopy that this new version of the solution combustion synthesis allows the maximization of the exothermic effect associated with the combustion reaction. On the other hand, it was shown that the traditional version of combustion synthesis involving the use of a single fuel, such as urea or β-alanine, does not ensure the formation of Ca4Al2Fe2O10 unless subsequent thermal treatments are applied. It was suggested that the occurrence of combustion reactions cannot be regarded only in terms of adiabatic temperature, as the kinetic aspects overrule the thermodynamic ones.


2020 ◽  
Vol 38 (9) ◽  
pp. 976-982
Author(s):  
Redouan El Khalfaouy ◽  
Servet Turan ◽  
Miguel A. Rodriguez ◽  
Kamil Burak Dermenci ◽  
Umut Savacı ◽  
...  

RSC Advances ◽  
2015 ◽  
Vol 5 (89) ◽  
pp. 73315-73322 ◽  
Author(s):  
Cheng-Gong Han ◽  
Chunyu Zhu ◽  
Genki Saito ◽  
Tomohiro Akiyama

A series of LiBixLaxMn2−2xO4 (x = 0, 0.002, 0.005, 0.010, 0.020) samples were synthesized by solution combustion synthesis in combination with calcination.


2010 ◽  
Vol 1278 ◽  
Author(s):  
V. R. Orante-Barrón ◽  
C. Cruz-Vázquez ◽  
R. Bernal ◽  
G. Denis ◽  
E. G. Yukihara

AbstractThermoluminescence (TL) of La2O3 is reported for the first time. Novel La2O3 phosphor was obtained by solution combustion synthesis (SCS) in which a redox combustion process between lanthanum nitrate and urea at 500 °C is accomplished. The powder samples obtained were annealed at 900 °C during 2 h in air. X-Ray Diffraction (XRD) results showed the hexagonal phase of La2O3 for annealed powder samples. The TL glow curve obtained after exposure to beta radiation of these samples, displayed two maxima located at ˜ 101 °C and ˜ 200 °C, and a shoulder at ˜ 247 °C. Results from experiments such as dose response and fading showed that annealed La2O3 powder obtained by SCS is a promising material for radiation dosimetry applications.


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