Evaluation of organochlorine pesticides in soil using ultrasound-assisted liquid phase microextraction

2015 ◽  
Vol 7 (4) ◽  
pp. 1366-1371 ◽  
Author(s):  
Wenting Zhao ◽  
Tong Wu ◽  
Jindong Li ◽  
Runhua Lu ◽  
Peng Wang ◽  
...  

Procedure used for ultrasound-assisted liquid phase microextraction (USA-LPME).

2013 ◽  
Vol 675 ◽  
pp. 260-263 ◽  
Author(s):  
Du Shu Huang ◽  
Ya Shun Chen ◽  
He Ping Yan ◽  
Na Wu ◽  
Wei Liu ◽  
...  

A novel method for determination of organochlorine pesticides residuals (2,4-DDT and 4,4-DDT) in water samples through hollow fiber membrane-liquid phase microextraction using ionic liquid material as extractant coupled with high performance liquid chromatography has been developed. The effect of extraction parameters including pH of the feed solution, stirring rate and extraction time was investigated. The proposed method provided enrichment efficiency of 323 and 289 for 2,4-DDT and 4,4-DDT respectively. The method had good linear range of 0.5-50 μg /L and the limits of detection of the pesticides were 0.1 μg /L.


2013 ◽  
Vol 405 (12) ◽  
pp. 4235-4243 ◽  
Author(s):  
Morteza Moradi ◽  
Yadollah Yamini ◽  
Moslem Tayyebi ◽  
Hamid Asiabi

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