A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS

2005 ◽  
pp. 3472 ◽  
Author(s):  
Jean-Paul Amoureux ◽  
Alexandrine Flambard ◽  
Laurent Delevoye ◽  
Lionel Montagne
2003 ◽  
Vol 23 (4) ◽  
pp. 213-223 ◽  
Author(s):  
Jean-Paul Amoureux ◽  
Cláudia Morais ◽  
Julien Trebosc ◽  
João Rocha ◽  
Christian Fernandez

1982 ◽  
Vol 104 (3) ◽  
pp. 919-920 ◽  
Author(s):  
Eric Oldfield ◽  
Suzanne Schramm ◽  
Michael D. Meadows ◽  
Karen Ann Smith ◽  
Robert A. Kinsey ◽  
...  

1982 ◽  
Vol 13 (20) ◽  
Author(s):  
E. OLDFIELD ◽  
S. SCHRAMM ◽  
M. D. MEADOWS ◽  
K. A. SMITH ◽  
R. A. KINSEY ◽  
...  

1996 ◽  
Vol 51 (5-6) ◽  
pp. 321-329 ◽  
Author(s):  
R. E. Youngman ◽  
U. Werner-Zwanziger ◽  
J. W. Zwanziger

Abstract A comparison of high-resolution NMR methods for quadrupolar nuclei is presented. The samples studied are pure and modified boron oxide glasses, and the boron NMR spectra are recorded using three different experiments capable of high resolution: Double Rotation, Dynamic Angle Spinning, and Multiple-Quantum Magic Angle Spinning. Resolution of the similar ring and nonring boron sites in these glasses, in the presence of disorder, provides a realistic study of the strengths and limitations of these experiments. Conclusions about the relative applicability of these experiments in different situations are presented.


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