Fine tunable aqueous solution synthesis of textured flexible SnS2 thin films and nanosheets

2015 ◽  
Vol 17 (14) ◽  
pp. 9282-9287 ◽  
Author(s):  
Peter Nørby ◽  
Simon Johnsen ◽  
Bo Brummerstedt Iversen

We present an environmentally benign aqueous synthesis method to obtain fine tunable layered SnS2 thin films as well as methods to obtain freestanding nanosheets or transfer to flexible substrates.

RSC Advances ◽  
2015 ◽  
Vol 5 (108) ◽  
pp. 88950-88957 ◽  
Author(s):  
Xiaoqing Yu ◽  
Kaiqi Li ◽  
Haihui Zhou ◽  
Shudan Wei ◽  
Changjun Zhang ◽  
...  

A modified Hummers method and an aqueous solution synthesis method have been adopted to prepare curly graphene nanosheets/manganese oxide (CGN/MnO2) composite using multiwalled carbon nanotubes and KMnO4 as precursors in this paper.


2020 ◽  
Vol 17 (8) ◽  
pp. 628-630
Author(s):  
Vu Binh Duong ◽  
Pham Van Hien ◽  
Tran Thai Ngoc ◽  
Phan Dinh Chau ◽  
Tran Khac Vu

A simple and practical method for the synthesis on a large scale of altretamine (1), a wellknown antitumor drug, has been successfully developed. The synthesis method involves the conversion of cyanuric chloride (2) into altretamine (1) by dimethylamination of 2 with an aqueous solution of 40% dimethylamine and potassium hydroxide in 1, -dioxan 4in one step to give altretamine (1) in high yield.


2018 ◽  
Vol 6 (1) ◽  
pp. 22-30
Author(s):  
C. Lalhriatpuia ◽  
◽  
Thanhming liana ◽  
K. Vanlaldinpuia

The photocatalytic activity of Nanopillars-TiO2 thin films was assessed in the degradation of Bromophenol blue (BPB) dye from aqueous solution under batch reactor operations. The thin films were characterized by the XRD, SEM and AFM analytical methods. BET specific surface area and pore sizes were also obtained. The XRD data showed anatase phase of TiO2 particles with average particle size of 25.4 and 21.9 nm, for S1 and S2 catalysts respectively. The SEM and AFM images indicated the catalyst composed with Nanosized pillars of TiO2, evenly distributed on the surface of the substrate. The average height of the pillars was found to be 180 and 40 nm respectively for the S1 and S2 catalyst. The BET specific surface area and pore sizes of S1 and S2 catalyst were found to be 5.217 and 1.420 m2/g and 7.77 and 4.16 nm respectively. The photocatalytic degradation of BPB using the UV light was studied at wide range of physico-chemical parametric studies to determine the mechanism of degradation as well as the practical applicability of the technique. The batch reactor operations were conducted at varied pH (pH 4.0 to 10.0), BPB initial concentration (1.0 to 20.0 mg/L) and presence of several interfering ions, i.e., cadmium nitrate, copper sulfate, zinc chloride, sodium chloride, sodium nitrate, sodium nitrite, glycine, oxalic acid and EDTA in the photocatalytic degradation of BPB. The maximum percent removal of BPB was observed at pH 6.0 and a low initial concentration of the pollutant highly favours the photocatalytic degradation using thin films. The presence of several interfering ions suppressed the photocatalytic activity of thin films to some extent. The time dependence photocatalytic degradation of BPB was demonstrated with the pseudo-first-order rate kinetics. Study was further extended with total organic carbon measurement using the TOC (Total Organic Carbon) analysis. This demonstrated an apparent mineralization of BPB from aqueous solutions.


Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 724
Author(s):  
Tong Li ◽  
Masaya Ichimura

Magnesium hydroxide (Mg(OH)2) thin films were deposited by the drop-dry deposition (DDD) method using an aqueous solution containing Mg(NO3)2 and NaOH. DDD was performed by dropping the solution on a substrate, heating-drying, and rinsing in water. Effects of different deposition conditions on the surface morphology and optical properties of Mg(OH)2 thin films were researched. Films with a thickness of 1−2 μm were successfully deposited, and the Raman peaks of Mg(OH)2 were observed for them. Their transmittance in the visible range was 95% or more, and the bandgap was about 5.8 eV. It was found that the thin films have resistivity of the order of 105 Ωcm. Thus, the transparent and semiconducting Mg(OH)2 thin films were successfully prepared by DDD.


2021 ◽  
pp. 1-1
Author(s):  
C. M. Madrid Aguilar ◽  
A. V. Svalov ◽  
A. A. Kharlamova ◽  
E. E. Shalygina ◽  
A. Larranaga ◽  
...  

2017 ◽  
Vol 1 (7) ◽  
Author(s):  
Irene Lucas ◽  
Pilar Jiménez-Cavero ◽  
J. M. Vila-Fungueiriño ◽  
Cesar Magén ◽  
Soraya Sangiao ◽  
...  

2016 ◽  
Vol 45 (43) ◽  
pp. 17312-17318 ◽  
Author(s):  
Eun-Kyung Kim ◽  
Dasom Park ◽  
Nabeen K. Shrestha ◽  
Jinho Chang ◽  
Cheol-Woo Yi ◽  
...  

An aqueous solution based synthetic method for binder-free Ag2Te thin films using ion exchange induced chemical transformation of Ag/AgxO thin films.


1999 ◽  
Vol 19 (6-7) ◽  
pp. 1409-1412 ◽  
Author(s):  
S.M Zanetti ◽  
E.R Leite ◽  
E Longo ◽  
J.A Varela

Nano Letters ◽  
2014 ◽  
Vol 14 (11) ◽  
pp. 6547-6553 ◽  
Author(s):  
Zhaoyang Lin ◽  
Yu Chen ◽  
Anxiang Yin ◽  
Qiyuan He ◽  
Xiaoqing Huang ◽  
...  

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