Development and characterization of custom-engineered and compacted nanoparticles as calibration materials for quantification using LA-ICP-MS

2014 ◽  
Vol 29 (6) ◽  
pp. 955-962 ◽  
Author(s):  
Daniel Tabersky ◽  
Norman A. Luechinger ◽  
Michael Rossier ◽  
Eric Reusser ◽  
Kathrin Hametner ◽  
...  
Keyword(s):  
Flame Spray ◽  
Icp Ms ◽  
Nano Material ◽  
Flame Spray Synthesis ◽  
Calibration Materials

Flame spray synthesis was used to produce a reference nano-material with a customized composition for use in LA-ICP-MS.

Characterization of calibration materials for trace element analysis and fingerprint studies of gold using LA-ICP-MS

2009 ◽  
Vol 24 (4) ◽  
pp. 476 ◽  
Author(s):  
Robert Kovacs ◽  
Sandra Schlosser ◽  
Samuel Philipp Staub ◽  
Alexander Schmiderer ◽  
Ernst Pernicka ◽  
...  
Keyword(s):  
Trace Element ◽  
Trace Element Analysis ◽  
Element Analysis ◽  
Icp Ms ◽  
Calibration Materials

Characterization of Different Types of Biomass Wastes Using Thermogravimetric and ICP-MS Analyses

2020 ◽  
Vol 70 (12) ◽  
pp. 4594-4600
Keyword(s):  
Thermogravimetric Analysis ◽  
Food Industry ◽  
Wood Waste ◽  
Biomass Ash ◽  
Minor Elements ◽  
Ms Analysis ◽  
Icp Ms ◽  
Different Types

The purpose of this study was to characterize some types of biomass wastes resulted from different activities such as: agriculture, forestry and food industry using thermogravimetric and ICP-MS analyses. Also, it was optimized an ICP-MS method for the determination of As, Cd and Pb from biomass ash samples. The ICP-MS analysis revealed that the highest concentration of metals (As, Cd, Pb) was recorded in the wood waste ash sample, also the thermogravimetric analysis indicated that the highest amount of ash was obtained for the same sample (26.82%). The biomass wastes mentioned in this study are alternative recyclable materials, reusable as pellets and briquettes. Keywords: ash, biomass, ICP-MS, minor elements, TG

Comparative study on the homogeneity of polymeric calibration materials using LA-ICP-MS

2008 ◽  
Vol 23 (7) ◽  
pp. 1038 ◽  
Author(s):  
Christoph Simons ◽  
Stephanie Hanning ◽  
Anne Wegner ◽  
Christian Mans ◽  
Anton Janßen ◽  
...  
Keyword(s):  
Comparative Study ◽  
Icp Ms ◽  
Calibration Materials

Matrix effects using an ICP-MS with a single positive ion lens and grounded stop: analyte mass dependent?

2017 ◽  
Vol 32 (5) ◽  
pp. 951-966 ◽  
Author(s):  
John W. Olesik ◽  
Shi Jiao
Keyword(s):  
Gas Flow ◽  
Matrix Effects ◽  
Mass Matrix ◽  
Gas Flow Rate ◽  
Icp Ms ◽  
Single Positive ◽  
Mass Dependent ◽  
Positive Ion ◽  
Comprehensive Characterization

Comprehensive characterization of ICP-MS matrix effects as a function of analyte mass, matrix mass, lens voltage and nebulizer gas flow rate was carried out.

Photocatalytic Activity of W-Doped TiO2 Nanopowders

2008 ◽  
Vol 11 (1) ◽  
Author(s):  
Katarzyna A. Michalow ◽  
Andri Vital ◽  
Andre Heel ◽  
Thomas Graule ◽  
Felix A. Reifler ◽  
...  
Keyword(s):  
Titanium Dioxide ◽  
Photocatalytic Activity ◽  
Specific Surface ◽  
Dopant Concentration ◽  
Flame Spray ◽  
Titanium Tetra Isopropoxide ◽  
Flame Spray Synthesis ◽  
One Step ◽  
Tio2 Nanopowders ◽  
Doped Titanium Dioxide

AbstractPolycrystalline tungsten-doped titanium dioxide nanopowders within a dopant concentration of 0-1 at.% were prepared by a one-step flame spray synthesis (FSS). Mixtures of titanium tetra-isopropoxide dissolved in ethanol and tungsten hexacarbonyl solubilized in tetrahydrofuran were used as precursors. The specific surface area (SSA) of the powders was between 40 and 130 m

Optimization and Characterization of Biogenic Silver Nanoparticles Synthesized by Leaves Extract of Alphonsea Madraspatana

2021 ◽  
Vol 17 ◽  
Author(s):  
Amita Sahu ◽  
Sudhanshu Shekhar Swain ◽  
Goutam Ghosh ◽  
Deepak Pradhan ◽  
Dipak Kumar Sahu ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Volume Ratio ◽  
Xrd Analysis ◽  
Biofilm Inhibition ◽  
Nano Silver ◽  
E Coli ◽  
Biogenic Silver Nanoparticles ◽  
Icp Ms ◽  
Anti Oxidant

Background: Literature evidences as well as traditional uses of genus Alphonsea reveal significant antimicrobial and anti-oxidant activity, which encourages to consider A. madraspatana to have potent antimicrobials, there by offering potential adjuncts to synthesize improved antimicrobial Silver nanoparticles (AgNPs). The objective of the present exposition is to optimize reaction parameters to synthesize antimicrobial Biogenic Silver nanoparticles (BAgNPs) from extract of A. madraspatana leaves (AML) and to evaluate the effect against bacteria. Methods: BAgNPs was synthesized by optimized reaction. The Synthesized nanoparticles were characterized by UV, IR, ICP-MS and XRD analysis. The antibacterial potency of optimized BAgNPs was evaluated against E. coli by comparing with positive controls. Results: Results of optimization process indicate nanoscale BAgNPs were produced at operating temp. of 45°C for 120 min at pH 8 with 1:5 volume ratio of AgNO3 and extract. Optimized BAgNPs exhibits relatively higher antimicrobial activity (31±1mm) compared to Ciprofloxacin (27±1mm) and marketed nano silver (28± 2 mm). The developed BAgNPs shows comparable biofilm inhibition (86.50%) as compared to marketed nano silver (88.10%) and Ciprofloxacin (83.10%). Conclusion: Experimental evidence suggests methanolic extract of AML under predefined conditions successfully generate nano-template of silver with better antibacterial response against E. coli.

scholarly journals AF4-UV-MALS-ICP-MS/MS, spICP-MS, and STEM-EDX for the Characterization of Metal-Containing Nanoparticles in Gas Condensates from Petroleum Hydrocarbon Samples

2018 ◽  
Vol 91 (1) ◽  
pp. 1164-1170 ◽  
Author(s):  
Daniel Ruhland ◽  
Kenneth Nwoko ◽  
Magali Perez ◽  
Jörg Feldmann ◽  
Eva M. Krupp
Keyword(s):  
Petroleum Hydrocarbon ◽  
Gas Condensates ◽  
Icp Ms

Geochemical Characterization of Lapita Pottery Via Inductively Coupled Plasma-mass Spectrometry (ICP-MS)

Archaeometry ◽  
2004 ◽  
Vol 46 (1) ◽  
pp. 35-46 ◽  
Author(s):  
D. J. Kennett ◽  
A. J. Anderson ◽  
M. J. Cruz ◽  
G. R. Clark ◽  
G. R. Summerhayes
Keyword(s):  
Mass Spectrometry ◽  
Inductively Coupled Plasma ◽  
Geochemical Characterization ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Plasma Mass Spectrometry
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