Titania coatings on high and low surface area spherical silica particles by a sol–gel method

2000 ◽  
Vol 10 (12) ◽  
pp. 2818-2822 ◽  
Author(s):  
Jaime Retuert ◽  
Raul Quijada ◽  
Victor M. Fuenzalida
Keyword(s):  
Surface Area ◽  
Sol Gel ◽  
Silica Particles ◽  
Gel Method ◽  
Sol Gel Method ◽  
Spherical Silica ◽  
Spherical Silica Particles ◽  
Titania Coatings

Synthesis of spherical silica particles by sol-gel method and application

2008 ◽  
Vol 19 (8) ◽  
pp. 977-983 ◽  
Author(s):  
Kiyomi Fuchigami ◽  
Yoshinari Taguchi ◽  
Masato Tanaka
Keyword(s):  
Sol Gel ◽  
Silica Particles ◽  
Gel Method ◽  
Sol Gel Method ◽  
Spherical Silica ◽  
Spherical Silica Particles

scholarly journals Synthesis of Spherical Silica by Sol-Gel Method and Its Application as Catalyst Support

2011 ◽  
Vol 10 (2) ◽  
pp. 25
Author(s):  
Anirut Leksomboon ◽  
Bunjerd Jongsomjit
Keyword(s):  
Particle Size ◽  
Ethylene Glycol ◽  
Specific Surface ◽  
Surface Area ◽  
Specific Surface Area ◽  
Sol Gel ◽  
Weight Ratio ◽  
Gel Method ◽  
Sol Gel Method ◽  
Spherical Silica

In this present study, the spherical silica support was synthesized from tetraethyloxysilane (TEOS), water, sodium hydroxide, ethylene glycol and n-dodecyltrimethyl ammonium bromide (C12TMABr). The particle size was controlled by variation of the ethylene glycol co-solvent weight ratio of a sol-gel method preparation in the range of 0.10 to 0.50. In addition, the particle size apparently increases with high weight ratio of co-solvent, but the particle size distribution was broader. The standard deviation of particle diameter is large when the co-solvent weight ratio is more than 0.35 and less than 0.15. However, the specific surface area was similar for all weight ratios ranging from 1000 to 1300 m2/g. The synthesized silica was spherical and has high specific surface area. The cobalt was impregnated onto the obtained silica to produce the cobalt catalyst used for CO2 hydrogenation.</

Synthesis and structural characteristics of high surface area TiO2 aerogels by ultrasonic-assisted sol–gel method

2018 ◽  
Vol 29 (7) ◽  
pp. 075702 ◽  
Author(s):  
Feng Qingge ◽  
Cai Huidong ◽  
Lin Haiying ◽  
Qin Siying ◽  
Liu Zheng ◽  
...  
Keyword(s):  
Surface Area ◽  
Structural Characteristics ◽  
High Surface ◽  
Sol Gel ◽  
High Surface Area ◽  
Gel Method ◽  
Sol Gel Method ◽  
Ultrasonic Assisted

Performance of Polishing Slurries containing Silica Particles grown by Sol-Gel Method

2000 ◽  
Vol 613 ◽  
Author(s):  
Sun Hyuk Bae ◽  
Jae-Hyun So ◽  
Seung-Man Yang ◽  
Do Hyun Kim
Keyword(s):  
Fumed Silica ◽  
Sol Gel ◽  
Particle Growth ◽  
Silica Particles ◽  
Gel Method ◽  
Sol Gel Method ◽  
Irregular Shapes ◽  
Wafer Polishing ◽  
Transmission Electron ◽  
Silica Slurry

ABSTRACTSilica slurry used as abrasives in wafer polishing process is made by dispersing silica particles in an alkali solution. Since commercially available colloidal or fumed silica particles need some modifications to be directly used as abrasive slurry due to their small sizes, irregular shapes or broad size distribution, we have prepared silica abrasives by particle growth of fumed silica or colloidal silica as seeds by sol-gel method. Silica slurries prepared by this step-wise growth from commercial seeds were tested using one-armed polisher for the comparison with commercial slurries and showed the performance comparable to commercial slurries. Microstructures of polishing slurries were investigated using transmission electron microscopy and ARES rheometer. From the result, stability of the slurry was found to be more important than the primary particle sizes for the polishing performance.

