One-pot synthesis of ordered mesoporous transition metal–zirconium oxophosphate composites with excellent textural and catalytic properties

2015 ◽  
Vol 39 (2) ◽  
pp. 1322-1329 ◽  
Author(s):  
Zhichao Miao ◽  
Huahua Zhao ◽  
Jian Yang ◽  
Jun Zhao ◽  
Huanling Song ◽  
...  

A series of ordered M–X–ZrPO materials were successfully synthesized via a facile and general one-pot evaporation-induced self-assembly (EISA) strategy.

2021 ◽  
Author(s):  
Xiaoqi Wang ◽  
Xiaoning Liu ◽  
Richard Lee Smith ◽  
Yining Liang ◽  
Xinhua Qi

This work reports one-pot synthesis of metal-linked OMCs, using lignin from agricultural waste sources as a sole carbon precursor, through coordinated interactions between lignin functional groups and metal ligands with classical solvent evaporation induced self-assembly.


RSC Advances ◽  
2015 ◽  
Vol 5 (61) ◽  
pp. 49287-49294 ◽  
Author(s):  
Kwan Wee Tan ◽  
Hiroaki Sai ◽  
Spencer W. Robbins ◽  
Jörg G. Werner ◽  
Tobias N. Hoheisel ◽  
...  

One-pot synthesis of periodically mesostructured γ-alumina using an ABC triblock terpolymer as structure-directing agent and in situ derived rigid carbon scaffold.


2018 ◽  
Vol 5 (1) ◽  
pp. 59-66 ◽  
Author(s):  
Svetlana Pavlova ◽  
Yuliya Fedorova ◽  
Arkadii Ishchenko ◽  
Maxim Melgunov ◽  
Elena Melgunova ◽  
...  

Abstract The ordered mesoporous Mg- and Ni-Mg-alumina samples of general formula xwt%Mg-Al2O3 and ywt%Nixwt% Mg-Al2O3(x, y = 5, 10 % wt) have been prepared by the one-pot evaporation induced self-assembly (EISA) method using Pluronic P123 as a template. The textural and structural properties of the prepared samples have been characterized by N2adsorption-desorption analysis, BET, XRD, TEM with EDX, HAADF-STEM, and H2-TPR. The samples calcined at 700°C had an ordered mesoporous structure with a SSA of 170-250 m2/g, a pore volume of 0.5-0.64 cm3/g and a narrow distribution of the pore size (mean 12-16 nm). For the catalysts prepared by the one-pot EISA method, the size of the metal Ni particles was in the range of 3-12 nm and was conditioned by their confinement in the mesopores and the interaction with MgO and Al2O3. Testing in methane dry reforming in the 15v.% CH4+ 15v.%CO2feed, with He balance, at 650-750°C and the contact time of 0.015 s has shown the higher activity and stability of the ordered mesoporous 10w%Ni- 10w%Mg-Al2O3catalysts prepared by the one-pot method as compared with the catalyst of the same composition obtained by impregnation.


2021 ◽  
Vol 23 (4) ◽  
pp. 1861-1870
Author(s):  
Yiwei Tang ◽  
Mo Qiu ◽  
Jirui Yang ◽  
Feng Shen ◽  
Xiaoqi Wang ◽  
...  

Ni-Doped OMC with high catalytic activity and stability for furfural hydrogenation to furfuryl alcohol was prepared by a one-pot evaporation-induced self-assembly process with biomass-derived gallic acid as carbon precursor and Ni2+ as crosslinker.


2017 ◽  
Vol 5 (30) ◽  
pp. 7465-7471 ◽  
Author(s):  
Wei Song ◽  
Maoqiang Chi ◽  
Mu Gao ◽  
Bing Zhao ◽  
Ce Wang ◽  
...  

We describe a self-assembly directed method that allows the one-pot synthesis of Au/polyaniline nanorices with enhanced peroxidase-like activity.


2011 ◽  
Vol 115 (26) ◽  
pp. 12873-12882 ◽  
Author(s):  
Shiyou Hao ◽  
Hong Chang ◽  
Qiang Xiao ◽  
Yijun Zhong ◽  
Weidong Zhu

ChemInform ◽  
2014 ◽  
Vol 45 (13) ◽  
pp. no-no
Author(s):  
T. A. Jenifer Vijay ◽  
Kebbahalli N. Nandeesh ◽  
Goravanahalli M. Raghavendra ◽  
Kanchugarakoppal S. Rangappa ◽  
Kempegowda Mantelingu

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