In situ ATR-IR observation of nucleation and crystal growth of KH2PO4 in aqueous solution

CrystEngComm ◽  
2013 ◽  
Vol 15 (48) ◽  
pp. 10445 ◽  
Author(s):  
Congting Sun ◽  
Dongfeng Xue
1998 ◽  
Vol 66 (7) ◽  
pp. S487-S490 ◽  
Author(s):  
H. Shindo ◽  
M. Ohashi

2020 ◽  
Author(s):  
Keishiro Yamashita ◽  
Kazuki Komatsu ◽  
Hiroyuki Kagi

An crystal-growth technique for single crystal x-ray structure analysis of high-pressure forms of hydrogen-bonded crystals is proposed. We used alcohol mixture (methanol: ethanol = 4:1 in volumetric ratio), which is a widely used pressure transmitting medium, inhibiting the nucleation and growth of unwanted crystals. In this paper, two kinds of single crystals which have not been obtained using a conventional experimental technique were obtained using this technique: ice VI at 1.99 GPa and MgCl<sub>2</sub>·7H<sub>2</sub>O at 2.50 GPa at room temperature. Here we first report the crystal structure of MgCl2·7H2O. This technique simultaneously meets the requirement of hydrostaticity for high-pressure experiments and has feasibility for further in-situ measurements.


2020 ◽  
Vol 20 (10) ◽  
pp. 6604-6609
Author(s):  
Shanshan Liu ◽  
Guochun Zhang ◽  
Kai Feng ◽  
Yanyang Han ◽  
Tao He ◽  
...  

1995 ◽  
Vol 66 (21) ◽  
pp. 2912-2913 ◽  
Author(s):  
M. Davison ◽  
K. P. O’Donnell ◽  
U. M. Noor ◽  
D. Uttamchandani ◽  
L. E. A. Berlouis

RSC Advances ◽  
2021 ◽  
Vol 11 (33) ◽  
pp. 20486-20497
Author(s):  
Zhiyan Liu ◽  
Rui Ma ◽  
Wenjie Du ◽  
Gang Yang ◽  
Tao Chen

Chitosan hydrogel is regenerated from alkali/urea aqueous solution and the lithium sulfonate second network is introduced by electron beam radiation-initiated in situ free radical polymerization. The freeze-dried aerogel has CO2 capture capacity.


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