Determination of atrazine in surface waters by combination of POCIS passive sampling and ELISA detection

2011 ◽  
Vol 13 (9) ◽  
pp. 2582 ◽  
Author(s):  
Ivo Černoch ◽  
Milan Fránek ◽  
Iva Diblíková ◽  
Klára Hilscherová ◽  
Tomáš Randák ◽  
...  
Keyword(s):  
Surface Waters ◽  
Passive Sampling

Fluctuations of Annual Precipitation and Water Resources Quality in Ukraine

2016 ◽  
Vol 10 (4s) ◽  
pp. 621-629
Author(s):  
Valentina Pidlisnyuk ◽  
◽  
John Harrington JR ◽  
Yulia Melnyk ◽  
Yuliya Vystavna ◽  
...  
Keyword(s):  
Water Resources ◽  
Surface Waters ◽  
Precipitation Amount ◽  
Ion Concentration ◽  
Annual Precipitation ◽  
Resource Quality ◽  
Phosphate Ion ◽  
Regional Trends

The article focuses on examining the influence of fluctuations in annual precipitation amount on the quality of surface waters. Water quality was estimated with data on BOD, COD and phosphate–ion concentration within five selected regions of Ukraine. Analysis of the precipitation data (1991 – 2010) showed different regional trends. Using the statistics, determination of the interconnection between precipitation amount and water resources quality were done. The obtained regularities and associated uncertainties can be used for prediction of changes in water resource quality and as a guide for future adaptation to possible climate change.

scholarly journals Polydimethylsiloxane Rods for the Passive Sampling of Pesticides in Surface Waters

Water ◽  
2013 ◽  
Vol 5 (3) ◽  
pp. 1366-1379 ◽  
Author(s):  
Azziz Assoumani ◽  
Christelle Margoum ◽  
Yannick Lassalle ◽  
Bernard Herbreteau ◽  
Karine Faure ◽  
...  
Keyword(s):  
Surface Waters ◽  
Passive Sampling

Dosage du Sr-90 dans l'eau des lacs et des rivières du Québec par précipitation avec l'oxine et comptage β

1988 ◽  
Vol 66 (1) ◽  
pp. 174-177 ◽  
Author(s):  
E. Haddad ◽  
L. Zikovsky
Keyword(s):  
Detection Limit ◽  
Surface Waters ◽  
New Method ◽  
The Mean ◽  
Better Than

A new method for the determination of Sr-90 dissolved in surface waters has been developed. It is based on the precipitation of Sr with 8-hydroxyquinoline at pH 11.3 and counting of β particles with energy above 150 keV. The detection limit obtained is 0.5 mBq/L and the mean yield is 28%. The decontamination factors from other β emitters achieved are better than 10 000. This method has been used to measure the Sr-90 in 5 lakes and 5 rivers in Québec and activities ranging from 3 to 15 mBq/L were obtained. This new method is as efficient and reliable as conventional techniques while being less tedious.

scholarly journals Fast UHPLC-MS/MS for the Simultaneous Determination of Azithromycin, Erythromycin, Fluoxetine and Sotalol in Surface Water Samples

2021 ◽  
Vol 11 (18) ◽  
pp. 8316
Author(s):  
Mira Azzi ◽  
Sylvain Ravier ◽  
Assem Elkak ◽  
Bruno Coulomb ◽  
Jean-Luc Boudenne
Keyword(s):  
Surface Water ◽  
Simultaneous Determination ◽  
Surface Waters ◽  
Water Samples ◽  
High Performance ◽  
Chemical Properties ◽  
Environmental Water ◽  
Butyl Ether ◽  
Flight Mass Spectrometry

