Hollow fiber supported ionic liquid membrane microextraction for speciation of mercury by high-performance liquid chromatography-inductively coupled plasma mass spectrometry

2015 ◽  
Vol 7 (3) ◽  
pp. 1140-1146 ◽  
Author(s):  
Zhenhua Wang ◽  
Qingzhong Xu ◽  
Saiyu Li ◽  
Lingyu Luan ◽  
Jian Li ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Hollow Fiber ◽  
Inductively Coupled Plasma ◽  
High Performance ◽  
Liquid Membrane ◽  
Inorganic Mercury ◽  
High Sensitivity ◽  
Inductively Coupled ◽  
Supported Ionic Liquid ◽  
Plasma Mass Spectrometry

Hollow fiber supported ionic liquid membrane microextraction for the preconcentration of monomethylmercury and inorganic mercury with high sensitivity detection.

scholarly journals Concrete Examination of 100-Year-Old Bridge Structure above the Kłodnica River Flowing through the Agglomeration of Upper Silesia in Gliwice: A Case Study

Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 981
Author(s):  
Barbara Słomka-Słupik ◽  
Jacek Podwórny ◽  
Beata Grynkiewicz-Bylina ◽  
Marek Salamak ◽  
Bibianna Bartoszek ◽  
...  
Keyword(s):  
Inductively Coupled Plasma ◽  
High Performance ◽  
Chloride Content ◽  
Technical Condition ◽  
Inductively Coupled ◽  
Bridge Safety ◽  
Free Chloride ◽  
Management Processes ◽  
Icp Ms ◽  
Plasma Mass Spectrometry

The article analyzes the composition of concrete taken from various elements from a 100-year-old bridge in South Poland, so as to analyze its technical condition. The main methods applied during experimental work were: Designation of pH, free chloride content, salinity, XRD and SEM examinations, as well as metals determination using inductively coupled plasma mass spectrometry (ICP­MS), high-performance liquid chromatography (HPLC)-ICP-MS, and cold-vapor atomic absorption spectroscopy (CV-AAS). The concrete of the bridge was strongly carbonated and decalcified with an extremely high content of chlorides. The pH of the concrete was in a range from 10.5 to 12.0. Acid soluble components were between 9.9% and 17.6%. Typical sulfate corrosion phases of concrete were not detected. Friedels’ salt was found only at the extremity of an arch. The crown block was corroded to the greatest extent. Various heavy metals were absorbed into the concrete, likely from previous centuries, when environmental protection policy was poor. The applied research methodology can be used on bridges exposed to specific external influences. The acquired knowledge can be useful in the management processes of the bridge infrastructure. It can help in making decisions about decommissioning or extending the life cycle of the bridge. This work should also sensitize researchers and decision-makers to the context of “bridge safety”.

Simultaneous speciation of arsenic and mercury in fish by high-performance liquid chromatography inductively coupled plasma mass spectrometry

2021 ◽  
Author(s):  
Yung-Chun Chen ◽  
Shiuh-Jen Jiang
Keyword(s):  
Mass Spectrometry ◽  
Liquid Chromatography ◽  
Inductively Coupled Plasma ◽  
High Performance ◽  
Dynamic Reaction ◽  
Dynamic Reaction Cell ◽  
Reaction Cell ◽  
Inductively Coupled ◽  
Mercury In Fish ◽  
Plasma Mass Spectrometry

Liquid chromatography and dynamic reaction cell inductively coupled plasma mass spectrometry are used in tandem for the simultaneous speciation of arsenic and mercury in fish.

Arsenic compounds in tissues of the leatherback turtle, Dermochelys coriacea

1994 ◽  
Vol 74 (2) ◽  
pp. 463-466 ◽  
Author(s):  
J.S. Edmonds ◽  
Y. Shibata ◽  
R.I.T. Prince ◽  
K.A. Francesconi ◽  
M. Morita
Keyword(s):  
Mass Spectrometry ◽  
Inductively Coupled Plasma ◽  
High Performance ◽  
Pectoral Muscle ◽  
Dermochelys Coriacea ◽  
Aqueous Extracts ◽  
Arsenic Compounds ◽  
Leatherback Turtle ◽  
Inductively Coupled ◽  
Plasma Mass Spectrometry

Examination of extracts of tissues of a leatherback turtle, Dermochelys coriacea (L.) (Reptilia: Dermochelyidae) by high-performance liquid chromatography inductively coupled plasma-mass spectrometry has demonstrated the presence of arsenobetaine, arsenocholine and inorganic arsenate in heart muscle and liver, and arsenobetaine and inorganic arsenate in pectoral muscle. Although arsenobetaine was the major form in all tissues, inorganic arsenate and arsenocholine accounted for 50% and 15% respectively of arsenic in aqueous extracts of the liver.

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