scholarly journals Nanosized TiO2Photocatalyst Powder via Sol-Gel Method: Effect of Hydrolysis Degree on Powder Properties

2009 ◽  
Vol 2009 ◽  
pp. 1-8 ◽  
Author(s):  
Nor Hafizah ◽  
Iis Sopyan
Keyword(s):  
Crystal Structure ◽  
Surface Area ◽  
Sol Gel ◽  
Xrd Analysis ◽  
Gel Method ◽  
Sol Gel Method ◽  
Hydrolysis Degree ◽  
Method Effect ◽  
Powder Properties ◽  
Dta Curves

NanosizedTiO2powder was synthesized via sol-gel method using titanium tetraisopoxide (TPT) as the precursor. Mol ratios of water to TPT were varied from 1 (Powder A), 2 (Powder B), 3 (Powder C), and 4 (Powder D) to evaluate effect of hydrolysis degree. TG/DTA curves showed that amorphous phase turned to anatase crystal structure at ca. 415, 337, 310, and339∘C for Powders A, B, C, and D, respectively. XRD analysis showed that all the synthesizedTiO2powders were 100% in anatase form with Powders B and C showing considerably higher crystallinities. The powders obtained at lower water to TPT mol ratios were spherical in shape and they became bar-like shapes higher mol ratios. The lower hydrolysis degree led to higher surface area of the Powder A (24.8 m2/g) compared to Powder B (14.6 m2/g). From phenol photocatalytic measurement, Powder B was the most efficient attributed to its higher crystallinity.

The Influence of Water Content on the Growth of the Hybrid-Silica Particles by Sol-Gel Method

Silicon ◽  
2020 ◽  
Author(s):  
Xijia Zhao ◽  
Yihan Wang ◽  
Jianhui Luo ◽  
Pingmei Wang ◽  
Peiwen Xiao ◽  
...  
Keyword(s):  
Water Content ◽  
Sol Gel ◽  
Silica Particles ◽  
Gel Method ◽  
Sol Gel Method ◽  
Hybrid Silica ◽  
Influence Of Water

Preparation and Performance of Porous Membrane Materials Using the Sol-Gel Method

2010 ◽  
Vol 33 ◽  
pp. 251-253
Author(s):  
Peng Zhang ◽  
Gang Chen ◽  
Bin Guo ◽  
Shu Kang Cheng
Keyword(s):  
Sol Gel ◽  
Porous Membrane ◽  
Silica Particles ◽  
High Tech ◽  
Experimental Conditions ◽  
Preparation Methods ◽  
Gel Method ◽  
Membrane Materials ◽  
Sol Gel Method ◽  
And Performance

Porous membrane materials have the universal use, so it is widely considered as one of the most promising high-tech. Different membranes have different preparation methods. In this paper, the sol-gel method was applied to prepare silica particles using ammonia as catalyst of TEOS hydrolysis, then silica particles were mixed with polyethylene, and finally silica particles were dissolved with hydrofluoric acid, leaving holes, the porous materials were obtained. The results show that: (1) In this experimental conditions, the size of silica particles are closely related to the water content of the system. (2) The size of silica particles affects the agglomeration of particles. The size of silica particles are smaller, the agglomeration is more obvious. (3) As the content of PE increases, the porosity of the samples decreases continuously; in theory, when the content of silica is low, the hole will be greater.

Properties of anion exchange membrane based on polyamine: Effect of functionalized silica particles prepared by sol–gel method

2018 ◽  
Vol 322 ◽  
pp. 85-92 ◽  
Author(s):  
Narges Ataollahi ◽  
Elisa Cappelletto ◽  
Keti Vezzù ◽  
Vito Di Noto ◽  
Gianni Cavinato ◽  
...  
Keyword(s):  
Anion Exchange ◽  
Sol Gel ◽  
Silica Particles ◽  
Anion Exchange Membrane ◽  
Functionalized Silica ◽  
Gel Method ◽  
Sol Gel Method ◽  
Exchange Membrane
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