A novel non-centrosymmetric metallophosphate-borate compound via ionothermal synthesis

2009 ◽  
pp. 5287 ◽  
Author(s):  
Zhuojia Lin ◽  
David S. Wragg ◽  
Philip Lightfoot ◽  
Russell E. Morris
Keyword(s):  
Ionothermal Synthesis ◽  
Borate Compound

scholarly journals An accelerated and effective synthesis of zinc borate from zinc sulfate using sonochemistry

2020 ◽  
Vol 43 (1) ◽  
pp. 7-14
Author(s):  
Ali Can Ersan ◽  
Azmi Seyhun Kipcak ◽  
Meral Yildirim Ozen ◽  
Nurcan Tugrul
Keyword(s):  
Inorganic Compounds ◽  
Zinc Borate ◽  
High Yield ◽  
X Ray Diffraction ◽  
Ultrasonic Probe ◽  
Minimum Particle Size ◽  
Effective Synthesis ◽  
Ft Ir ◽  
Lower Temperature ◽  
Borate Compound

AbstractRecently, sonochemistry has been used for the synthesis of inorganic compounds, such as zinc borates. In this study using zinc sulphate heptahydrate (ZnSO4·7H2O) and boric acid (H3BO3) as starting materials, a zinc borate compound in the form of Zn3B6O12·3.5H2O was synthesized using an ultrasonic probe. Product’s characterization was carried out with using X-ray diffraction (XRD), Scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FT-IR) and Raman spectroscopy. Zinc borate compound’s chemical bond structure was observed with Raman and FTIR. From the XRD results it was seen that Zn3B6O12·3.5H2O can be quickly synthesized upon heating at 80°C and 85°C (55 min) or 90°C (45 min) in very high yield (>90%). The minimum particle size obtained was ~143 μm from the SEM results. Zinc borate compound was synthesized at a lower temperature in less time than other synthesized zinc metal compound in literature.

ChemInform Abstract: Ionothermal Synthesis, Crystal Structure, and Magnetic Study of Co2PO4OH Isostructural with Caminite.

ChemInform ◽  
2014 ◽  
Vol 45 (21) ◽  
pp. no-no
Author(s):  
Guangmei Wang ◽  
Martin Valldor ◽  
Eike T. Spielberg ◽  
Anja-Verena Mudring
Keyword(s):  
Crystal Structure ◽  
Magnetic Study ◽  
Ionothermal Synthesis

Template-Free Tuning of Nanopores in Carbonaceous Polymers through Ionothermal Synthesis

2009 ◽  
Vol 21 (8) ◽  
pp. 897-901 ◽  
Author(s):  
Pierre Kuhn ◽  
Aurélien Forget ◽  
Jürgen Hartmann ◽  
Arne Thomas ◽  
Markus Antonietti
Keyword(s):  
Ionothermal Synthesis ◽  
Template Free

Ionothermal Synthesis in an Ionic Liquid and Crystal Structure of [C4H12N2] [CoCl4]

2016 ◽  
Vol 40 (8) ◽  
pp. 475-477 ◽  
Author(s):  
Taifan Sun ◽  
Shide Feng ◽  
Bin Lu ◽  
Qinghai Cai
Keyword(s):  
Crystal Structure ◽  
Ionic Liquid ◽  
Ionothermal Synthesis

Ionothermal synthesis and lithium storage performance of core/shell structured amorphous@crystalline Ni–P nanoparticles

CrystEngComm ◽  
2012 ◽  
Vol 14 (23) ◽  
pp. 7942 ◽  
Author(s):  
Heng Zhang ◽  
Yi Lu ◽  
Chang-Dong Gu ◽  
Xiu-Li Wang ◽  
Jiang-Ping Tu
Keyword(s):  
Core Shell ◽  
Lithium Storage ◽  
Ionothermal Synthesis ◽  
Storage Performance

Ultrafast microwave-enhanced ionothermal synthesis of luminescent crystalline polyimide nanosheets for highly selective sensing of chromium ions

2013 ◽  
Vol 29 ◽  
pp. 128-130 ◽  
Author(s):  
Juan-Ding Xiao ◽  
Ling-Guang Qiu ◽  
Yu-Peng Yuan ◽  
Xia Jiang ◽  
An-Jian Xie ◽  
...  
Keyword(s):  
Chromium Ions ◽  
Ionothermal Synthesis
Sign in / Sign up

Export Citation Format

Share Document