Silica-based surface molecular imprinting for recognition and separation of lysozymes

2014 ◽  
Vol 6 (21) ◽  
pp. 8584-8591 ◽  
Author(s):  
Cenjin Zhang ◽  
Yuzhi Wang ◽  
Yigang Zhou ◽  
Junxia Guo ◽  
Yanjin Liu
Keyword(s):  
Aqueous Solution ◽  
Molecular Imprinting ◽  
Sol Gel ◽  
Inorganic Polymer ◽  
Surface Molecular Imprinting ◽  
Molecularly Imprinted ◽  
Mild Conditions ◽  
Sol Gel Process

A highly selective surface molecularly imprinted inorganic polymer composed of tetraethoxysilane and 3-aminopropyltriethoxysilane has been prepared by a sol–gel process on silica submicroparticles in aqueous solution under simple and mild conditions.

scholarly journals Carbon Quantum Dots Encapsulated Molecularly Imprinted Fluorescence Quenching Particles for Sensitive Detection of Zearalenone in Corn Sample

Toxins ◽  
2018 ◽  
Vol 10 (11) ◽  
pp. 438 ◽  
Author(s):  
Manyu Shao ◽  
Ming Yao ◽  
Sarah De Saeger ◽  
Liping Yan ◽  
Suquan Song
Keyword(s):  
Quantum Dots ◽  
Fluorescence Quenching ◽  
Sol Gel ◽  
Carbon Quantum Dots ◽  
Detection Range ◽  
Molecularly Imprinted ◽  
Relative Standard ◽  
Sol Gel Process ◽  
One Step ◽  
Optimized Conditions

An eco-friendly and efficient one-step approach for the synthesis of carbon quantum dots (CDs) that encapsulated molecularly imprinted fluorescence quenching particles (MIFQP) and their application for the determination of zearalenone (ZEA) in a cereal sample are described in this study. CDs with high luminescence were first synthesized, and then encapsulated in the silica-based matrix through a non-hydrolytic sol-gel process. The resulting ZEA-imprinted particles exhibited not only an excellent specific molecular recognition of ZEA, but also good photostability and obvious template binding-induced fluorescence quenching. Under the optimized conditions, the fluorescence intensity of MIFQP was inversely proportional to the concentration of ZEA. By validation, the detection range of these fluorescence quenching materials for ZEA was between 0.02 and 1.0 mg L−1, and the detection limit was 0.02 mg L−1 (S/N = 3). Finally, the MIFQP sensor was successfully applied for ZEA determination in corn with recoveries from 78% to 105% and the relative standard deviation (RSD %) was lower than 20%, which suggests its potential in actual applications.

Organic–inorganic hybrids having a talc-like structure as suitable hosts to guest a wide range of species

2018 ◽  
Vol 47 (9) ◽  
pp. 2925-2932 ◽  
Author(s):  
J. Brendlé
Keyword(s):  
Hybrid Materials ◽  
Sol Gel ◽  
Step Method ◽  
Mild Conditions ◽  
Condensation Reactions ◽  
Wide Range ◽  
Sol Gel Process ◽  
Hydrolysis And Condensation ◽  
One Step

The sol–gel process involving hydrolysis and condensation reactions is an attractive way to form siloxane based hybrid materials since it is a one-step method performed under mild conditions.

Preparation of a novel molecularly imprinted polymer by the sol–gel process for sensing creatinine

2012 ◽  
Vol 711 ◽  
pp. 83-90 ◽  
Author(s):  
Ta-Jen Li ◽  
Po-Yen Chen ◽  
Po-Chin Nien ◽  
Chia-Yu Lin ◽  
R. Vittal ◽  
...  
Keyword(s):  
Molecularly Imprinted Polymer ◽  
Sol Gel ◽  
Imprinted Polymer ◽  
Molecularly Imprinted ◽  
Sol Gel Process

Preparation of Titanium Hexacyanoferrate Microspheres (Diameter <70 μm) by Water Extraction Variant of Sol-Gel Process and its Application to Sorption of 137Cs from Nuclear Reactor Cooling Water

1995 ◽  
Vol 412 ◽  
Author(s):  
A. Deptula ◽  
A. G. Chmielewski ◽  
W. Lada ◽  
T. Olczak
Keyword(s):  
Aqueous Solution ◽  
Nuclear Reactor ◽  
Sol Gel ◽  
Cooling Water ◽  
Special Procedure ◽  
Sol Gel Process ◽  
High Sorption ◽  
Emulsion Drops ◽  
Titania Sol ◽  
Dta Studies

AbstractTitanium hexacyanoferrate microspheres (diameter <70km) were obtained in the following steps: (1) extraction of chlorides from an aqueous solution of TiCl4 with long chain amine -Primene JMT- in paraffin diluent (the resulting sol has the concentration 320 g TiO2/dm3 and the mole ratio Cl-: Ti4+ = 1.83); (2) blending of titania sol with an aqueous solution of K4 Fe(CN)6. 3H2O (280 g/dm3) in order to obtain final sols with Fe(CN)64-: Ti4+ mole ratio of 0.05 - 0.1; (3) formation of multicomponent sol emulsion in 2-ethylhexanol-1 containing I vol. % of Ethomen S/15 (EH), (4) gelation of emulsion drops by extraction of water with partially dehydrated EH; (5) filtration and washing with acetone; (6) drying at 140°C using a special procedure elaborated on the basis of TG and DTA studies.The final product is insoluble in water and exhibits high sorption efficiency of 137 Cs.

A surface molecularly imprinted electrospun polyethersulfone (PES) fiber mat for selective removal of bilirubin

2017 ◽  
Vol 5 (29) ◽  
pp. 5763-5773 ◽  
Author(s):  
Keke Wu ◽  
Wufeng Yang ◽  
Yanpeng Jiao ◽  
Changren Zhou
Keyword(s):  
Molecular Imprinting ◽  
Selective Removal ◽  
Surface Molecular Imprinting ◽  
Molecularly Imprinted

Electrospinning and surface molecular imprinting were used together to prepare a surface molecularly imprinted electrospun polyethersulfone (PES) fiber mat for selective removal of bilirubin.

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