Liquid-phase microextraction as an attractive tool for multielement trace analysis in combination with X-ray fluorescence spectrometry: an example of simultaneous determination of Fe, Co, Zn, Ga, Se and Pb in water samples

2011 ◽  
Vol 26 (10) ◽  
pp. 1979 ◽  
Author(s):  
Rafal Sitko ◽  
Karina Kocot ◽  
Beata Zawisza ◽  
Barbara Feist ◽  
Katarzyna Pytlakowska
Keyword(s):  
Liquid Phase ◽  
Simultaneous Determination ◽  
Water Samples ◽  
Trace Analysis ◽  
Fluorescence Spectrometry ◽  
Liquid Phase Microextraction ◽  
X Ray

Determination of Organochlorine Pesticides in Water Samples through Hollow Fiber Membrane-Liquid Phase Microextraction Using Ionic Liquid Material as Extractant

2013 ◽  
Vol 675 ◽  
pp. 260-263 ◽  
Author(s):  
Du Shu Huang ◽  
Ya Shun Chen ◽  
He Ping Yan ◽  
Na Wu ◽  
Wei Liu ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Liquid Phase ◽  
Organochlorine Pesticides ◽  
Hollow Fiber ◽  
Water Samples ◽  
Hollow Fiber Membrane ◽  
Fiber Membrane ◽  
Liquid Phase Microextraction ◽  
Liquid Material

A novel method for determination of organochlorine pesticides residuals (2,4-DDT and 4,4-DDT) in water samples through hollow fiber membrane-liquid phase microextraction using ionic liquid material as extractant coupled with high performance liquid chromatography has been developed. The effect of extraction parameters including pH of the feed solution, stirring rate and extraction time was investigated. The proposed method provided enrichment efficiency of 323 and 289 for 2,4-DDT and 4,4-DDT respectively. The method had good linear range of 0.5-50 μg /L and the limits of detection of the pesticides were 0.1 μg /L.

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