The preparation of a highly ordered long-range lamellar silica structure with large interlayer spacingsElectronic supplementary information (ESI) available: Figs. S1–3: XRD, adsorption–desorption isotherms and SEM image. See http://www.rsc.org/suppdata/cc/b2/b204053k/

2002 ◽  
pp. 1614-1615 ◽  
Author(s):  
An-Wu Xu ◽  
Jimmy. C. Yu ◽  
Yue-Peng Cai ◽  
Hua-Xin Zhang ◽  
Li-Zhi Zhang
Keyword(s):  
Long Range ◽  
Supplementary Information ◽  
Sem Image ◽  
Desorption Isotherms ◽  
Adsorption Desorption

scholarly journals Synthesis and Characterization of Nanoporous Monetite Which Can Be Applicable for Drug Carrier

2012 ◽  
Vol 2012 ◽  
pp. 1-5 ◽  
Author(s):  
Esmael Salimi ◽  
Jafar Javadpour
Keyword(s):  
Surface Area ◽  
Cetyltrimethylammonium Bromide ◽  
Drug Carrier ◽  
Synthesis And Characterization ◽  
X Ray ◽  
Plate Shape ◽  
Desorption Isotherms ◽  
Adsorption Desorption

Wormhole-like mesostructured monetite was successfully synthesized using cetyltrimethylammonium bromide (C19H42BrN, CTAB), as a porosity agent. X-ray techniques and FTIR reveal that the crystalline grains consist of highly crystalline pure monetite phase. Monetite rods with diameter around 20–40 nm and length in the range of 50–200 nm were confirmed by FESEM and TEM. Based on N2adsorption-desorption isotherms investigation, surface area increased up to 31.5 m2/g due to the removal of surfactant after calcinations at 400°C. The results indicate that CTAB can not only affect monetite crystallization but also change particles morphology from plate shape to rod-like.

Characterization of mesoporous region by the scanning of the hysteresis loop in adsorption–desorption isotherms

Adsorption ◽  
2021 ◽  
Author(s):  
C. F. Toncón-Leal ◽  
J. Villarroel-Rocha ◽  
M. T. P. Silva ◽  
T. P. Braga ◽  
K. Sapag
Keyword(s):  
Hysteresis Loop ◽  
Desorption Isotherms ◽  
Adsorption Desorption

scholarly journals Synthesis of material MOFs (Fe-BTC) by mechanic-chemical method and its application in the reactive dye degradation

2021 ◽  
Vol 10 (1) ◽  
pp. 21-27
Author(s):  
Tuan Vu Anh ◽  
Hoa Vu Thi ◽  
Manh Nguyen Ba ◽  
Giang Le Ha ◽  
Trang Pham Thi Thu ◽  
...  
Keyword(s):  
Chemical Method ◽  
Dye Degradation ◽  
Reactive Dye ◽  
High Photocatalytic Activity ◽  
N2 Adsorption ◽  
X Ray ◽  
Sem Image ◽  
Grinding Method ◽  
High Initial Concentration ◽  
Adsorption Desorption

Nano Fe-BTC materials were successfully synthesized by mechanical chemical grinding method. Samples were characterized by X-ray difraction (XRD), Fourier-transform infrared spectroscopy (FTIR), N2 adsorption–desorption, Scanning electron microscopy (SEM), Energy-dispersive X-ray spectroscopy (EDS). SEM image of Fe-BTC-60 showed the particle size of 40–60 nm. Fe-BTC nanocomposites were tested for the photocatalytic degradation of reactive yellow 145 (RY-145) in aqueous solution. Fe-BTC composites exhibited high photocatalytic activity. Thus, at pH of 3 and high initial concentration of 100 mg RY-145/L, removal efficiency reached the value of 97.45% after 90 min of reaction.

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