Structural and spectroscopic properties of Yb3+-doped MgAl2O4 nanocrystalline spinel

2014 ◽  
Vol 43 (21) ◽  
pp. 7752-7759 ◽  
Author(s):  
Rafal J. Wiglusz ◽  
Georges Boulon ◽  
Yannick Guyot ◽  
Malgorzata Guzik ◽  
Dariusz Hreniak ◽  
...  

Pechini's sol–gel method was successfully applied to obtain an Yb3+-doped MgAl2O4 spinel nanopowder. The regularity between the observed structural and spectroscopic measurements was described in detail.

Author(s):  
Massaud Mostafa ◽  
Ziyad Alrowaili ◽  
Gehad Rahwan ◽  
Melad Gerges

Perovskite type (Pb1-1.5x Lax0.5x)TiO3 (PLT) ceramics with x = 0.21, 0.22, 0.23, 0.24, 0.25 were prepared by the sol-gel method. Their structural, optical, and dielectric properties were investigated. The crystallite compounds were obtained by calcinating the mixture of PbCO3, TiO2, and La2O3 at 1000ºC for different time periods. After 4 h annealing, PLT23 sample, no secondary phases have been observed in the XRD spectrum of the PLT sample with 23% La content (PLT23). This sample appears to be notably distinguished in its structural, optical, and dielectric characteristics compared with other samples.


2016 ◽  
Vol 45 (39) ◽  
pp. 15541-15551 ◽  
Author(s):  
Chang Sung Lim ◽  
Aleksandr S. Aleksandrovsky ◽  
Maxim S. Molokeev ◽  
Aleksandr S. Oreshonkov ◽  
Denis A. Ikonnikov ◽  
...  

Triple molybdates NaCaLa(1−x−y)(MoO4)3:xEr3+,yYb3+were synthesized by the microwave sol–gel method.


1998 ◽  
Vol 275-277 ◽  
pp. 420-423 ◽  
Author(s):  
W. Stręk ◽  
P.J. Dereń ◽  
K. Maruszewski ◽  
E. Pawlik ◽  
W. Wojcik ◽  
...  

2021 ◽  
Author(s):  
Touka Dabbebi ◽  
S. Hcini ◽  
B. Alzahrani ◽  
H. Rahmouni ◽  
A. Mallah ◽  
...  

Abstract Polycrystalline Mg0.5Co0.5Fe1.6Al0.4O4 ferrite was prepared with sol-gel method. This sample was characterized by powder X-ray diffraction (XRD), Scanning electron microscopy, and impedance spectroscopy. X-ray diffraction analysis combined with the Rietveld refinement confirmed that the sample crystallizes in a single-phase cubic spinel structure with (SG: \(Fd\stackrel{-}{3}m\)). Electrical conductivity obeying the Jonscher power law indicates that the prepared material exhibits semiconductor behavior, and the conduction process follows the “non-overlapping small polaron tunnelling” model between neighbors’ sites. The behavior of dielectric constants such as permittivity and loss coefficient has been interpreted based on the Maxwell-Wagner's theory of interfacial polarization. The curves of imaginary parts of impedance (Z'') and modulus (M'') show a dielectric-relaxation phenomenon in the sample with activation energy near to that determined from the dc conductivity study. Nyquist plots (Z″ vs. Z') show a monotonic decrease in both grain resistance (Rg) and grain boundary resistance (Rgb) with increasing temperature such as Rgb > > Rg. This result confirms that the transport mechanism for Mg0.5Co0.5Fe1.6Al0.4O4 compound is governed by the grain boundaries effect.


2012 ◽  
Vol 10 (8) ◽  
pp. 081601-81604 ◽  
Author(s):  
Shaojun Liu Shaojun Liu ◽  
Haiyuan Li Haiyuan Li ◽  
Yongxing Tang Yongxing Tang ◽  
Lili Hu Lili Hu

2014 ◽  
Vol 29 (8) ◽  
pp. 807
Author(s):  
WANG Min ◽  
NIU Chao ◽  
DONG Zhan-Jun ◽  
CHE Yin-Sheng ◽  
DONG Duo ◽  
...  

2011 ◽  
Vol 10 (2) ◽  
pp. 187-192 ◽  
Author(s):  
Ramona-Crina Suciu ◽  
Marcela Corina Rosu ◽  
Teofil Danut Silipas ◽  
Emil Indrea ◽  
Violeta Popescu ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document