Chromatographic development for the determination of pharmaceuticals in environmental water samples is particularly challenging when the analytes have significantly different physico-chemical properties (solubility, polarity, pKa) often requiring multiple chromatographic methods for each active component. This paper presents a method for the simultaneous determination of azithromycin, erythromycin (antibiotics), fluoxetine (anti-depressant) and sotalol (b-blocker) in surface waters by ultra-high-performance liquid chromatography coupled with ultra-high-resolution time-of-flight mass spectrometry. These pharmaceuticals—presenting a broad spectrum of polarity (0.24 ≤ log Kow ≤ 4.05)—were separated on a C-18 analytical column, after a simple filtration step for freshwater samples or after a liquid–liquid extraction with Methyl-tertio-butyl ether (MTBE) for seawater samples. The optimized separation method (in terms of nature of column and eluent, elution gradient, and of mass spectrometric parameters), enable one to reach limits of detection ranging between 2 and 7 ng L−1 and limits of quantification between 7 and 23 ng L−1 for the four targeted molecules, within a three minute run. This method was validated using samples collected from three different surface waters in Lebanon (freshwater and seawater) and analytical results were compared with those obtained in surface waters sampled in a French river, equivalent in terms of human activities. Using this method, we report the highest concentration of pharmaceuticals found in surface water (up to 377 ng L−1 and 268 ng L−1, respectively, for azithromycin and erythromycin, in the Litani river, Lebanon).

Anomalously low electrostatic bending stiffness of graphene oxide 2D membranes regulates its environmental fate in aquatic ecosystems

2021 ◽  
Author(s):  
Mohamad Ali Sanjari Shahrezaei ◽  
Seyed Mohammad-Reza Taheri ◽  
Hesam Nikfazan ◽  
Alexandra Satalov ◽  
Mohsen Moazzami Gudarzi ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Environmental Impact ◽  
Surface Waters ◽  
Aquatic Ecosystems ◽  
Environmental Fate ◽  
2D Materials ◽  
Bending Stiffness ◽  
High Importance

Though deemed to be of high importance for the determination of environmental impact of 2D materials upon their release into surface waters, control over the conformational engineering of atomically thin...

scholarly journals Properties, processes and regimes of soil solutions and surface waters

2020 ◽  
Vol 175 ◽  
pp. 12022
Author(s):  
Guriyat Podvolotskaya ◽  
Sergey Belopukhov ◽  
Vitaly Savich ◽  
Andrey Sorokin ◽  
Nikolay Tyutrin
Keyword(s):  
Biological Activity ◽  
Surface Water ◽  
Surface Waters ◽  
Pair Correlation ◽  
Rate Of Change ◽  
Water Soluble ◽  
Soil Solutions ◽  
Different Depths ◽  
Different Soils

Soil solutions and the surface waters are characterized by properties, processes and regimes. Soil solutions of different soils and their surface water have different biological activity and change the activity of dissolved stimulants and inhibitors. The object of the study are soil solutions of the main types of soils obtained in the model experiments with the ratio of soils: water equal to 1:1 and 1: 2, soil solutions and surface water in the flooding of soils with water for 1 week – 3 months. The research method consisted in the assessment of pH, Eh, activity of K, NO3, NH4, Ca, Mg by conventional methods, assessment of concentrations of water-soluble compounds extracted from soils by ionite membranes, in the assessment of biological activity of solutions using biotests. The following is suggested for additional evaluation: the using of cation and anion membranes, determination of interrelation between the properties of waters, equation of pair correlation and multiply regression. The informative value of the gradient of surface water concentrations at different distances from the floor of the reservoir, at different depths of the overwatered soils is shown. The mobility of Ca, Mg, Fe, Mn in soils and the content of their water-soluble forms depends on both pH and Eh, whose influence on the content of water-soluble forms of the considered cations shows the effects of synergy and antagonism. The rate of change in the composition of soil solutions during soil flooding depends on a combination of soil properties, temperature, and duration of flooding. Soil solutions of different soils and their surface waters have differentrates.

Quantitative use of passive sampling data to derive a complete seasonal sequence of flood event loads: a case study for maize herbicides in Luxembourg

2020 ◽  
Vol 22 (2) ◽  
pp. 294-304
Author(s):  
Tom Gallé ◽  
Marion Frelat ◽  
Viola Huck ◽  
Michael Bayerle ◽  
Denis Pittois ◽  
...  
Keyword(s):  
Surface Waters ◽  
Passive Sampling ◽  
Complete Sequence ◽  
Passive Sampler ◽  
Flood Event

Passive sampler monitoring in surface waters can provide a complete sequence of pesticide event loads for an application season.

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