Synthesis of perovskite-type manganites Yb1−xDyxMnO3 (0.1 ≤ x ≤ 0.5) via solid-state reaction and high-pressure flux methods followed by structural characterization and magnetic property studies

2015 ◽  
Vol 39 (4) ◽  
pp. 2596-2601 ◽  
Author(s):  
Yingnan Zhang ◽  
Fuyang Liu ◽  
Tong Zheng ◽  
Ziqing Zhang ◽  
Wei Liu ◽  
...  
Keyword(s):  
High Pressure ◽  
Magnetic Property ◽  
Solid State ◽  
Single Crystal ◽  
Structural Characterization ◽  
Solid State Reaction ◽  
Structural Difference ◽  
Paramagnetic Property ◽  
Perovskite Type

h-Yb1−xDyxMnO3 (0.1 ≤ x ≤ 0.5) and single crystal o-Yb0.5Dy0.5MnO3 were firstly synthesized, and o-Yb0.5Dy0.5MnO3 has the paramagnetic property due to slight structural difference.

Solid-state reaction of niobium with diamond carbon at high pressure and high temperature to form superconducting composite

2021 ◽  
Vol 31 (3) ◽  
pp. 415-418
Author(s):  
Vladimir Yu. Osipov ◽  
Fedor M. Shakhov ◽  
Nikolai M. Romanov ◽  
Kazuyuki Takai
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Solid State ◽  
Solid State Reaction

Synthesis and structural characterization of a magnesium phthalocyanine(3–) anion

2012 ◽  
Vol 16 (01) ◽  
pp. 154-162 ◽  
Author(s):  
Edwin W.Y. Wong ◽  
Daniel B. Leznoff
Keyword(s):  
Absorption Spectrum ◽  
Solid State ◽  
Single Crystal ◽  
Structural Characterization ◽  
Heterometallic Complex ◽  
State Structure ◽  
Solid State Structure ◽  
X Ray ◽  
X Ray Crystallography

The reduction of magnesium phthalocyanine (MgPc) with 2.2 equivalents of potassium graphite in 1,2-dimethoxyethane (DME) gives [K2(DME)4]PcMg(OH)(1) in 67% yield. Compound 1 was structurally characterized using single crystal X-ray crystallography and was found to be a monomeric, heterometallic complex consisting of a μ3-OH ligand that bridges a [MgIIPc3-]- anion to two potassium cations solvated by four DME molecules. An absorption spectrum of 1 confirms the Pc ligand is singly reduced and has a 3–charge. The solid-state structure of 1 does not indicate breaking of the aromaticity of the Pc ligand. Compound 1 is only the second Pc3- complex and the first reduced MgPc to be isolated and structurally characterized.

Large-scale synthesis of single-crystal alpha manganese sesquioxide nanowires via solid-state reaction

2009 ◽  
Vol 63 (8) ◽  
pp. 661-663 ◽  
Author(s):  
Yong Ren ◽  
Qingfang Liu ◽  
Jianbo Wang ◽  
Haibo Wang ◽  
Desheng Xue
Keyword(s):  
Solid State ◽  
Single Crystal ◽  
Solid State Reaction ◽  
Large Scale ◽  
Large Scale Synthesis

Single Crystal Formation by Solid-State Reaction Between p-Benzoquinone and 2,4,5-Trichlorophenol

2002 ◽  
Vol 55 (4) ◽  
pp. 271 ◽  
Author(s):  
N. B. Singh ◽  
A. Pathak ◽  
R. Fröhlich
Keyword(s):  
Hydrogen Bond ◽  
Solid State ◽  
Single Crystal ◽  
Single Crystals ◽  
Solid State Reaction ◽  
Carbonyl Oxygen ◽  
Crystal Formation ◽  
X Ray Diffraction ◽  
X Ray

Vapours of p-benzoquinone (BQ) have been found to react with solid 2,4,5-trichlorophenol (TCP). The reaction product (BQ-TCP) separated in the form of monoclinic single crystals, the structure of which was determined by X-ray diffraction to reveal that the two molecules are linked by a single hydrogen bond between the carbonyl oxygen of BQ and the phenolic hydrogen of TCP.

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