Trilayer-cubic core–shell structure of PbS/EuS nanocrystals revealed by the combination of the synchrotron small-angle X-ray scattering method and energy-dispersive X-ray spectroscopy

2013 ◽  
Vol 42 (45) ◽  
pp. 16216 ◽  
Author(s):  
Hiroyasu Masunaga ◽  
Hiroki Ogawa ◽  
Takuya Nakashima ◽  
Tsuyoshi Kawai ◽  
Takaaki Hikima ◽  
...  
Keyword(s):  
Small Angle ◽  
Shell Structure ◽  
Energy Dispersive ◽  
Core Shell ◽  
Scattering Method ◽  
X Ray ◽  
X Ray Scattering ◽  
Core Shell Structure ◽  
Ray Scattering

scholarly journals Crystallization of BaF2 from droplets of phase separated glass – evidence of a core–shell structure by ASAXS

CrystEngComm ◽  
2020 ◽  
Vol 22 (30) ◽  
pp. 5031-5039
Author(s):  
Armin Hoell ◽  
Vikram Singh Raghuwanshi ◽  
Christian Bocker ◽  
Andreas Herrmann ◽  
Christian Rüssel ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Small Angle ◽  
Shell Structure ◽  
Core Shell ◽  
X Ray Diffraction ◽  
X Ray ◽  
X Ray Scattering ◽  
Transmission Electron ◽  
Core Shell Structure

Glasses with the mol% compositions 1.88 Na2O·15.04 K2O·7.52 Al2O3·69.56 SiO2·6.00 BaF2 and 1.88 Na2O·15.03 K2O·7.52 Al2O3·69.52 SiO2·6.00 BaF2·0.05 SmF3 were studied using X-ray diffraction, transmission electron microscopy, and anomalous small-angle X-ray scattering.

USE OF SANS AND SAXS IN STUDY OF NANOPARTICLES

2005 ◽  
Vol 04 (05n06) ◽  
pp. 987-994 ◽  
Author(s):  
P. S. GOYAL ◽  
V. K. ASWAL
Keyword(s):  
Small Angle ◽  
Shell Structure ◽  
Small Angle Neutron Scattering ◽  
Core Shell ◽  
X Rays ◽  
X Ray ◽  
The Core ◽  
X Ray Scattering ◽  
Structure Of Nanoparticles ◽  
Core Shell Structure

Small Angle Neutron Scattering (SANS) and Small Angle X-ray Scattering (SAXS), anong other available techniques, are the nost sought after techniques for studying the sizes and shapes of nanoparticles. The contrast between particle and its surrounding is different for X-rays and neutrons. Thus a combined SANS and SAXS study, at times, provides information about the core and the shell structure of nanoparticles. This paper gives an introduction to the techniques of SANS and SAXS and shows results of a study of core-shell structure for a micelle (nanaoparticle of organic material).

scholarly journals Synthesis and Advanced Characterization of Polymer-Protein Core-Shell Nanoparticles

Catalysts ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 730
Author(s):  
Erik Sarnello ◽  
Tao Li
Keyword(s):  
Particle Size ◽  
Small Angle ◽  
Core Shell ◽  
Assembly Process ◽  
Shell Nanoparticles ◽  
X Ray ◽  
X Ray Scattering ◽  
Wide Range ◽  
Core Shell Nanoparticles ◽  
Ray Scattering

Enzyme immobilization techniques are widely researched due to their wide range of applications. Polymer–protein core–shell nanoparticles (CSNPs) have emerged as a promising technique for enzyme/protein immobilization via a self-assembly process. Based on the desired application, different sizes and distribution of the polymer–protein CSNPs may be required. This work systematically studies the assembly process of poly(4-vinyl pyridine) and bovine serum albumin CSNPs. Average particle size was controlled by varying the concentrations of each reagent. Particle size and size distributions were monitored by dynamic light scattering, ultra-small-angle X-ray scattering, small-angle X-ray scattering and transmission electron microscopy. Results showed a wide range of CSNPs could be assembled ranging from an average radius as small as 52.3 nm, to particles above 1 µm by adjusting reagent concentrations. In situ X-ray scattering techniques monitored particle assembly as a function of time showing the initial particle growth followed by a decrease in particle size as they reach equilibrium. The results outline a general strategy that can be applied to other CSNP systems to better control particle size and distribution for various applications.

Small-Angle X-Ray Scattering Method to Determine the Size Distribution of Gold Nanoparticles Chemisorbed by Thiol Ligands

2004 ◽  
Vol 43 (11A) ◽  
pp. 7742-7746 ◽  
Author(s):  
Osami Nagao ◽  
Genta Harada ◽  
Tadashi Sugawara ◽  
Akito Sasaki ◽  
Yoshiyasu Ito
Keyword(s):  
Gold Nanoparticles ◽  
Size Distribution ◽  
Small Angle ◽  
Scattering Method ◽  
X Ray ◽  
X Ray Scattering ◽  
Thiol Ligands ◽  
Ray Scattering

scholarly journals Trends in anomalous small-angle X-ray scattering in grazing incidence for supported nanoalloyed and core-shell metallic nanoparticles

2012 ◽  
Vol 208 (1) ◽  
pp. 231-244 ◽  
Author(s):  
P. Andreazza ◽  
H. Khelfane ◽  
O. Lyon ◽  
C. Andreazza-Vignolle ◽  
A. Y. Ramos ◽  
...  
Keyword(s):  
Small Angle ◽  
Metallic Nanoparticles ◽  
Grazing Incidence ◽  
Core Shell ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering
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